The effect of biradical concentration on the performance of DNP-MAS-NMR

Journal of Magnetic Resonance

Volumn 216, Issue , 2012, Pages 209-212

  Lange, Sascha ^a   Linden, Arne H ^a   Akbey, Ümit ^a   Trent Franks, W ^a   Loening, Nikolaus M ^b   Rossum, Barth Jan Van ^a   Oschkinat, Hartmut ^a  

^a LEIBNIZ INSTITUT FÜR MOLEKULARE PHARMAKOLOGIE   (Germany)

^b LEWIS AND CLARK COLLEGE   (United States)

Author keywords

Biradical; Dynamic nuclear polarization; Solid state NMR; TOTAPOL

Indexed keywords

BIRADICAL; BIRADICAL CENTERS; CLOSE PROXIMITY; CROSS POLARIZATIONS; DYNAMIC NUCLEAR POLARIZATION; ELECTRON SPIN POLARIZATION; LINE BROADENING; MAS NMR; NMR RELAXATION; NMR SIGNALS; NUCLEAR SPINS; ORDERS OF MAGNITUDE; ORGANIC BIRADICALS; PARAMAGNETIC EFFECT; PARAMAGNETIC RELAXATION ENHANCEMENTS; PARAMAGNETIC SHIFTS; PER UNIT; RADICAL CONCENTRATION; REPETITION RATE; SIGNAL INTENSITIES; SIGNAL TO NOISE; SIGNALS OF INTERESTS; SOLID STATE NMR; TOTAPOL; UNPAIRED ELECTRONS;

AMINO ACIDS; EXPERIMENTS; MAGNETIC MOMENTS; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; PARAMAGNETISM; SPIN DYNAMICS;

SPIN POLARIZATION;

CARBON; CHOLINERGIC RECEPTOR; NEUROTOXIN; NITROGEN; PROLINE; PROTON;

ALGORITHM; ARTICLE; CHEMISTRY; ELECTRON SPIN RESONANCE; ISOTOPE LABELING; METABOLISM; METHODOLOGY; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY;

ALGORITHMS; CARBON ISOTOPES; ELECTRON SPIN RESONANCE SPECTROSCOPY; ISOTOPE LABELING; MAGNETIC RESONANCE SPECTROSCOPY; NEUROTOXINS; NITROGEN ISOTOPES; PROLINE; PROTONS; RECEPTORS, CHOLINERGIC;

EID: 84858332807     PISSN: 10907807     EISSN: 10960856     Source Type: Journal    
DOI: 10.1016/j.jmr.2012.01.002     Document Type: Article

References (33)

