Preparation of a Pyrazosulfuron-Ethyl Imprinted Polymer with Hydrophilic External Layers by Reversible Addition-Fragmentation Chain Transfer Precipitation and Grafting Polymerization

Analytical Letters

Volumn 44, Issue 16, 2011, Pages 2617-2632

  Yang, Lixia ^a   Fan, Zhijin ^a   Wang, Teng ^a   Cai, Wensheng ^a   Yang, Meixian ^a   Jiang, Ping ^a   Zhang, Min ^a   Dong, Xiangchao ^a  

^a NANKAI UNIVERSITY   (China)

Author keywords

Molecularly imprinted polymer; Precipitation polymerization; Pyrazosulfuron ethyl; Reversible addition fragmentation chain transfer process; Surface modification

Indexed keywords

EID: 84863255858     PISSN: 00032719     EISSN: 1532236X     Source Type: Journal    
DOI: 10.1080/00032719.2011.553007     Document Type: Article

References (29)

1. Barner, L. 2009. Synthesis of microspheres as versatile functional scaffolds for materials science applications. Adv. Mater. 21 (29): 2547 - 2553.
2. Barner, L., C. Li, X. J. Hao, M. H. Stenzel, C. Barner-Kowollik, and T. P. Davis. 2004. Synthesis of core-shell poly(divinylbenzene) microspheres via reversible addition fragmentation chain transfer graft polymerization of styrene. J. Polymer Sci. A. 42 (20): 5067 - 5076.
3. Barsbay, M., O. Guven, T. P. Davis, C. Barner-Kowollik, and L. Barner. 2009. RAFT-mediated polymerization and grafting of sodium 4-styrenesulfonate from cellulose initiated via gamma-radiation. Polymer, 50 (4): 973 - 982.
4. Beltran, A., R. M. Marce, P. A. G. Cormack, and E. Borrull. 2009. Synthesis by precipitation polymerisation of molecularly imprinted polymer microspheres for the selective extraction of carbamazepine and oxcarbazepine from human urine. J. Chromatogr. A 1216 (12): 2248 - 2253.
5. Brandrup, J., E. H. Immergut, and E. A. Grulke. 1999. Polymer Handbook. New York, USA: Wiley.
6. Carabias-Martinez, R., E. Rodriguez-Gonzalo, E. Herrero-Hernandez, and M. E. Diaz-Garcia. 2005. Development and characterisation of a molecularly imprinted polymer prepared by precipitation polymerisation for the determination of phenylurea herbicides. J. Sep. Sci. 28 (5): 453 - 461.
7. Cassiano, N. M., V. V. Lima, R. V. Oliveira, A. C. de Pietro, and Q. B. Cass. 2006. Development of restricted-access media supports and their application to the direct analysis of biological fluid samples via high-performance liquid chromatography. Anal. Bioanal. Chem. 384 (7-8): 1462 - 1469.
8. Chiefari, J., Y. K. Chong, F. Ercole, J. Krstina, J. Jeffery, T. P. T. Le, R. T. A. Mayadunne, G. F. Meijs, C. L. Moad, G. Moad, E. Rizzardo, and S. H. Thang. 1998. Living free-radical polymerization by reversible addition-fragmentation chain transfer: The RAFT process. Macromolecules, 31 (16): 5559 - 5562.
9. Chopra, D., T. P. Mohan, K. S. Rao, and T. N. Guru-Row. 2004. Ethyl 5-[(4,6-dimethoxypyrimidin-2-yl)ureidosulfonyl]-1-methyl-1 H-pyrazole-4-carboxylate. Acta Crystallogr. Sect. E. 60: 2418 - 2420.
10. Dirion, B., Z. Cobb, E. Schillinger, L. I. Andersson, and B. Sellergren. 2003. Water-compatible molecularly imprinted polymers obtained via high-throughput synthesis and experimental design. J. Am. Chem. Soc. 125 (49): 15101 - 15109.
11. Frisch, M. J., G. W. Trucks, H. B. Schlegel, G. E. Scuseria, M. A. Robb, J. R. Cheeseman, et al. 2004. Gaussian 03; rev. C.02. Wallingford, CT, USA: Gaussian Inc.
12. Haginaka, J., and H. Sanbe. 2000. Uniform-sized molecularly imprinted polymers for 2-arylpropionic acid derivatives selectively modified with hydrophilic external layer and their applications to direct serum injection analysis. Anal. Chem. 72 (21): 5206 - 5210.
13. Haginaka, J., H. Takekira, K. Hosoya, and N. Tanaka. 1999. Uniform-sized molecularly imprinted polymer for (S)-naproxen selectively modified with hydrophilic external layer. J. Chromatogr. A 849 (2): 331 - 339.
