Structural characterization of the head-to-head isomers of the [Pd2(Ph2Ppy)2Cl2] and [PtPd(Ph2Ppy)2I2] complexes (Ph2Ppy = 2-(diphenylphosphino)pyridine)

Inorganica Chimica Acta

Volumn 359, Issue 9, 2006, Pages 2933-2941

  Párkányi, László ^a   Szalontai, Gábor ^b   Besenyei, Gábor ^a  

^a CHEMICAL RESEARCH CENTER   (Hungary)

^b UNIVERSITY OF PANNONIA   (Hungary)

Author keywords

2 (Diphenylphosphino)pyridine; 31P MAS NMR; Crystal structure; Dimeric palladium complexes; Head to head isomers

Indexed keywords

CRYSTAL STRUCTURE; GEOMETRY; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; PALLADIUM COMPOUNDS; PYRIDINE; SINGLE CRYSTALS;

13C NMR SPECTRUM; 31P MAS-NMR; INTERNAL STRAINS; PALLADIUM COMPLEXES; PHOSPHORUS DONOR; SINGLE CRYSTAL X-RAY DIFFRACTION; SQUARE PLANAR GEOMETRY; STRUCTURAL CHARACTERIZATION;

ISOMERS;

EID: 33747465508     PISSN: 00201693     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.ica.2005.12.021     Document Type: Article

References (33)

1. Holloway R.G., Penfold B.R., Colton R., and McCormick M.J. J. Chem. Soc., Chem. Commun. (1976) 485
2. Brown M.P., Puddephatt R.J., Rashidi M., and Seddon K.R. J. Chem. Soc., Dalton Trans. (1977) 951
3. Lee C.L., Yang Y.P., Rettig S.J., James B.R., Nelson D.A., and Lilga M.A. Organometallics 5 (1986) 2220
4. Besenyei G., Lee C.L., Gulinski J., Rettig S.J., James B.R., Nelson D.A., and Lilga M.A. Inorg. Chem. 26 (1987) 3622
5. Puddephatt R.J. Chem. Soc. Rev. 12 (1983) 99
6. Chaudret B., Delavaux B., and Poilblanc R. Coord. Chem. Rev. 86 (1988) 191
7. Foch I., Párkányi L., Besenyei G., Simándi L.I., and Kálmán A. J. Chem. Soc., Dalton Trans. (1999) 293
8. Besenyei G., Párkányi L., Szalontai G., Holly S., Pápai I., Keresztury G., and Nagy A. Dalton Trans. (2004) 2041
9. Besenyei G., Párkányi L., Foch I., and Simándi L.I. Angew. Chem. Int., Ed. 39 (2000) 956
10. Besenyei G., Lee C.L., Xie Y., and James B.R. Inorg. Chem. 30 (1991) 2446
11. Szalontai G., and Besenyei G. Inorg. Chim. Acta 357 (2004) 4413
12. Szalontai G., and Besenyei G. Monats. Chem. 136 (2005) 663
13. Wu G., and Wasylishen R.E. J. Chem. Phys. 98 (1993) 6138
14. First synthesis:. Maisonnet A., Farr J.P., Olmstead M.M., Hunt C.T., and Balch A.L. Inorg. Chem. 21 (1982) 3961
15. 2Ppy:. Zhang Z.Z., and Cheng H. Coord. Chem. Rev. 147 (1996) 1
16. Espinet P., and Soulantica K. Coord. Chem. Rev. 193-195 (1999) 499
17. Haeberlen U. High Resolution NMR in Solids Suppl. 1 (1976), Academic Press, New York
18. G.M. Sheldrick, shelxs-97 Program for Crystal Structure Solution, University of Göttingen, Germany, 1997.
19. G.M. Sheldrick, shelxl-97 Program for Crystal Structure Refinement, University of Göttingen, Germany, 1997.
20. Spek A.L. J. Appl. Cryst. 36 (2003) 7
21. Ukai T., Kawazura H., Ishii Y., Bonnett J.J., and Ibers J.A. J. Organomet. Chem. 65 (1974) 253
22. Farr J.P., Wood F.E., and Balch A.L. Inorg. Chem. 22 (1983) 3387
23. Suzuki T., and Fujita J. Bull. Chem. Soc. Jpn. 65 (1992) 1016
24. Suzuki T., Iitaka N., Kurachi S., Kita M., Kashiwabara K., Ohba S., and Fujita J. Bull. Chem. Soc. Jpn. 65 (1992) 1817
25. 13C NMR of Transition Metal Phosphine Complex (1979), Springer, Heidelberg
26. Lewitt M.H., Raleigh D.P., Cruzet F., and Griffin R.G. J. Chem. Phys. 92 (1990) 6347
27. Eichele K., Wu G., and Wasylishen R.E. J. Magn. Res. A 101 (1993) 157
28. Tekely P., Cardinnet C., Potrebowski M.J., Sebald A., Reichert D., and Luz Z. J. Chem. Phys. 116 (2002) 7607
29. G. Szalontai, G. Besenyei, unpublished results.
30. Xie Y., Lee C.L., Yang Y., Rettig S.J., and James B.R. Can. J. Chem. 70 (1992) 751
31. Besenyei G., Párkányi L., Gács-Baitz E., and James B.R. Inorg. Chim. Acta 327 (2002) 179
32. Kálmán A., Párkányi L., and Argay Gy. Acta Crystallogr., Sect. B 49 (1993) 1039
33. Fábián L., and Kálmán A. Acta Crystallogr., Sect. B 55 (1999) 1099