Review of HPLC methods and HPLC methods with mass spectrometric detection for direct determination of aspirin with its metabolite(s) in various biological matrices

Biomedical Chromatography

Volumn 26, Issue 8, 2012, Pages 906-941

  Mullangi, Ramesh ^a   Sharma, Kuldeep ^a   Srinivas, Nuggehally R ^b  

^a JUBILANT BIOSYS LTD   (India)

^b Vanthys Pharmaceutical Develpment P Ltd   (India)

Author keywords

Aspirin; Bioanalytical methods; HPLC; LC MS MS; Metabolites; Review

Indexed keywords

BIOMOLECULES; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; MASS SPECTROMETRY; SALICYLIC ACID;

ASPIRIN; BIOANALYTICAL METHODS; BIOLOGICAL MATRIXES; DIRECT DETERMINATION; HPLC; HPLC METHOD; LC-MS-MS; LC.MS/MS; MASS SPECTROMETRIC DETECTION; PROPERTY;

METABOLITES;

ACETYLSALICYLIC ACID; BENZOIC ACID DERIVATIVE; CAFFEINE; DRUG METABOLITE; GENTISIC ACID; PARACETAMOL; PYRIDOSTIGMINE; SALICYLIC ACID; SALICYLURIC ACID;

ACCURACY; ANALYTIC METHOD; BLOOD SAMPLING; BODY FLUID; CENTRIFUGATION; DRUG BLOOD LEVEL; DRUG HALF LIFE; DRUG TRANSFORMATION; DRUG URINE LEVEL; FLUORESCENCE; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; HUMAN; LIQUID CHROMATOGRAPHY; MASS SPECTROMETRY; NONHUMAN; PHARMACODYNAMICS; QUANTITATIVE ANALYSIS; REVIEW; TANDEM MASS SPECTROMETRY; VALIDATION PROCESS;

EID: 84864025618     PISSN: 02693879     EISSN: 10990801     Source Type: Journal    
DOI: 10.1002/bmc.2694     Document Type: Review

References (34)

