Time-dependent column performance of cholesterol-based stationary phases for HPLC by LC characterization and solid-state NMR spectroscopy

Journal of Separation Science

Volumn 35, Issue 13, 2012, Pages 1582-1588

  Yeman, Helen ^a   Nicholson, Tim M ^a   Friebolin, Volker ^a   Steinhauser, Lisa ^a   Matyska, Maria T ^b   Pesek, Joseph J ^b   Albert, Klaus ^a  

^a UNIVERSITY OF TÜBINGEN   (Germany)

^b SAN JOSE STATE UNIVERSITY   (United States)

Author keywords

Cholesterol based stationary phases; Column performance; HPLC; Solid state NMR spectroscopy

Indexed keywords

CHEMICALLY BONDED; COLUMN PERFORMANCE; HPLC; LABORATORY CONDITIONS; LONG TERM STABILITY; SEPARATION BEHAVIORS; SOLID STATE NMR; SOLID-STATE NMR SPECTROSCOPY; SPACER MOLECULES; STANDARD REFERENCE MATERIAL; STATIONARY PHASIS; SYNTHESIS ROUTE; THREE PHASIS; TIME-DEPENDENT;

CHOLESTEROL; COMPLEXATION; SEPARATION; SOLID STATE PHYSICS; SURFACE CHEMISTRY; SYNTHESIS (CHEMICAL);

NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY;

10 UNDECANOATE CHOLESTEROL; AMINOPROPYL CHOLESTEROL; CHOLESTEROL; N 6 AMINOHEXYL AMINOPROPYL; UNCLASSIFIED DRUG;

ARTICLE; CHOLESTEROL SYNTHESIS; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; LIQUID CHROMATOGRAPHY; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; PHYSICAL CHEMISTRY; PRIORITY JOURNAL;

ADSORPTION; CHOLESTEROL; CHROMATOGRAPHY, HIGH PRESSURE LIQUID; MAGNETIC RESONANCE SPECTROSCOPY; MOLECULAR STRUCTURE; TIME FACTORS;

EID: 84863646802     PISSN: 16159306     EISSN: 16159314     Source Type: Journal    
DOI: 10.1002/jssc.201200079     Document Type: Article

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