-
1
-
-
51949102215
-
-
Shibuya, G. M.; Kanady, J. S.; Vanderwal, C. D. J. Am. Chem. Soc. 2008, 130, 12514-12518
-
(2008)
J. Am. Chem. Soc.
, vol.130
, pp. 12514-12518
-
-
Shibuya, G.M.1
Kanady, J.S.2
Vanderwal, C.D.3
-
3
-
-
0003535761
-
-
Wiley-VCH: Weinheim.
-
Rossberg, M.; Lendle, W.; Pfleiderer, G.; Tögel, A.; Dreher, E.-L.; Langer, E.; Rassaerts, H.; Kleinschmidt, P.; Strack, H.; Cook, R.; Beck, U.; Lipper, K.-A.; Torkelson, T. R.; Löser, E.; Beutel, K. K.; Mann, T. Ullmann's Encyclopedia of Industrial Chemistry; Wiley-VCH: Weinheim, 2006.
-
(2006)
Ullmann's Encyclopedia of Industrial Chemistry
-
-
Rossberg, M.1
Lendle, W.2
Pfleiderer, G.3
Tögel, A.4
Dreher, E.-L.5
Langer, E.6
Rassaerts, H.7
Kleinschmidt, P.8
Strack, H.9
Cook, R.10
Beck, U.11
Lipper, K.-A.12
Torkelson, T.R.13
Löser, E.14
Beutel, K.K.15
Mann, T.16
-
5
-
-
79952656192
-
-
Jana, R.; Pathak, T. P.; Sigman., M. S. Chem. Rev. 2011, 111, 1417-1492
-
(2011)
Chem. Rev.
, vol.111
, pp. 1417-1492
-
-
Jana, R.1
Pathak, T.P.2
Sigman, M.S.3
-
8
-
-
59049103973
-
-
Yoshimitsu, T.; Fukumoto, N.; Tanaka, T. J. Org. Chem. 2009, 74, 696-702
-
(2009)
J. Org. Chem.
, vol.74
, pp. 696-702
-
-
Yoshimitsu, T.1
Fukumoto, N.2
Tanaka, T.3
-
9
-
-
77955703986
-
-
Yoshimitsu, T.; Fujumoto, N.; Nakatani, R.; Kojima, N.; Tanaka, T. J. Org. Chem. 2010, 75, 5425-5437
-
(2010)
J. Org. Chem.
, vol.75
, pp. 5425-5437
-
-
Yoshimitsu, T.1
Fujumoto, N.2
Nakatani, R.3
Kojima, N.4
Tanaka, T.5
-
10
-
-
59049083939
-
-
Nilewski, C.; Geisser, R. W.; Carreira, E. M. Nature 2009, 457, 573-576
-
(2009)
Nature
, vol.457
, pp. 573-576
-
-
Nilewski, C.1
Geisser, R.W.2
Carreira, E.M.3
-
11
-
-
67650555672
-
-
Bedke, D. K.; Shibuya, G. M.; Pereira, A.; Gerwick, W. H.; Haines, T. H.; Vanderwal, C. D. J. Am. Chem. Soc. 2009, 131, 7570-7572
-
(2009)
J. Am. Chem. Soc.
, vol.131
, pp. 7570-7572
-
-
Bedke, D.K.1
Shibuya, G.M.2
Pereira, A.3
Gerwick, W.H.4
Haines, T.H.5
Vanderwal, C.D.6
-
12
-
-
77950407857
-
-
Bedke, D. K.; Shibuya, G. M.; Pereira, A. R.; Gerwick, W. H.; Vanderwal, C. D. J. Am. Chem. Soc. 2010, 132, 2542-2543
-
(2010)
J. Am. Chem. Soc.
, vol.132
, pp. 2542-2543
-
-
Bedke, D.K.1
Shibuya, G.M.2
Pereira, A.R.3
Gerwick, W.H.4
Vanderwal, C.D.5
-
14
-
-
84985534727
-
-
Eckert, H.; Foster, B. Angew. Chem., Int. Ed. Engl. 1987, 26, 894-895
-
(1987)
Angew. Chem., Int. Ed. Engl.
