Solid effect in magic angle spinning dynamic nuclear polarization

Journal of Chemical Physics

Volumn 137, Issue 5, 2012, Pages

  Corzilius, Björn ^a   Smith, Albert A ^a   Griffin, Robert G ^a  

^a MASSACHUSETTS INSTITUTE OF TECHNOLOGY   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

DOUBLE-QUANTUM; DYNAMIC NUCLEAR POLARIZATION; EFFICIENT COUPLING; FIELD DEPENDENCE; GD-DOTA; HIGH MAGNETIC FIELDS; HOMONUCLEAR; MAGIC ANGLE; MICROWAVE FIELD; MICROWAVE POWER; NUCLEAR POLARIZATION; NUCLEAR SPIN STATE; ORGANIC RADICALS; RATE DETERMINING STEP; RATE LIMITING; SAMPLE VOLUME; SPIN DIFFUSIONS; THEORETICAL MODELS;

EXPERIMENTS; GADOLINIUM; SPIN DYNAMICS; SPIN POLARIZATION;

MAGIC ANGLE SPINNING;

GADOLINIUM 1,4,7,10-TETRAAZACYCLODODECANE-N,N',N'',N'''-TETRAACETATE; GADOTERIC ACID; HETEROCYCLIC COMPOUND; ORGANOMETALLIC COMPOUND; TRITYL DERIVATIVE;

ARTICLE; CHEMISTRY; DIFFUSION; MAGNETIC FIELD; MICROWAVE RADIATION; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; THEORETICAL MODEL;

DIFFUSION; HETEROCYCLIC COMPOUNDS; MAGNETIC FIELDS; MAGNETIC RESONANCE SPECTROSCOPY; MICROWAVES; MODELS, THEORETICAL; ORGANOMETALLIC COMPOUNDS; TRITYL COMPOUNDS;

EID: 84864835513     PISSN: 00219606     EISSN: None     Source Type: Journal    
DOI: 10.1063/1.4738761     Document Type: Article

References (46)

