Single-pass flow-through reaction cell for high-temperature and high-pressure in situ neutron diffraction studies of hydrothermal crystallization processes

Journal of Applied Crystallography

Volumn 45, Issue 2, 2012, Pages 166-173

  Xia, Fang ^a,b   Brugger, Joël ^a,b   Qian, Gujie ^b,c   Ngothai, Yung ^a   Oneill, Brian ^a   Zhao, Jing ^a,b   Pullen, Stewart ^d   Olsen, Scott ^d   Pring, Allan ^a,b  

^a UNIVERSITY OF ADELAIDE   (Australia)

^b SOUTH AUSTRALIAN MUSEUM   (Australia)

^c UNIVERSITY OF SOUTH AUSTRALIA   (Australia)

^d AUSTRALIAN NUCLEAR SCIENCE AND TECHNOLOGY ORGANISATION   (Australia)

Author keywords

celestine (SrS 4); hydrothermal cells; in situ neutron diffraction; mineral replacement reactions; strontianite (SrCO 3); vacuum furnaces

Indexed keywords

AUSTRALIAN NUCLEAR SCIENCE AND TECHNOLOGIES; BACK PRESSURES; BEAM LINES; CELESTINE (SRS 4); CONSTANT TEMPERATURE; CONVERSION RATES; EFFECT OF PRESSURE; FLOW-THROUGH CELLS; FLOWTHROUGH; HIGH TEMPERATURE; HYDROTHERMAL CONDITIONS; HYDROTHERMAL CRYSTALLIZATION; IN-SITU; IN-SITU NEUTRON DIFFRACTION; INNOVATIVE DESIGN; NONLINEAR EFFECT; POWDER DIFFRACTOMETERS; REACTION CELLS; REACTION MODULE; REAL TIME; REPLACEMENT REACTIONS; ROOM TEMPERATURE; STRONTIANITE (SRCO 3); SUPER-CRITICAL;

CELLS; CYTOLOGY; DESIGN; DIFFRACTOMETERS; FLOW RATE; NEUTRON DIFFRACTION; SUBSTITUTION REACTIONS; VACUUM FURNACES;

PRESSURE EFFECTS;

PASSIFLORA;

EID: 84859752159     PISSN: 00218898     EISSN: 16005767     Source Type: Journal    
DOI: 10.1107/S0021889812002300     Document Type: Article

References (48)

