Superficially porous particles columns for super fast HPLC separations

Biomedical Chromatography

Volumn 26, Issue 8, 2012, Pages 1001-1008

  Ali, Imran ^a   Al Othman, Zeid A ^b   Al Za'abi, Mohammed ^c  

^a JAMIA MILLIA ISLAMIA CENTRAL UNIVERSITY   (India)

^b KING SAUD UNIVERSITY   (Saudi Arabia)

^c Sultan Qaboos University College of Medicine and Health Sciences   (Oman)

Author keywords

Ascentis Express; Halo; Kinetex; Separation mechanism; Super fast separations; Superficially porous silica particles

Indexed keywords

POROUS MATERIALS; SILICA GEL;

ASCENTIS EXPRESS; FAST SEPARATION; HALO; KINETEX; PARTICLE COLUMN; POROUS SILICA; SEPARATION MECHANISM; SILICA PARTICLES; SUPER FAST SEPARATION; SUPERFICIALLY POROUS SILICUM PARTICLE;

PORE SIZE;

ACETOPHENONE; AFLATOXIN; AMIDE; AMITRIPTYLINE; AMOXAPINE; BENZENE; BOVINE SERUM ALBUMIN; BRADYKININ; CAFFEINE; CATECHIN; CLOMIPRAMINE; CYANURIC ACID; DESIPRAMINE; DOXEPIN; EPIGALLOCATECHIN; IMIPRAMINE; INSULIN; KALLIDIN; NAPHTHALENE; NORDOXEPIN; NORTRIPTYLINE; PHENOL; POLYSTYRENE; RESORCINOL; SILICON DIOXIDE; SULFATHIAZOLE; TIANEPTINE; TOLUENE; UNINDEXED DRUG; URACIL;

COLUMN CHROMATOGRAPHY; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; INTERMETHOD COMPARISON; MEASUREMENT; PARTICLE SIZE; POROSITY; REVIEW; SEPARATION TECHNIQUE; STRUCTURE ANALYSIS; TRANSPORT KINETICS;

EID: 84863999292     PISSN: 02693879     EISSN: 10990801     Source Type: Journal    
DOI: 10.1002/bmc.2690     Document Type: Review

References (38)

