메뉴 건너뛰기




Volumn 26, Issue 10, 2012, Pages 1232-1240

Isotope effects associated with the preparation and methylation of fatty acids by boron trifluoride in methanol for compound-specific stable hydrogen isotope analysis via gas chromatography/thermal conversion/isotope ratio mass spectrometry

Author keywords

[No Author keywords available]

Indexed keywords

ALKYLATION; EXTRACTION; HYDROGEN; ISOTOPES; MASS SPECTROMETRY; METHANOL; PALMITIC ACID; PHASE SEPARATION; SALTS; SATURATED FATTY ACIDS;

EID: 84859875970     PISSN: 09514198     EISSN: 10970231     Source Type: Journal    
DOI: 10.1002/rcm.6188     Document Type: Article
Times cited : (9)

References (29)
  • 1
    • 0032755860 scopus 로고    scopus 로고
    • Compound-specific D/H ratios of lipid biomarkers from sediments as a proxy for environmental and climatic conditions
    • A. L. Sessions, T. W. Burgoyne, A. Schimmelmann, J. M. Hayes,. Compound-specific D/H ratios of lipid biomarkers from sediments as a proxy for environmental and climatic conditions. Org. Geochem. 1999, 30, 1193.
    • (1999) Org. Geochem. , vol.30 , pp. 1193
    • Sessions, A.L.1    Burgoyne, T.W.2    Schimmelmann, A.3    Hayes, J.M.4
  • 2
    • 0037110722 scopus 로고    scopus 로고
    • Hydrogen isotope fractionation in lipids of the methane-oxidizing bacterium Methylococcus capsulatus
    • A. L. Sessions, L. L. Jahnke, A. Schimmelmann, J. M. Hayes,. Hydrogen isotope fractionation in lipids of the methane-oxidizing bacterium Methylococcus capsulatus. Geochim. Cosmochim. Acta 2002, 66, 3955.
    • (2002) Geochim. Cosmochim. Acta , vol.66 , pp. 3955
    • Sessions, A.L.1    Jahnke, L.L.2    Schimmelmann, A.3    Hayes, J.M.4
  • 3
    • 0036966458 scopus 로고    scopus 로고
    • Hydrogen isotope ratios of palmitic acid in lacustrine sediments record late Quaternary climate variations
    • Y. Huang, B. Shuman, Y. Wang, T. Webb,. Hydrogen isotope ratios of palmitic acid in lacustrine sediments record late Quaternary climate variations. Geology 2002, 30, 1103.
    • (2002) Geology , vol.30 , pp. 1103
    • Huang, Y.1    Shuman, B.2    Wang, Y.3    Webb, T.4
  • 4
    • 0742324900 scopus 로고    scopus 로고
    • Carbon and hydrogen isotopic fractionation during lipid biosynthesis in a higher plant (Cryptomeria japonica)
    • Y. Chikaraishi, H. Naraoka, S. R. Poulson,. Carbon and hydrogen isotopic fractionation during lipid biosynthesis in a higher plant (Cryptomeria japonica). Phytochemistry 2004, 65, 323.
    • (2004) Phytochemistry , vol.65 , pp. 323
    • Chikaraishi, Y.1    Naraoka, H.2    Poulson, S.R.3
  • 8
    • 0001114648 scopus 로고
    • The determination of the D/H ratio of non-exchangeable hydrogen in cellulose extracted from aquatic and land plants
    • S. Epstein, C. J. Yapp, J. H. Hall,. The determination of the D/H ratio of non-exchangeable hydrogen in cellulose extracted from aquatic and land plants. Earth Planet. Sci. Lett. 1976, 30, 241.
    • (1976) Earth Planet. Sci. Lett. , vol.30 , pp. 241
    • Epstein, S.1    Yapp, C.J.2    Hall, J.H.3
  • 9
    • 12044254754 scopus 로고
    • Determination of the concentration and stable isotopic composition of nonexchangeable hydrogen in organic matter
    • A. Schimmelmann,. Determination of the concentration and stable isotopic composition of nonexchangeable hydrogen in organic matter. Anal. Chem. 1991, 63, 2456.
    • (1991) Anal. Chem. , vol.63 , pp. 2456
    • Schimmelmann, A.1
  • 10
    • 0000786090 scopus 로고
    • Derivatization of organic-compounds prior to gas-chromatographic combustion-isotope ratio mass-spectrometric analysis - Identification of isotope fractionation processes