14. Hogendoorn, E., and P. van Zoonen. 2000. Recent and future developments of liquid chromatography in pesticide trace analysis. J. Chromatogr. A. 892 (1-2): 435 - 453.
15. Hogendoorn, E. A., E. Dijkman, B. Baumann, C. Hidalgo, J. V. Sancho, and F. Hernandez. 1999. Strategies in using analytical restricted access media columns for the removal of humic acid interferences in the trace analysis of acidic herbicides in water samples by coupled column liquid chromatography with UV detection. Anal. Chem.71(6): 1111-1118.
16. Krevelen, D. W. 1990. Properties of Polymers., 3rd ed. Amsterdam, The Netherland: Elsevier Science Publishers.
17. Lai, J. P., M. L. Yang, R. Niessner, and D. Knopp. 2007. Molecularly imprinted microspheres and nanospheres for di(2-ethylhexyl)phthalate prepared by precipitation polymerization. Anal. Bioanal. Chem. 389 (2): 405 - 412.
18. Lee, A. W. M., Chan, W. H., and Wong, H. C. 1988. One pot phase-transfer synthesis of trithiocarbonates from carbon-disulfide and alkyl-halides. Synth. Commun. 18 (13): 1531 - 1536.
19. Li, M., X. C. Lin, and Z. H. Xie. 2009. Investigation of enantiomer recognition of molecularly imprinted polymeric monoliths in pressurized capillary electrochromatography screening the amino acids and their derivatives. J. Chromatogr. A. 1216 (27): 5320 - 5326.
20. Pan, G. Q., B. Y. Zu, X. Z. Guo, Y. Zhang, C. X. Li, and H. Q. Zhang. 2009. Preparation of molecularly imprinted polymer microspheres via reversible addition-fragmentation chain transfer precipitation polymerization. Polymer, 50 (13): 2819 - 2825.
21. Puoci, F., F. Iemma, G. Cirillo, M. Curcio, O. I. Parisi, U. G. Spizzirri, and N. Picci. 2009. New restricted access materials combined to molecularly imprinted polymers for selective recognition/release in water media. Eur. Polym. J. 45 (6): 1634 - 1640.
22. Sambe, H., K. Hoshina, and J. Haginaka. 2007. Molecularly imprinted polymers for triazine herbicides prepared by multi-step swelling and polymerization method - their application to the determination of methylthiotriazine herbicides in river water. J. Chromatogr. A. 1152 (1-2): 130 - 137.
23. Sanbe, H., and J. Haginaka. 2003. Restricted access media-molecularly imprinted polymer for propranolol and its application to direct injection analysis of beta-blockers in biological fluids. Analyst, 128 (6): 593 - 597.
24. Tamayo, F. G., E. Turiel, and A. Martin-Esteban. 2007. Molecularly imprinted polymers for solid-phase extraction and solid-phase microextraction: Recent developments and future trends. J. Chromatogr. A. 1152 (1-2): 32 - 40.
25. Tang, K. J., S. W. Chen, X. H. Gu, H. J. Wang, J. Dai, and J. Tang. 2008. Preparation of molecularly imprinted solid phase extraction using bensulfuron-methyl imprinted polymer and clean-up for the sulfonylurea-herbicides in soybean. Anal. Chim. Acta. 614 (1): 112 - 118.
26. Wang, J. F., P. A. G. Cormack, D. C. Sherrington, and E. Khoshdel. 2003. Monodisperse, molecularly imprinted polymer microspheres prepared by precipitation polymerization for affinity separation applications. Angew. Chem. Int. Ed. 42 (43): 5336 - 5338.
27. Ye, L., P. A. G. Cormack, and K. Mosbach. 2001. Molecular imprinting on microgel spheres. Anal. Chim. Acta. 435 (1): 187 - 196.
28. Yoshimatsu, K., K. Reimhult, A. Krozer, K. Mosbach, K. Sode, and L. Ye. 2007. Uniform molecularly imprinted microspheres and nanoparticles prepared by precipitation polymerization: The control of particle size suitable for different analytical applications. Anal. Chim. Acta. 584 (1): 112 - 121.
29. Zhang, Y., and X. C. Dong. 2008. Evaluation of enrofloxacin imprinted polymeric microspheres synthesized with living/controlled radical polymerization. Fenxi Ceshi Xuebao, 27: 1025 - 1030.