1. A. W. Overhauser, Phys. Rev. 92 (2), 411-415 (1953). 10.1103/PhysRev.92. 411
2. T. R. Carver and C. P. Slichter, Phys. Rev. 92 (1), 212-213 (1953). 10.1103/PhysRev.92.212.2
3. M. Abraham, R. W. Kedzie, and C. D. Jeffries, Phys. Rev. 106 (1), 165-166 (1957). 10.1103/PhysRev.106.165
4. A. Abragam and W. G. Proctor, C. R. Hebd. Seances Acad. Sci. 246 (15), 2253-2256 (1958).
5. C. D. Jeffries, Phys. Rev. 117 (4), 1056-1069 (1960). 10.1103/PhysRev.117.1056
6. A. V. Kessenikh, V. I. Lushchikov, A. A. Manenkov, and Y. V. Taran, Sov. Phys. Solid State 5 (2), 321-329 (1963).
7. C. F. Hwang and D. A. Hill, Phys. Rev. Lett. 18 (4), 110-112 (1967). 10.1103/PhysRevLett.18.110
8. C. F. Hwang and D. A. Hill, Phys. Rev. Lett. 19 (18), 1011-1014 (1967). 10.1103/PhysRevLett.19.1011
9. D. S. Wollan, Phys. Rev. B 13 (9), 3671-3685 (1976). 10.1103/PhysRevB.13. 3671
10. D. S. Wollan, Phys. Rev. B 13 (9), 3686-3696 (1976). 10.1103/PhysRevB.13. 3686
11. M. Goldman, Spin Temperature and Nuclear Magnetic Resonance in Solids (Oxford University Press, London, 1970).
12. A. Abragam and M. Goldman, Rep. Prog. Phys. 41 (3), 395-467 (1978). 10.1088/0034-4885/41/3/002
13. W. T. Wenckebach, Appl. Magn. Reson. 34 (3-4), 227-235 (2008). 10.1007/s00723-008-0121-9
14. J. H. Ardenkjær-Larsen, I. Laursen, I. Leunbach, G. Ehnholm, L. G. Wistrand, J. S. Petersson, and K. Golman, J. Magn. Reson. 133 (1), 1-12 (1998). 10.1006/jmre.1998.1438
15. C. F. Koelsch, J. Am. Chem. Soc. 79 (16), 4439-4441 (1957). 10.1021/ja01573a053
16. T. Maly, G. T. Debelouchina, V. S. Bajaj, K. N. Hu, C. G. Joo, M. L. Mak-Jurkauskas, J. R. Sirigiri, P. C. A. van der Wel, J. Herzfeld, R. J. Temkin, and R. G. Griffin, J. Chem. Phys. 128 (5), 052211 (2008). 10.1063/1.2833582
17. A. B. Barnes, G. De Paepe, P. C. A. van der Wel, K. N. Hu, C. G. Joo, V. S. Bajaj, M. L. Mak-Jurkauskas, J. R. Sirigiri, J. Herzfeld, R. J. Temkin, and R. G. Griffin, Appl. Magn. Reson. 34 (3-4), 237-263 (2008). 10.1007/s00723-008- 0129-1
18. R. G. Griffin and T. F. Prisner, Phys. Chem. Chem. Phys. 12 (22), 5737-5740 (2010). 10.1039/c0cp90019b
19. K. N. Hu, V. S. Bajaj, M. Rosay, and R. G. Griffin, J. Chem. Phys. 126 (4), 044512 (2007). 10.1063/1.2429658
20. K. N. Hu, H. H. Yu, T. M. Swager, and R. G. Griffin, J. Am. Chem. Soc. 126 (35), 10844-10845 (2004). 10.1021/ja039749a
21. C. Song, K.-N. Hu, C.-G. Joo, T. M. Swager, and R. G. Griffin, J. Am. Chem. Soc. 128 (35), 11385-11390 (2006). 10.1021/ja061284b
22. K. N. Hu, C. Song, H. H. Yu, T. M. Swager, and R. G. Griffin, J. Chem. Phys. 128 (5), 052302 (2008). 10.1063/1.2816783
23. Y. Matsuki, T. Maly, O. Ouari, H. Karoui, F. Le Moigne, E. Rizzato, S. Lyubenova, J. Herzfeld, T. Prisner, P. Tordo, and R. G. Griffin, Angew. Chem., Int. Ed. 48 (27), 4996-5000 (2009). 10.1002/anie.200805940
24. A. B. Barnes, B. Corzilius, M. L. Mak-Jurkauskas, L. B. Andreas, V. S. Bajaj, Y. Matsuki, M. L. Belenky, J. Lugtenburg, J. R. Sirigiri, R. J. Temkin, J. Herzfeld, and R. G. Griffin, Phys. Chem. Chem. Phys. 12 (22), 5861-5867 (2010). 10.1039/c003763j
25. K. R. Thurber, W. M. Yau, and R. Tycko, J. Magn. Reson. 204 (2), 303-313 (2010). 10.1016/j.jmr.2010.03.016