    • G. Rieley,. Derivatization of organic-compounds prior to gas-chromatographic combustion-isotope ratio mass-spectrometric analysis-identification of isotope fractionation processes. Analyst 1994, 119, 915.
    • (1994) Analyst , vol.119 , pp. 915
    • Rieley, G.1
  • 11
    • 4244130654 scopus 로고
    • The rapid preparation of fatty acid esters for gas chromatographic analysis
    • L. D. Metcalfe, A. A. Schmitz,. The rapid preparation of fatty acid esters for gas chromatographic analysis. Anal. Chem. 1961, 33, 363.
    • (1961) Anal. Chem. , vol.33 , pp. 363
    • Metcalfe, L.D.1    Schmitz, A.A.2
  • 12
    • 0017256755 scopus 로고
    • Estimation of plasma free fatty acids as the trimethylsilyl (TMS) esters
    • A. Kuksis, J. J. Myher, L. Marai, K. Geher,. Estimation of plasma free fatty acids as the trimethylsilyl (TMS) esters. Anal. Biochem. 1976, 70, 302.
    • (1976) Anal. Biochem. , vol.70 , pp. 302
    • Kuksis, A.1    Myher, J.J.2    Marai, L.3    Geher, K.4
  • 13
    • 4243190715 scopus 로고
    • Preparation of fatty acid methyl esters and dimethylacetals from lipids with boron fluoride-methanol
    • W. R. Morrison, L. M. Smith,. Preparation of fatty acid methyl esters and dimethylacetals from lipids with boron fluoride-methanol. J. Lipid Res. 1964, 5, 600.
    • (1964) J. Lipid Res. , vol.5 , pp. 600
    • Morrison, W.R.1    Smith, L.M.2
  • 15
    • 0033030936 scopus 로고    scopus 로고
    • Measurement of deuterium incorporation into fatty acids by gas chromatography/isotope ratio mass spectrometry
    • C. M. Scrimgeour, I. S. Begley, M. L. Thomason,. Measurement of deuterium incorporation into fatty acids by gas chromatography/isotope ratio mass spectrometry. Rapid Commun. Mass Spectrom. 1999, 13, 271.
    • (1999) Rapid Commun. Mass Spectrom. , vol.13 , pp. 271
    • Scrimgeour, C.M.1    Begley, I.S.2    Thomason, M.L.3
  • 16
    • 0037236681 scopus 로고    scopus 로고
    • Preservation of lipid hydrogen isotope ratios in Miocene lacustrine sediments and plant fossils at Clarkia, northern Idaho, USA
    • H. Yang, Y. Huang,. Preservation of lipid hydrogen isotope ratios in Miocene lacustrine sediments and plant fossils at Clarkia, northern Idaho, USA. Org. Geochem. 2003, 34, 413.
    • (2003) Org. Geochem. , vol.34 , pp. 413
    • Yang, H.1    Huang, Y.2
  • 17
    • 34249045987 scopus 로고    scopus 로고
    • Hydrogen isotopic variability in leaf waxes among terrestrial and aquatic plants around Blood Pond, Massachusetts (USA)
    • J. Hou, W. J. D'Andrea, D. MacDonald, Y. Huang,. Hydrogen isotopic variability in leaf waxes among terrestrial and aquatic plants around Blood Pond, Massachusetts (USA). Org. Geochem. 2007, 38, 977.
    • (2007) Org. Geochem. , vol.38 , pp. 977
    • Hou, J.1    D'Andrea, W.J.2    MacDonald, D.3    Huang, Y.4
  • 18
    • 33846541257 scopus 로고    scopus 로고
    • 13C and δd relationships among three n-alkyl compound classes (n-alkanoic acid, n-alkane and n-alkanol) of terrestrial higher plants
    • 13C and δD relationships among three n-alkyl compound classes (n-alkanoic acid, n-alkane and n-alkanol) of terrestrial higher plants. Org. Geochem. 2007, 38, 198.
    • (2007) Org. Geochem. , vol.38 , pp. 198
    • Chikaraishi, Y.1    Naraoka, H.2
  • 19
    • 0022232953 scopus 로고
    • Acid catalysis of alkyl hydrogen exchange and configurational isomerisation reactions: Acyclic isoprenoid acids
    • A. V. Larcher, R. Alexander, S. J. Rowland, R. I. Kagi,. Acid catalysis of alkyl hydrogen exchange and configurational isomerisation reactions: acyclic isoprenoid acids. Org. Geochem. 1986, 10, 1015.
