Characterization of AgI nanoparticles synthesized in a spinning disk reactor

Chemical Engineering Journal

Volumn 183, Issue , 2012, Pages 466-472

  Liu, Hwai Shen ^a   Wang, Yao Hsuan ^a   Li, Chih Chan ^a   Tai, Clifford Y ^a  

^a NATIONAL TAIWAN UNIVERSITY   (Taiwan)

Author keywords

AgI nanoparticle; Continuous mode; Particle characterization; Phase transition; Protecting agent; Spinning disk reactor

Indexed keywords

CONTINUOUS MODE; CRYSTAL MORPHOLOGIES; DISK ROTATION; KI SOLUTION; LIQUID-LIQUID REACTIONS; MEAN SIZE; OPERATING VARIABLES; PARTICLE CHARACTERIZATION; POLYVINYL PYRROLIDONE; PRODUCT YIELDS; PROTECTING AGENT; SILVER IODIDE; SILVER NITRATES; SPINNING DISK REACTOR; SPINNING DISKS; SURFACE BONDING; TRANSITION POINT; TWO-STREAM;

LIQUIDS; NANOPARTICLES; PHASE TRANSITIONS; POTASSIUM; POTASSIUM IODIDE; SILVER HALIDES;

SILVER;

EID: 84862785250     PISSN: 13858947     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.cej.2011.12.035     Document Type: Article

References (16)

1. Sax R.I., Goldsmith P. Nucleation of water grops by Brownian contact with AgI and other aerosolos. Q. J. R. Met. Soc. 1972, 98:60-72.
2. Makiura R., Yonemura T., Yamada T., Yamauchi M., Ikeda R., Kitagawa H., Kato K., Takata M. Size-controlled stabilization of the superionic phase to room temperature in polymer-coated AgI nanoparticles. Nat. Mater. 2009, 8:476-480.
3. Zhang Z., Zhao B., Hu L. PVP protective mechanism of ultrafine silver powder synthesized by chemical reduction processes. J. Solid State Chem. 1996, 121:105-110.
4. Owens B.B. Solid state electrolytes: overview of materials and applications during the last third of the Twenieth Century. J. Power Sources 2000, 90:2-8.
5. Chen J.F., Wang Y.H., Guo F., Wang X.M., Zheng C. Synthesis of nanoparticles with novel technology: high-gravity reactive precipitation. Ind. Eng. Chem. Res. 2000, 39:948-954.
6. Cafiero L.M., Baffi G., Chianese A., Jachuck R.J.J. Process intensification: precipitation of barium sulfate using a spinning disk reactor. Ind. Eng. Chem. Res. 2002, 5240-5246.
7. Ramshaw C. The spinning disc reactor. Re-Engineering Chemical Processing Plant: Process Intensification 2004, Marcel Dekker, USA. A. Stankiewicz, J.A. Moulijn (Eds.).
8. Tai C.Y., Tai C.T., Chang M.H., Liu H.S. Synthesis of magnesium hydroxide and oxide nanoparticles using a spinning disk reactor. Ind. Eng. Chem. Res. 2007, 46:5536-5541.
9. Tai C.Y., Wang Y.H., Liu H.S. A green process for preparing silver nanoparticles using spinning disk reactor. AIChE J. 2008, 54:445-452.
10. Tai C.Y., Wang Y.H., Kuo Y.W., Chang M.H., Liu H.S. Synthesis of silver particles below 10nm using spinning disk reactor. Chem. Eng. Sci. 2009, 64:3112-3119.
11. Tai C.Y., Wang Y.H., Tai C.T., Liu H.S. Preparation of silver nanoparticles using a spinning disk reactor in a continuous mode. Ind. Eng. Chem. Res. 2009, 48:10104-10109.
12. Shaviv R., Westrum E.F., Gronvold F., Stolen S., Inaba A., Fuji H., Chihara H. Heat capacity, thermodynamic properties, and transitions of silver iodide. J. Chem. Thermodyn. 1989, 21:631-651.
13. Wang Y., Mo J., Cai W., Yao L., Zhang L. Large-scale synthesis of α-AgI nanoparticles. Mater. Lett. 2002, 56:502-506.
14. Berry C.R. Structure and optical absorption of AgI microcrystals. Phys. Rev. 1967, 161:848-851.
15. Y. H. Wang, A green chemical process for preparing silver nanoparticles using the high-gravity technique. Master's thesis, National Taiwan University (2006).
16. Bai J., Li Y., Zhang C., Liang X., Yang Q. Preparing AgBr nanoparticles in poly(vinyl pyrrolidone) (PVP) nanofibers. Colloids Surf. A 2008, 329:165-168.