Enhancing the quality of separation in one-dimensional peptide mapping using mathematical transformation

Chromatographia

Volumn 75, Issue 5-6, 2012, Pages 305-312

  Berky, Róbert ^a   Fekete, Szabolcs ^a   Fekete, Jenö ^a  

^a BUDAPEST UNIVERSITY OF TECHNOLOGY AND ECONOMICS   (Hungary)

Author keywords

Acquity CSH column; Biosimilar; Core shell particles; Enhanced resolution; Liquid chromatography; Peptide map

Indexed keywords

ARTICLE; FLOW RATE; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; LIQUID CHROMATOGRAPHY; MATHEMATICAL MODEL; PARTICLE SIZE; PEPTIDE MAPPING; POROSITY; PRIORITY JOURNAL; PROTEIN ANALYSIS; PROTEIN STRUCTURE;

EID: 84862897700     PISSN: 00095893     EISSN: 16121112     Source Type: Journal    
DOI: 10.1007/s10337-012-2181-0     Document Type: Article

References (20)

1. Swartz M, Krull I (2009) Analytical Method Validation for Bio-technology Proteins, Peptides, and Antibodies. Chromatography-online, LCGC http://www.chromatographyonline.findanalytichem. com/lcgc/. Accessed July 2009
2. Validation Of Analytical Procedures: Text and Methodology Q2(R1) (1994) ICH harmonised tripartite guideline. http://www. ich.org. Accessed 27 Oct 1994
3. Specifications: Test Procedures and Acceptance Criteria for Bio-technological/Biological Products Q6B (1999) ICH Harmonised Tripartite Guideline. http://www.ich.org. Accessed 10 March 1999
4. Comparability of Biotechnological/Biological Products Subject to Changes in their Manufacturing Process Q5E (2004) ICH Harmonised Tripartite Guideline. http://www.ich.org. Accessed 18 Nov 2004
5. Rathore AS (2009) Follow-on protein products: scientific issues, development and challenges. Trends Biotechnol 27:698-705
6. Facchetti I, Vallaa A, Vigevania A (1993) RP-HPLC peptide mapping methods for the analysis of recombinant human pro-urokinase. J Pharm Biomed Anal 11:737-744 (Pubitemid 23273043)
7. Marchetti N, Guiochon G (2007) High peak capacity separations of peptides in reversed-phase gradient elution liquid chromatog-raphy on columns packed with porous shell particles. J Chroma-togr A 1176:206-216 (Pubitemid 350184022)
8. Molnar I (2002) Computerized design of separation strategies by reversed-phase liquid chromatography: development of DryLab software. J Chromatogr A 965:175-194 (Pubitemid 34876317)
9. Shalliker RA, Stevenson PG, Shock D, Mnatsakanyan M, Dasgupta PK, Guiochon G (2010) Application ofpower functions to chromatographic data for the enhancement of signal to noise ratios and separation resolution. J Chromatogr A 1217:5693-5699
10. Gritti F, Guiochon G (2011) The mass transfer kinetics in columns packed with Halo-ES shell particles. J Chromatogr A 1218:907-921
11. Fekete S, Fekete J (2011) Fast gradient screening of pharma-ceuticals with 5 cm long, narrow bore reversed-phase columns packed with sub-3 μ m core-shell and sub-2 μ m totally porous particles. Talanta 84:416-423
12. Gritti F, Guiochon G (2007) Comparative study of the perfor-mance of columns packed with several new fine silica particles: would the external roughness of the particles affect column properties? J Chromatogr A 1166:30-46 (Pubitemid 47361151)
13. Gritti F, Guiochon G (2010) Performance ofcolumns packed with the new shell Kinetex-C18 particles in gradient elution chroma-tography. J Chromatogr A 1217:1604-1615
14. Schuster SA, Wagner BM, Boyes BE, Kirkland JJ (2010) Wider pore superficially porous particles for peptide separations by HPLC. J Chromatogr Sci 48:566-571
15. Fekete S, Ganzler K, Fekete J (2011) Efficiency of the new sub-2 μ m core-shell (KinetexTM) column in practice, applied for small and large molecule separation. J Pharm Biomed Anal 54:482-490
16. Olah E, Fekete S, Fekete J, Ganzler K (2010) Comparative study of new shell-type, sub-2 μ m fully porous and monolith stationary phases, focusing on mass-transfer resistance. J Chromatogr A 1217:3642-3653
17. Swartz ME, Murphy B, Sievers D (2004) UPLC: expanding the limits of HPLC. GIT Lab J 8:43-45
18. Swartz ME (2005) UPLC: an introduction and review. J Liquid Chromatogr 28:1253-1266
19. Alaerts G, Arevalo MM, Dumarey M, Dejaegher B, Noppe N, Matthijs N, Verbeke JS, Heyden YV (2010) Exploratory analysis of chromatographic fingerprints to distinguish rhizoma chuanx-iong and rhizoma ligustici. J Chromatogr A 1217:7706-7716
20. Diez C, Barrado E, Marinero P, Sanz M (2008) Orthogonal array optimization of a multiresidue method for cereal herbicides in soils. J Chromatogr A 1180:10-23