1. Abu-Qare A and Abou-Donia MB. A validated HPLC method for the determination of pyridostigmine bromide, acetaminophen, acetyl salicylic acid and caffeine in rat plasma and urine. Journal of Pharmaceutical and Biomedical Analysis 2001; 26: 939-947.
2. Amick EN and Mason WD. Determination of aspirin, salicylic acid, salicyluric acid and gentisic acid in human plasma and urine by high pressure liquid chromatography. Analytical Letters 1979; 12: 629-640.
3. Bae SK, Seo KA, Jung EJ, Kim HS, Yeo CW, Shon JH, Park KM, Liu KH and Shin JG. Determination of acetylsalicylic acid and its major metabolite, salicylic acid, in human plasma using liquid chromatography-tandem mass spectrometry: application to pharmacokinetic study of Astrix® in Korean healthy volunteers. Biomedical Chromatography 2008; 22: 590-595.
4. Bakar SK and Niazi S. High-performance liquid chromatographic determination of aspirin and its metabolites in plasma and urine. Journal of Pharmaceutical Sciences 1983; 72: 1020-1023.
5. Brandon RA, Eadie MJ and Smith MT. A sensitive liquid chromatographic assay for plasma aspirin and salicylate concentrations after low doses of aspirin. Therapeutic Drug Monitoring 1985; 7: 216-221.
6. Buskin JN, Upton RA and Williams RA. Improved liquid-chromatography of aspirin, salicylate and salicyluric acid in plasma, with a modification for determining aspirin metabolites in urine. Clinical Chemistry 1982; 28: 1200-1203.
7. Cham BE, Ross-Lee L, Bochner F and Imhoff DM. Measurement and pharmacokinetics of acetylsalicylic acid by a novel high-performance liquid chromatographic assay. Therapeutic Drug Monitoring 1980; 2: 365-372.
8. Gaspari F and Locatelli M. Determination of aspirin and salicylic acid in uremic patient's plasma using reversed-phase high-performance liquid chromatography. Therapeutic Drug Monitoring 1987; 9: 243-247.
9. Harrison LI, Funk ML and Ober RE. High-pressure liquid chromatographic determination of salicylsalicylic acid, aspirin and salicylic acid in human plasma and urine. Journal of Pharmaceutical Sciences 1980; 69: 1268-1271.
10. Hennekens CH, Buring JE, Sandercock P, Collins R and Peto R. Aspirin and other antiplatelet agents in the secondary and primary prevention of cardiovascular disease. Circulation 1989; 80: 749-756.
11. 14C]aspirin in man. Xenobiotica 1982; 12: 601-610.
12. Kees F, Jehnich D and Grobecker H. Simultaneous determination of acetyl salicylic acid and salicylic acid in human plasma by high-performance liquid chromatography. Journal of Chromatography B 1996; 677: 172-177.
13. Klimes J, Sochor J, Zahradnícek M and Sedlácek J. Simultaneous high-performance liquid chromatographic determination of salicylates in whole blood, plasma and isolated erythrocytes. Journal of Chromatography 1992; 584: 221-228.
14. Krivosíková Z, Spustová V and Dzúrik R. A highly sensitive HPLC method for the simultaneous determination of acetylsalicylic, salicylic and salicyluric acids in biologic fluids: pharmacokinetic, metabolic and monitoring implications. Methods and Findings in Experimental and Clinical Pharmacology 1996; 18: 527-532.
15. Kwong TC. Analysis of acetylsalicylic acid and its metabolite by liquid chromatography. Journal of Liquid Chromatography and Related Technologies 1987; 10: 305-321.
16. Lo LY and Bye A. Specific and sensitive method for the determination of aspirin and salicylic acid in plasma using reversed-phase high-performance liquid chromatography. Journal of Chromatography 1980; 181: 473-477.
17. Mason WD and Winer N. Kinetics of aspirin, salicylic acid and salicyluric acid following oral administration of aspirin as a table and two buffered solutions. Journal of Pharmaceutical Sciences 1981; 70: 262-265.
18. Mays DC, Sharp DE, Beach CA, Kershaw RA, Bianchine JR and Gerber N. Improved method for the determination of aspirin and its metabolites in biological fluids by high-performance liquid chromatography: applications to human and animal studies. Journal of Chromatography B 1984; 311: 301-309.
19. McMahon G and Kelly MT. Determination of aspirin and salicylic acid in human plasma by column-switching liquid chromatography using on-line solid-phase extraction. Analytical Chemistry 1998; 70: 409-414.
20. Nieder M and Jaeger H. Determination of acetylsalicylic acid and salicylic acid in blood and plasma by HPLC. Journal High Resolution Chromatography and Chromatography Communications 1983; 6: 655-660.
21. O'Kruk RJ, Adams MA and Philp RB. Rapid and sensitive determination of acetylsalicylic acid and its metabolites using reversed-phase high-performance liquid chromatography. Journal of Chromatography 1984; 310: 343-352.
22. Peng GW, Gadalla MAF, Smith V, Peng A and Chiou WL. Simple and rapid high-pressure liquid chromatographic simultaneous determination of aspirin, salicylic acid and salicyluric acid in plasma. Journal of Pharmaceutical Sciences 1978; 67: 710-712.
23. Pirola R, Bareggi SR and De Benedittis G. Determination of acetylsalicylic acid and salicylic acid in skin and plasma by high-performance liquid chromatography. Journal of Chromatography B 1998; 705: 309-315.
24. Reidl U. Determination of acetylsalicylic acid and metabolites in biological fluids by high-performance liquid chromatography. Journal of Chromatography 1983; 272: 325-331.
25. Reilly IA and FitzGerald GA. Aspirin in cardiovascular diseases. Drugs 1988; 35: 154-176.
26. Rumble RH, Roberts MS and Wanwimolruk S. Determination of aspirin and its major metabolites in plasma by high-performance liquid chromatography without solvent extraction. Journal of Chromatography 1981; 225: 252-260.
27. Shen J, Wanwimolruk S, Clark CR and Roberts MS. A sensitive assay for aspirin and its metabolites using reversed-phase ion-pair high-performance liquid chromatography. Journal of Liquid Chromatography 1990; 13: 751-761.
28. Siebert DM and Bochner F. Determination of plasma aspirin and salicylic acid concentrations after low aspirin doses by high-performance liquid chromatography with post-column hydrolysis and fluorescence detection. Journal of Chromatography 1987; 420: 425-431.
29. Srinivas NR. Applicability of bioanalysis of multiple analytes in drug discovery and development: review of select case studies including assay development considerations. Biomedical Chromatography 2006; 20: 383-414.
30. Tebbett IR, Omile CI and Danesh B. Determination of paracetamol, salicylic acid and acetyl salicylic acid in serum by high-performance liquid chromatography. Journal of Chromatography 1985; 329: 196-198.
31. Wahlin-Boll E, Brantmark B, Hanson A, Melander A and Nilsson C. High-pressure liquid chromatographic determination of acetylsalicylic acid, salicylic acid, diflunisal, indomethacin, indoprofen and indobufen. European Journal of Clinical Pharmacology 1981; 20: 375-378.
32. Wilson JT, Howell RL, Holladay MW, Brilis GM, Chrastil J, Watson JT and Taber DF. Gentisuric acid: metabolic formation in animals and identification as a metabolite of aspirin in human. Clinical Pharmacology and Therapeutics 1978; 23: 635-643.
33. Xu X, Koetzner L, Boulet J, Maselli H, Beyenhof J and Grover G. Rapid and sensitive determination of acetylsalicylic acid and salicylic acid in plasma using liquid chromatography-tandem mass spectrometry: application to pharmacokinetic study. Biomedical Chromatography 2009; 23: 973-979.
34. Yamamoto E, Takakuwa S, Kato T and Asakawa N. Sensitive determination of aspirin and its metabolites in plasma by LC-UV using on-line solid-phase extraction with methycellulose-immobilized anion-exchange restricted access media. Journal of Chromatography B 2007; 846: 132-138.