Chiral capillary liquid chromatography based on penicillin G acylase immobilized on monolithic epoxy silica column

Journal of Chromatography A

Volumn 1234, Issue , 2012, Pages 45-49

  Gotti, Roberto ^a   Fiori, Jessica ^a   Calleri, Enrica ^b   Temporini, Caterina ^b   Lubda, Dieter ^c   Massolini, Gabriella ^b  

^a UNIVERSITY OF BOLOGNA   (Italy)

^b UNIVERSITY OF PAVIA   (Italy)

^c MERCK KGAA   (Germany)

Author keywords

Capillary liquid chromatography; Chiral separation; Immobilization; Penicillin G acylase; Silica monolith

Indexed keywords

ARYLPROPIONIC ACIDS; BACK PRESSURES; CAPILLARY COLUMNS; CAPILLARY LIQUID CHROMATOGRAPHY; CHIRAL RECOGNITION; CHIRAL SEPARATION; ENANTIORESOLUTION; ENANTIOSEPARATIONS; EPOXY-SILICA; FUSED-SILICA CAPILLARIES; KETOPROFEN; MOBILE PHASE; MONOLITHIC CAPILLARY COLUMN; MONOLITHIC SILICA; PENICILLIN G ACYLASE; PHOSPHATE BUFFERS; PLATE HEIGHT; RETENTION TIME; SILICA MONOLITH; STATIONARY PHASE; UV DETECTION; VALIDATION DATA;

ANTIBIOTICS; CHIRALITY; ENZYME IMMOBILIZATION; LIQUID CHROMATOGRAPHY; RADIOACTIVE WASTE VITRIFICATION;

FUSED SILICA;

ARYLPROPIONIC ACID DERIVATIVE; EPOXIDE; FLURBIPROFEN; KETOPROFEN; PENICILLIN AMIDASE; POLITEF; SILICON DIOXIDE; SUPROFEN;

ARTICLE; CAPILLARY LIQUID CHROMATOGRAPHY; CHIRALITY; DRUG DETERMINATION; ELECTRICALLY ASSISTED CAPILLARY LIQUID CHROMATOGRAPHY; ENZYME IMMOBILIZATION; LIQUID CHROMATOGRAPHY; PRIORITY JOURNAL; SEPARATION TECHNIQUE; TABLET; ULTRAVIOLET RADIATION; VALIDITY;

CHROMATOGRAPHY, LIQUID; ENZYMES, IMMOBILIZED; KETOPROFEN; LINEAR MODELS; PENICILLIN AMIDASE; REPRODUCIBILITY OF RESULTS; SENSITIVITY AND SPECIFICITY; SILICON DIOXIDE; STEREOISOMERISM;

EID: 84858793659     PISSN: 00219673     EISSN: 18733778     Source Type: Journal    
DOI: 10.1016/j.chroma.2011.11.048     Document Type: Article

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