Use of solid phase microextraction (SPME) in the analysis of the reduced sulfur compounds (RSC) and its experimental limitations

Microchemical Journal

Volumn 103, Issue , 2012, Pages 42-48

  Kabir, Ehsanul ^a   Kim, Ki Hyun ^a  

^a Sejong University   (South Korea)

Author keywords

Carboxen PDMS fiber; Pulsed flame photometric detection; Reduced sulfur compounds; Solid phase microextraction

Indexed keywords

EID: 84862776755     PISSN: 0026265X     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.microc.2012.01.005     Document Type: Article

References (35)

1. Shearer R., O'Neal D., Rios R., Baker M. Analysis of sulfur compounds by capillary column gas chromatography with sulfur chemiluminescence detection. J. Chromatogr. Sci. 1990, 28:24-28.
2. Pandey S.K., Kim K.-H. A review of methods for the determination of reduced sulfur compounds (RSCs) in air. Environ. Sci. Technol. 2009, 29:3020-3029.
3. Wardencki W. Problems with the determination of environmental sulphur compounds by gas chromatography. J. Chromatogr. A 1998, 793:1-19.
4. Helmig D. Air analysis by gas chromatography. J. Chromatogr. A 1999, 843:129-146.
5. Willig S., Lacorn M., Claus R. Development of a rapid and accurate method for the determination of key compounds of pig odor. J. Chromatogr. A 2004, 1038:11-18.
6. Firor R.L., Quimby B.D. A comparison of sulfur selective detectors for low-level analysis in gaseous streams. Application Note provided by Agilent Technologies, Inc 2001, 5988-2426EN.
7. MacTaggart D.L., Farwell S.O., Burdge J.R., Cai Z.-T., Haakenson T.J., Bamesberger W.L. A continuous monitor-sulfur chemiluminescence detector (CM-SCD) system for the measurement of total gaseous sulfur species in air. Atmos. Environ. 1999, 33:625-632.
8. Swan H.B., Ivey J.P. Evaluation of two sulfur specific detectors for the measurement of dimethylsulfide gas concentrations at Macquarie Island and Cape Grim during ACE-1. Baseline Atmospheric Program (Australia) 1999, 15-23.
9. Kim K.-H. Performance characterization of the GC/PFPD for H2S, CH3SH, DMS, and DMDS in air. Atmos. Environ. 2005, 39:2235-2242.
10. Kim K.-H., Ju D.W., Joo S.W. The evaluation of recovery rate associated with the use of thermal desorption system for the analysis of atmospheric reduced sulfur compounds (RSC) using the GC/PFPD method. Talanta 2005, 67:955-959.
11. Kim K.-H., Choi Y.J., Jeon E.C., Sunwoo Y. Characterization of malodorous sulfur compounds in landfill gas. Atmos. Environ. 2005, 39:1103-1112.
12. Kim K.-H. The properties of calibration errors in the analysis of reduced sulfur compounds by the combination of a loop injection system and the GC/PFPD method. Anal. Chim. Acta 2006, 566:75-80.
13. Kim K.-H., Choi G.-H., Choi Y.-J., Song H.N., Yang H.-S., Oh J.-M. The effects of sampling materials selection in the collection of reduced sulfur compounds in air. Talanta 2006, 68:1713-1719.
14. Pandey S.K., Kim K.-H. The fundamental properties of the direct injection method in the analysis of gaseous reduced sulfur by gas chromatography with a pulsed flame photometric detector. Anal. Chim. Acta 2008, 615:165-173.
15. Ras M.R., Marcé R.M., Borrull F. Solid-phase microextraction-gas chromatography to determine volatile organic sulfur compounds in the air at sewage treatment plants. Talanta 2008, 77:774-778.
16. Vassilakos C., Papadopoulos A., Lahaniati M., Maggos T., Bartzis J., Papagianakopoulos P. Measurements of sulfur pollutants and VOC concentrations in the atmosphere of a suburban area in Greece. Fresenius Environ. Bull. 2002, 11:516-521.