, vol.26
, pp. 894-895
-
-
Eckert, H.1
Foster, B.2
-
18
-
-
0026353192
-
-
Goren, Z.; Heeg, M. J.; Mobashery, S. J. Org. Chem. 1991, 56, 7186-7188
-
(1991)
J. Org. Chem.
, vol.56
, pp. 7186-7188
-
-
Goren, Z.1
Heeg, M.J.2
Mobashery, S.3
-
19
-
-
0028856269
-
-
Avdagic, A.; Gelo-Pujic, M.; Sunjic, V. Synthesis 1995, 11, 1427-1431
-
(1995)
Synthesis
, vol.11
, pp. 1427-1431
-
-
Avdagic, A.1
Gelo-Pujic, M.2
Sunjic, V.3
-
20
-
-
34250644975
-
-
Portada, T.; Roje, M.; Raza, Z.; Caplar, V.; Zinic, M.; Sunjic, V. Eur. J. Org. Chem. 2007, 5, 838-856
-
(2007)
Eur. J. Org. Chem.
, vol.5
, pp. 838-856
-
-
Portada, T.1
Roje, M.2
Raza, Z.3
Caplar, V.4
Zinic, M.5
Sunjic, V.6
-
22
-
-
84864132796
-
-
CCDC 879959 (compound 2b) and 879960 (compound 2c) contain the supplementary crystallographic data for this paper, which can be obtained free of charge via, or by emailing data-request@ccdc.cam.ac.uk, or by contacting The Cambridge Crystallographic Data Centre, 12, Union Road, Cambridge CB2 1EZ, U.K. fax: +44 1223 336033. See SI
-
CCDC 879959 (compound 2b) and 879960 (compound 2c) contain the supplementary crystallographic data for this paper, which can be obtained free of charge via www.ccdc.cam.ac.uk/ data-request/cif, or by emailing data-request@ccdc.cam.ac.uk, or by contacting The Cambridge Crystallographic Data Centre, 12, Union Road, Cambridge CB2 1EZ, U.K.; fax: +44 1223 336033. See SI.
-
-
-
-
23
-
-
0141677927
-
-
references therein
-
Lemoucheux, L.; Rouden, J.; Ibazizene, M.; Sobrio, F.; Lasne, M.-C. J. Org. Chem. 2003, 68, 7289-7297 and references therein
-
(2003)
J. Org. Chem.
, vol.68
, pp. 7289-7297
-
-
Lemoucheux, L.1
Rouden, J.2
Ibazizene, M.3
Sobrio, F.4
Lasne, M.-C.5
-
24
-
-
0037462354
-
-
Banwell, M. G.; Coster, M. J.; Harvey, M. J.; Moraes, J. J. Org. Chem. 2003, 68, 613-616
-
(2003)
J. Org. Chem.
, vol.68
, pp. 613-616
-
-
Banwell, M.G.1
Coster, M.J.2
Harvey, M.J.3
Moraes, J.4
-
26
-
-
84864119017
-
-
Ajaykumar, A. S.; Puranik, V. G.; Deshmukh, A. R. A. S. Synthesis 2007, 8, 1159-1164. Deshmukh and co-workers attempted similar triphosgene-TEA chlorination in THF at -20°C using α-branched a diaminoalcohol as a crude dihydrochloride salt (en route to their formal synthesis of (+)-biotin) to give the corresponding chloride in modest yield. Interestingly, when pure 6c was treated under these conditions, the reaction predominantly produced diethylcarbamate 7c and the chlorination product was not observed. We hypothesized that perhaps the rate of chloride substitution in Deshmukh's chemistry was tremendously amplified by the excess residual chloride ions obtained upon evaporation of the 20% HCl/MeOH deprotection solution which was employed to remove the N -Boc precursor
-
(2007)
Synthesis
, vol.8
, pp. 1159-1164
-
-
Ajaykumar, A.S.1
Puranik, V.G.2
Deshmukh, A.R.A.S.3
-
27
-
-
84864126925
-
-
3) for enantiomerically pure (S)-(2-chloropropyl)benzene. Masuda, S.; Nakajima, T.; Suga, S. Bull. Chem. Soc. Jpn. 1983, 56, 1086
-
(1983)
Bull. Chem. Soc. Jpn.
, vol.56
, pp. 1086
-
-
Masuda, S.1
Nakajima, T.2
Suga, S.3
|