1. Abrahim A, Al-Sayah M, Skrdla P, Bereznitski Y, Chen Y and Wu N. Practical comparison of 2.7 micron fused-core silica particles and porous sub-2 micron particles for fast separations in pharmaceutical process development. Journal of Pharmaceutical and Biomedical Analysis 2010; 51: 131-137.
2. Ali I, Gaitonde VD and Grahn A. Halo columns: new generation technology for high speed liquid chromatography. Journal of Chromatographic Science 2010; 48: 386-394.
3. Ali I, Al-Kindy SMZ, Suliman FO and Alam SD. Fast analysis of flavonoids in apple juice on new generation Halo column by SPE-HPLC. Analytical Methods 2011; 3: 2836-2841.
4. Alpert AJ. Hydrophilic-interaction chromatography for the separation of peptides, nucleic acids and other polar compounds. Journal of Chromatography. A 1990; 499: 177-196.
5. Bayram-Hahn Z, Grimes BA, Lind AM, Skudas R, Unger KK, Galarneau A, Iapichella J and Fajula F. Pore structural characteristics, size exclusion properties and column performance of two mesoporous amorphous silicas and their pseudomorphically transformed MCM-41 type derivatives. Journal of Separation Science 2007; 30: 3089-3103.
6. Berger TA. Characterization of a 2.6μm Kinetex porous shell hydrophilic interaction liquid chromatography column in supercritical fluid chromatography with a comparison to 3μm totally porous silica. Journal of Chromatography. A 2011; 1218: 4559-4568.
7. Cavazzini A, Gritti F, Kaczmarski K, Marchetti N and Guiochon G. Mass-transfer kinetics in a shell packing material for chromatography. Analytical Chemistry 2007; 79: 5972-5979.
8. Cunliffe JM and Maloney TD. Fused-core particle technology as an alternative to sub-2-microm particles to achieve high separation efficiency with low backpressure. Journal of Separation Science 2007; 30: 3104-3109.
9. DeStefano JJ, Langlois TJ and Kirkland JJ. Characteristics of superficially porous silica particles for fast HPLC: Some performance comparisons with sub-2-μm particles. Journal of Chromatography Science, 2008; 46: 254-260.
10. Done JN, Kennedy GJ and Knox JH. Revolution in liquid chromatography. Nature 1972; 237: 77-81.
11. Fanigliulo A, Cabooter D, Bellazzi G, Tramarin D, Allieri B, Rottigni A and Desmet G. Comparison of performance of high-performance liquid chromatography columns packed with superficially and fully porous 2.5μm particles using kinetic plots. Journal of Separation Science 2010; 33: 3655-3665.
12. Fekete S, Fekete J and Ganzler K. Shell and small particles: Evaluation of new column technology. Journal of Pharmaceutical and Biomedical Analysis 2009a; 49: 64-71.
13. Fekete S, Fekete J and Ganzler K. Characterization of new types of stationary phases for fast liquid chromatographic applications. Journal of Pharmaceutical and Biomedical Analysis 2009b; 50: 703-709.
14. Gritti F, Cavazzini A, Marchetti N and Guiochon G. Comparison between the efficiencies of columns packed with fully and partially porous C18 bonded silica materials. Journal of Chromatography A 2007a; 1157: 289-303.
15. Gritti F and Guiochon G. Comparative study of the performance of columns packed with several new fine silica particles. Would the external roughness of the particles affect column properties?. Journal of Chromatography A 2007b; 1166: 30-46.
16. Gritti F and Guiochon G. The mass transfer kinetics in columns packed with Halo-ES shell particles. Journal of Chromatography A 2011c; 1218: 907-921.
17. Gritti F, Leonardis I, Shock D, Stevenson P, Shalliker A and Guiochon G. Performance of columns packed with the new shell particles, Kinetex C18. Journal of Chromatography A 2010d; 1217: 1589-1603.
18. 18 particles in gradient elution chromatography. Journal of Chromatography A 2010e; 1217: 1604-1615.
19. Gritti F, Sanchez CA, Farkas T and Guiochon G. Achieving the full performance of highly efficient columns by optimizing conventional benchmark high performance liquid chromatography instruments. Journal of Chromatography A 2010f; 1217: 3000-3012.
20. Gritti F and Guiochon G. Non-invasive measurement of eddy diffusion in very efficient liquid chromatography columns packed with sub-3 mm shell particles. Chemical Engineering and Science 2010g; 65: 6327-6340.
21. Gritti F and Guiochon G. Comparison between the loading capacities of columns packed with partially and totally porous fine particles. What is the effective surface area available for adsorption?. Journal of Chromatography A 2007h; 1176: 107-122.
22. Grumbach ES, Wagrowski-Diehl MD, Mazzeo JR, Alden B and Iraneta PC. Hydrophilic interaction chromatography using silica columns for the retention of polar analytes and enhanced ESI-MS sensitivity. LC-GC 2004; 22: 1010-1023.
23. Hemström P and Irgun K. Hydrophilic interaction chromatography. Journal of Separation Science 2006; 29: 1784-1821.
24. Kaczmarski K and Guiochon G. Modeling of the mass-transfer kinetics in chromatographic columns packed with shell and pellicular particles. Analytical Chemistry 2007; 79: 4648-4656.
25. Kirkland JJ. Ultra-fast reversed-phase high-performance liquid chromatographic separations: an overview. Journal of Chromatographic Science 2000; 38: 535-544.
26. Kirkland JJ, Truszkowski FA, Dilks CH and Engel GS. Superficially porous silica microspheres for fast high-performance liquid chromatography of macromolecules. Journal of Chromatography. A 2000; 890: 3-13.
27. MAC-MOD Analytical Inc. Quick Tips for Converting Conventional Reversed Phase HPLC Separations to Ultra Fast Separations. MAC-MOD Analytical Inc.: Chadds Ford, PA, 2007. Available from:.
28. Majors RE. Anatomy of an LC column from the beginning to modern day. LC-GC 2006; 24: 248-266.
29. Marchetti N and Guiochon G. High peak capacity separations of peptides in reversed-phase gradient elution liquid chromatography on columns packed with porous shell particles. Journal of Chromatography. A 2007; 1176: 206-216.
30. Marchetti N, Cavazzini A, Gritti F and Guiochon G. Gradient elution separation and peak capacity of columns packed with porous shell particles. Journal of Chromatography. A 2007; 1163: 203-211.
31. McCalley DV. Evaluation of the properties of a superficially porous silica stationary phase in hydrophilic interaction chromatography. Journal of Chromatography. A 2008; 1193: 85-91.
32. Oláh E, Fekete S, Fekete J and Ganzler K. Comparative study of new shell-type, sub-2 micron fully porous and monolith stationary phases, focusing on mass-transfer resistance. Journal of Chromatography. A 2010; 1217: 3642-3653.
33. Pesek J and Matyska MT. A comparison of two separation modes: Hilic and aqueous normal phase chromatography. LC-GC 2007; 25: 480-490.
34. Rogers SD and Dorsey JG. Chromatographic silanol activity test procedures: the quest for a universal test. Journal of Chromatography. A 2000; 892: 57-65.
35. Tanaka N, Kobayashi H, Ishizuka N, Minakuchi H, Nakanishi K, Hosoya K and Ikegami T. Monolithic silica columns for high-efficiency chromatographic separations. Journal of Chromatography. A 2002; 965: 35-49.
36. Thompson JW, Mellors JS, Eschelbach JW and Jorgenson JW. Recent advances in ultra-high pressure liquid chromatography. LC-GC 2006; 24: 16-21.
37. Yang P, Litwinski GR, Pursch M, McCabe T and Kuppannan K. Separation of natural product using columns packed with fused-core particles. Journal of Separation Science 2009; 32: 1816-1822.
38. Yang P, McCabe T and Pursch M. Practical comparison of LC columns packed with different superficially porous particles for the separation of small molecules and medium size natural products. Journal of Separation Science 2011; 34: 2975-2982.