17. Muezzinoglu A. A study of volatile organic sulfur emissions causing urban odors. Chemosphere 2003, 51:245-252.
18. Chen Y., Pawliszyn J. Time-weighted average passive sampling with a solid-phase microextraction device. Anal. Chem. 2003, 75:2004-2010.
19. Haberhauer-Troyer C., Rosenberg E., Grasserbauer M. Evaluation of solid-phase microextraction for sampling of volatile organic sulfur compounds in air for subsequent gas chromatographic analysis with atomic emission detection. J. Chromatogr. A 1999, 848:305-315.
20. Namiesnik J., Zygmunt B., Jastrzebska A. Application of solid-phase microextraction for determination of organic vapours in gaseous matrices. J. Chromatogr. A 2000, 885:405-418.
21. Pastore P., Favaro G., Badocco D., Lavagnini I. Headspace solid phase micro extraction GC-ECD determination of volatile organic chlorinated hydrocarbons in soils. Chemosphere 2005, 95:741-756.
22. Musteata F.M., Pawliszyn J. Bioanalytical applications of solid-phase microextraction. Trends Anal. Chem. 2007, 26:36-45.
23. Koziel J., Jia M., Khaled A., Noah J., Pawliszyn J. Field air analysis with SPME device. Anal. Chim. Acta 1999, 400:153-162.
24. Hill P.G., Smith R.M. Determination of sulphur compounds in beer using headspace solid-phase microextraction and gas chromatographic analysis with pulsed flame photometric detection. J. Chromatogr. A 2000, 872:203.
25. Tuduri L., Desauziers V., Fanlo J.L., Koziel J., Jia M., Khaled A., Noah J., Pawliszyn J. Determination of absolute amount extracted by solid-phase microextraction: different approaches under examination. J. Microcolumn Sep. 2000, 12:550-557.
26. Nielsen A.T., Jonsson S. Trace determination of volatile sulfur compounds by solid-phase microextraction and GC-MS. Analyst 2002, 127:1045-1049.
27. Lestremau F., Desauziers V., Roux J.C., Fanlo J.L. Development of a quantification method for the analysis of malodorous sulphur compounds in gaseous industrial effluents by solid-phase microextraction and gas chromatography-pulsed flame photometric detection. J. Chromatogr. A 2003, 999:71-80.
28. Payne R., Labows J., Liu X. Released oral malodor measured by solid phase microextraction/gas chromatography mass spectrometry (HS-SPME-GC-MS) proceeding of ACS - flavor release no. 0841236925. ACS Symposium Series 2000, 763:86-97.
29. Murray R.A. Limitations to the use of solid-phase microextraction for quantitation of mixtures of volatile organic sulfur compounds. Anal. Chem. 2001, 73:1646-1649.
30. Fang Y., Qian M.C. Sensitive quantification of sulfur compounds in wine by headspace solid-phase microextraction technique. J. Chromatogr. A 2005, 1080:177.
31. López P., Brandsma S.A., Leonards P.E.G., De-Boe J. Methods for the determination of phenolic brominated flame retardants, and by-products, formulation intermediates and decomposition products of brominated flame retardants in water. J. Chromatogr. A 2009, 1216:334-345.
32. Górecki T., Yu X., Pawliszyn J. Theory of analyte extraction by selected porous polymer SPME fibres. Analyst 1999, 124:643-649.
33. Frank D., Owen C.M., Patterson J. Solid phase microextraction (SPME) combined with gas-chromatography and olfactometry-mass spectrometry for characterization of cheese aroma compounds. Lebensm. Wiss. Technol. 2004, 37:139-154.
34. Oestreich-Janzen S. Chemistry of coffee. Chem. Biol. 2010, 3:1085-1117.
35. Kabir E., Kim K.-H. An investigation on hazardous and odorous pollutants emission during cooking activities. J. Hazard. Mater. 2011, 188:443-454.