    • (1986) Org. Geochem. , vol.10 , pp. 1015
    • Larcher, A.V.1    Alexander, R.2    Rowland, S.J.3    Kagi, R.I.4
  • 20
    • 0041730391 scopus 로고    scopus 로고
    • Quantifying hydrogen-deuterium exchange of meteoritic dicarboxylic acids during aqueous extraction
    • M. Fuller, Y. Huang,. Quantifying hydrogen-deuterium exchange of meteoritic dicarboxylic acids during aqueous extraction. Meteoritics Planet. Sci. 2003, 38, 357.
    • (2003) Meteoritics Planet. Sci. , vol.38 , pp. 357
    • Fuller, M.1    Huang, Y.2
  • 21
    • 0001746545 scopus 로고
    • Isotope fractionation during gas chromatographic separations
    • B. D. Gunter, J. D. Gleason,. Isotope fractionation during gas chromatographic separations. J. Chromatogr. Sci. 1971, 9, 191.
    • (1971) J. Chromatogr. Sci. , vol.9 , pp. 191
    • Gunter, B.D.1    Gleason, J.D.2
  • 24
    • 0003733313 scopus 로고    scopus 로고
    • in, (Ed: M. V. Twigg). Manson Publishing, London, p
    • G. W. Bridger, M. S. Spencer, in The Catalyst Handbook, (Ed:, M. V. Twigg,). Manson Publishing, London, 1996, p. 441.
    • (1996) The Catalyst Handbook , pp. 441
    • Bridger, G.W.1    Spencer, M.S.2
  • 25
    • 0141527587 scopus 로고    scopus 로고
    • The O and H stable isotope composition of freshwaters in the British Isles. 1. Rainfall
    • W. G. Darling, J. C. Talbot,. The O and H stable isotope composition of freshwaters in the British Isles. 1. Rainfall. Hydrol. Earth Syst. Sci. 2003, 7, 163.
    • (2003) Hydrol. Earth Syst. Sci. , vol.7 , pp. 163
    • Darling, W.G.1    Talbot, J.C.2
  • 26
    • 0141638731 scopus 로고    scopus 로고
    • The O and H stable isotope composition of freshwaters in the British Isles. 2. Surface waters and groundwater
    • W. G. Darling, A. H. Bath, J. C. Talbot,. The O and H stable isotope composition of freshwaters in the British Isles. 2. Surface waters and groundwater. Hydrol. Earth Syst. Sci. 2003, 7, 183.
    • (2003) Hydrol. Earth Syst. Sci. , vol.7 , pp. 183
    • Darling, W.G.1    Bath, A.H.2    Talbot, J.C.3
  • 27
    • 67449104516 scopus 로고    scopus 로고
    • Investigation of fatty acid elongation and desaturation steps in Fusarium lateritium by quantitative two-dimensional deuterium NMR spectroscopy in chiral oriented media
    • V. Baillif, R. J. Robins, S. Le Feunteun, P. Lescot, I. Billault,. Investigation of fatty acid elongation and desaturation steps in Fusarium lateritium by quantitative two-dimensional deuterium NMR spectroscopy in chiral oriented media. J. Biol. Chem. 2009, 284, 10783.
    • (2009) J. Biol. Chem. , vol.284 , pp. 10783
    • Baillif, V.1    Robins, R.J.2    Le Feunteun, S.3    Lescot, P.4    Billault, I.5
  • 28
    • 0033895551 scopus 로고    scopus 로고
    • Cooperativity among molecules at interfaces in relation to various technological processes: Effect of chain length on the pKa of fatty acid salt solutions
    • J. R. Kanicky, A. F. Poniatowski, N. R. Mehta, D. O. Shah,. Cooperativity among molecules at interfaces in relation to various technological processes: effect of chain length on the pKa of fatty acid salt solutions. Langmuir 2000, 16, 172.
    • (2000) Langmuir , vol.16 , pp. 172
    • Kanicky, J.R.1    Poniatowski, A.F.2    Mehta, N.R.3    Shah, D.O.4
  • 29
    • 0003467672 scopus 로고
    • (4th edn.), Wiley Interscience, New York
    • J. March,. Advanced Organic Chemistry, (4th edn.), Wiley Interscience, New York. 1992.
    • (1992) Advanced Organic Chemistry
    • March, J.1


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.