1. Antao, S. M. & Hassan, I. (2009). Can. Mineral. 47, 1245-1255.
2. Baker, P. A., Kastner, M., Byerlee, J. D. & Lockner, D. A. (1980). Mar. Geol. 38, 185-203.
3. Brugger, J., Mcfadden, A., Lenehan, C. E., Etschmann, B., Xia, F., Zhao, J. & Pring, A. (2010). Chimia, 64, 693-698.
4. Brugger, J., Pring, A., Reith, F., Ryan, C., Etschmann, B., Liu, W., O'Neill, B. & Ngothai, Y. (2010). Radiat. Phys. Chem. 79, 151-161.
5. Carrillo, F. R., Uribe, P. & Castillejos, A. H. (1995). Miner. Eng. 8, 495-509.
6. Castillejos, A. H., delaCruz, F. P. & Uribe, A. (1996). Hydrometallurgy, 40, 207-222.
7. Christian, J. W. (1965). The Theory of Transformations in Metals and Alloys. Oxford: Pergamon Press.
8. Davis, M. E. & Lobo, R. F. (1992). Chem. Mater. 4, 756-768.
9. Evans, J. S. O., Francis, R. J., O'Hare, D., Price, S. J., Clark, S. M., Flaherty, J., Gordon, J., Nield, A. & Tang, C. C. (1995). Rev. Sci. Instrum. 66, 2442-2445.
10. Francis, R. J., O'Brien, S., Fogg, A. M., Halasyamani, P. S., O'Hare, D., Loiseau, T. & Ferey, G. (1999). J. Am. Chem. Soc. 121, 1002-1015.
11. Francis, R. J. & O'Hare, D. (1998). J. Chem. Soc. Dalton Trans. 19, 3133-3148.
12. Gray, E. M. & Bailey, I. F. (2008). J. Neutron Res. 16, 127-132.
13. Hanor, J. S. (2004). J. Sediment. Res. 74, 168-175.
14. Jacobsen, S. D., Smyth, J. R., Swope, R. J. & Downs, R. T. (1998). Can. Mineral. 36, 1053-1060.
15. Janssen, A., Putnis, A., Geisler, T. & Putnis, C. V. (2010). Mineral. Mag. 74, 633-644.
16. Larson, A. C. & Von Dreele, R. B. (2004). Report LAUR 86-748. Los Alamos National Laboratory, New Mexico, USA.
17. Lasaga, A. C. (1998). Kinetic Theory in the Earth Sciences. Princeton University Press.
18. Mesu, J. G., van der Eerden, A. M., de Groot, F. M. & Weckhuysen, B. M. (2005). J. Phys. Chem. B, 109, 4042-4047.
19. Nagy, K. L. & Lasaga, A. C. (1992). Geochim. Cosmochim. Acta, 56, 3093-3111.
20. Ok, K. M., O'Hare, D., Smith, R. I., Chowdhury, M. & Fikremariam, H. (2010). Rev. Sci. Instrum. 81, 125107.
21. O'Neill, B., Tenailleau, C., Ngothai, Y., Studer, A., Brugger, J. & Pring, A. (2006). Physica B, 385-386, 942-945.
22. Provis, J. L., van Deventer, J. S. J., Rademan, J. A. M. & Lorenzen, L. (2003). Hydrometallurgy, 70, 83-99.
23. Putnis, A. (2002). Mineral. Mag. 66, 689-708.
24. Putnis, A. (2009). Rev. Mineral. Geochem. 70, 87-124.
25. Qian, G., Brugger, J., Skinner, W. M., Chen, G. R. & Pring, A. (2010). Geochim. Cosmochim. Acta, 74, 5610-5630.
26. Qian, G., Xia, F., Brugger, J., Skinner,W. M., Bei, J., Chen, G. & Pring, A. (2011). Am. Mineral. 96, 1878-1893.
27. Rietveld, H. M. (1969). J. Appl. Cryst. 2, 65-71.
28. Rubisov, D. H., Krowinkel, J. M. & Papangelakis, V. G. (2000). Hydrometallurgy, 58, 1-11.
29. Ruiz, M. C., Vera, M. V. & Padilla, R. (2011). Hydrometallurgy, 105, 290-295.
30. Rutter, E. H. (1983). J. Geol. Soc. (London), 140, 725-740.
31. Sidhu, S. S., Heaton, L. R., Zauberis, D. D. & Campos, F. P. (1956). J. Appl. Phys. 27, 1040-1042.
32. Studer, A. J., Hagen, M. E. & Noakes, T. J. (2006). Physica B, 385-386, 1013-1015.
33. Suarez-Orduna, R., Rendon-Angeles, J. C., Lopez-Cuevas, J. & Yanagisawa, K. (2004). J. Phys. Condens. Matter, 16, S1331-S1344.
34. Tada, R. & Siever, R. (1986). Geochim. Cosmochim. Acta, 50, 29-36.
35. Tenailleau, C., Pring, A., Etschmann, B., Brugger, J., Grguric, B. A. & Putnis, A. (2006). Am. Mineral. 91, 706-709.
36. Toby, B. H. (2001). J. Appl. Cryst. 34, 210-213.
37. Walton, R. I., Francis, R. J., Halasyamani, P. S., O'Hare, D., Smith, R. I., Done, R. & Humphreys, R. J. (1999). Rev. Sci. Instrum. 70, 3391-3396.
38. Walton, R. I. & O'Hare, D. (2000). Chem. Commun. pp. 2283-2291.
39. Walton, R. I., Smith, R. I., Millange, F., Clark, I. J., Sinclair, D. C. & O'Hare, D. (2000). Chem. Commun. pp. 1267-1268.
40. Williams, G. R., Norquist, A. J. & O'Hare, D. (2006). Chem. Mater. 18, 3801-3807.
41. Xia, F., Brugger, J., Chen, G. R., Ngothai, Y., O'Neill, B., Putnis, A. & Pring, A. (2009). Geochim. Cosmochim. Acta, 73, 1945-1969.
42. Xia, F., Brugger, J., Ngothai, Y., O'Neill, B., Chen, G. & Pring, A. (2009). Cryst. Growth Des. 9, 4902-4906.
43. Xia, F., O'Neill, B., Ngothai, Y., Peak, J., Tenailleau, C., Etschmann, B., Qian, G., Brugger, J., Studer, A., Olsen, S. & Pring, A. (2010). J. Appl. Cryst. 43, 511-519.
44. Xia, F., Qian, G., Brugger, J., Studer, A., Olsen, S. & Pring, A. (2010). Rev. Sci. Instrum. 81, 105107.
45. Xia, F., Zhou, J.W., Brugger, J., Ngothai, Y., O'Neill, B., Chen, G. R. & Pring, A. (2008). Chem. Mater. 20, 2809-2817.
46. Xia, F., Zhou, J., Pring, A., Ngothai, Y., O'Neill, B., Brugger, J., Chen, G. & Colby, C. (2007). React. Kinet. Catal. Lett. 92, 257-266.
47. Zhao, J., Brugger, J., Grundler, P. V., Xia, F., Chen, G. & Pring, A. (2009). Am. Mineral. 94, 1541-1555.
48. Zhao, J., Xia, F., Pring, A., Brugger, J., Grundler, P. V. & Chen, G. (2010). Miner. Eng. 23, 451-453.