26. E. L. Dane, B. Corzilius, E. Rizzato, P. Stocker, T. Maly, A. A. Smith, R. G. Griffin, O. Ouari, P. Tordo, and T. M. Swager, J. Org. Chem. 77 (4), 1789-1797 (2012). 10.1021/jo202349j
27. M. K. Kiesewetter, B. Corzilius, A. A. Smith, R. G. Griffin, and T. M. Swager, J. Am. Chem. Soc. 134 (10), 4537-4540 (2012). 10.1021/ja212054e
28. Y. Hovav, A. Feintuch, and S. Vega, J. Magn. Reson. 207 (2), 176-189 (2010). 10.1016/j.jmr.2010.10.016
29. A. Feintuch, D. Shimon, Y. Hovav, D. Banerjee, I. Kaminker, Y. Lipkin, K. Zibzener, B. Epel, S. Vega, and D. Goldfarb, J. Magn. Reson. 209 (2), 136-141 (2011). 10.1016/j.jmr.2010.12.010
30. Y. Hovav, A. Feintuch, and S. Vega, J. Chem. Phys. 134 (7), 074509 (2011). 10.1063/1.3526486
31. A. A. Smith, B. Corzilius, A. B. Barnes, T. Maly, and R. G. Griffin, J. Chem. Phys. 136 (1), 015101 (2012). 10.1063/1.3670019
32. A. Schweiger and G. Jeschke, Principles of Pulse Electron Paramagnetic Resonance, 1st ed. (Oxford University Press, Oxford, 2001).
33. K. N. Hu, G. T. Debelouchina, A. A. Smith, and R. G. Griffin, J. Chem. Phys. 134 (12), 125105 (2011). 10.1063/1.3564920
34. F. Bloch, W. W. Hansen, and M. Packard, Phys. Rev. 69 (11-1), 680-680 (1946).
35. A. B. Barnes, M. L. Mak-Jurkauskas, Y. Matsuki, V. S. Bajaj, P. C. A. van der Wel, R. DeRocher, J. Bryant, J. R. Sirigiri, R. J. Temkin, J. Lugtenburg, J. Herzfeld, and R. G. Griffin, J. Magn. Reson. 198 (2), 261-270 (2009). 10.1016/j.jmr.2009.03.003
36. L. R. Becerra, G. J. Gerfen, R. J. Temkin, D. J. Singel, and R. G. Griffin, Phys. Rev. Lett. 71 (21), 3561-3564 (1993). 10.1103/PhysRevLett.71.3561
37. A. C. Torrezan, S. T. Han, I. Mastovsky, M. A. Shapiro, J. R. Sirigiri, R. J. Temkin, A. B. Barnes, and R. G. Griffin, IEEE Trans. Plasma Sci. 38 (6), 1150-1159 (2010). 10.1109/TPS.2010.2046617
38. M. Borghini, W. de Boer, and K. Morimoto, Phys. Lett. A 48 (4), 244-246 (1974). 10.1016/0375-9601(74)90487-3
39. T. Maly, L. B. Andreas, A. A. Smith, and R. G. Griffin, Phys. Chem. Chem. Phys. 12 (22), 5872-5878 (2010). 10.1039/c003705b
40. P. Miéville, V. Vitzthum, M. A. Caporini, S. Jannin, S. Gerber-Lemaire, and G. Bodenhausen, Magn. Reson. Chem. 49 (11), 689-692 (2011). 10.1002/mrc.2811
41. E. A. Nanni, A. B. Barnes, Y. Matsuki, P. P. Woskov, B. Corzilius, R. G. Griffin, and R. J. Temkin, J. Magn. Reson. 210 (1), 16-23 (2011). 10.1016/j.jmr.2011.02.001
42. A. Brinkmann, S. K. Vasa, H. Janssen, and A. P. M. Kentgens, Chem. Phys. Lett. 485 (4-6), 275-280 (2010). 10.1016/j.cplett.2009.12.054
43. V. Weis, M. Bennati, M. Rosay, J. A. Bryant, and R. G. Griffin, J. Magn. Reson. 140 (1), 293-299 (1999). 10.1006/jmre.1999.1841
44. B. Corzilius, A. A. Smith, A. B. Barnes, C. Luchinat, I. Bertini, and R. G. Griffin, J. Am. Chem. Soc. 133 (15), 5648-5651 (2011). 10.1021/ja1109002
45. A. Abragam, Principles of Nuclear Magnetic Resonance (Oxford University Press, New York, 1961).
46. See supplementary material at http://dx.doi.org/10.1063/1.4738761 E-JCPSA6-137-035229 for a detailed derivation of the DNP parameters for the zero quantum case.