1. F. Creuzet, A. McDermott, R. Gebhard, K. van der Hoef, M.B. Spijker-Assink, J. Herzfeld, J. Lugtenburg, M.H. Levitt, and R.G. Griffin Science 251 1991 783 786
2. F.M. Marassi, A. Ramamoorthy, and S.J. Opella Proc. Natl. Acad. Sci. U. S. A. 94 1997 8551 8556
3. M. Hiller, L. Krabben, K.R. Vinothkumar, F. Castellani, B.-J. van Rossum, W. Kühlbrandt, and H. Oschkinat ChemBioChem 6 2005 1679 1684
4. A.T. Petkova, Y. Ishii, J.J. Balbach, O.N. Antzutkin, R.D. Leapman, F. Delaglio, and R. Tycko Proc. Natl. Acad. Sci. U. S. A. 99 2002 16742 16747
5. C. Wasmer, A. Lange, H. van Melckebeke, A.B. Siemer, R. Riek, and B.H. Meier Science 319 2008 1523 1526
6. H. Heise, W. Hoyer, S. Becker, O.C. Andronesi, D. Riedel, and M. Baldus Proc. Natl. Acad. Sci. U. S. A. 102 2005 15871 15876
7. A. Pines, M.G. Gibby, and J.S. Waugh Chem. Phys. Lett. 15 1972 373 376
8. M. Maricq, and J. Waugh J. Chem. Phys. 70 1979 3300 3316
9. A.W. Overhauser Phys. Rev. 92 1953 411 415
10. D.A. Hall, D.C. Maus, G.J. Gerfen, S.J. Inati, L.R. Becerra, F.W. Dahlquist, and R.G. Griffin Science 276 1997 930
11. P.C.A. van der Wel, K.-N. Hu, J. Lewandowski, and R.G. Griffin J. Am. Chem. Soc. 128 2006 10840 10846
12. V.S. Bajaj, M.L. Mak Jurkauskas, M.L. Belenky, J. Herzfeld, and R.G. Griffin Proc. Natl. Acad. Sci. U. S. A. 106 2009 9244 9249
13. M. Rosay, V. Weis, K. Kreischer, and R. Temkin J. Am. Chem. Soc. 124 2002 3214 3215
14. U. Akbey, W.T. Franks, A. Linden, S. Lange, R.G. Griffin, B.-J. van Rossum, and H. Oschkinat Angew. Chem., Int. Ed. 49 2010 7803 7806
15. K.-N. Hu, H.-H. Yu, T.M. Swager, and R.G. Griffin J. Am. Chem. Soc. 126 2004 10844 10845
16. Y. Matsuki, T. Maly, O. Ouari, H. Karoui, F. Le Moigne, E. Rizzato, S. Lyubenova, J. Herzfeld, T. Prisner, P. Tordo, and RG. Griffin Angew. Chem., Int. Ed. 48 2009 4996 5000
17. C. Song, K.-N. Hu, C.-G. Joo, T.M. Swager, and R.G. Griffin J. Am. Chem. Soc. 128 2006 11385 11390
18. M. Rosay, L. Tometich, S. Pawsey, R. Bader, R. Schauwecker, M. Blank, P.M. Borchard, S.R. Cauffman, K.L. Felch, R.T. Weber, R.J. Temkin, R.G. Griffin, and W.E. Maas Phys. Chem. Chem. Phys. 12 2010 5850 5860
19. K.R. Thurber, and R. Tycko J. Magn. Reson. 196 2009 84 87
20. R.R. Ernst, G. Bodenhausen, A. Wokaun, Principles of Nuclear Magnetic Resonance in One and Two Dimensions, Oxford University Press, 1990.
21. A.H. Linden, W.T. Franks, U. Akbey, S. Lange, B.-J. van Rossum, and H. Oschkinat J. Biomol. NMR 51 2011 283 292
22. A.B. Barnes, B. Corzilius, M.L. Mak Jurkauskas, L.B. Andreas, V.S. Bajaj, Y. Matsuki, M.L. Belenky, J. Lugtenburg, J.R. Sirigiri, R.J. Temkin, J. Herzfeld, and R.G. Griffin Phys. Chem. Chem. Phys. 12 2010 5861 5867
23. A.H. Linden, S. Lange, W.T. Franks, U. Akbey, E. Specker, B.-J. van Rossum, and H. Oschkinat J. Am. Chem. Soc. 133 2011 19266 19269
24. S. Hartmann, and E. Hahn Phys. Rev. 128 1962 2042 2053
25. G.M. Clore, and J. Iwahara Chem. Rev. 109 2009 4108 4139
26. N. Bloembergen Physica 15 1949 386 426
27. A. Brough, C. Grey, and C. Dobson J. Am. Chem. Soc. 115 1993 7318 7327
28. T. Melnyk, and J. Rowlinson J. Comput. Phys. 7 1971 385 393
29. A.J. Rossini, A. Zagdoun, M. Lelli, D. Gajan, F. Rascón, M. Rosay, W.E. Maas, C. Copéret, A. Lesage, and L. Emsley Chem. Sci. 3 2011 108
30. K.R. Thurber, W.-M. Yau, and R. Tycko J. Magn. Reson. 204 2010 303 313
31. T. Maly, A.-F. Miller, and R.G. Griffin ChemPhysChem 11 2010 999 1001
32. V. Vitzthum, M.A. Caporini, and G. Bodenhausen J. Magn. Reson. 205 2010 177 179
33. A. Lesage, M. Lelli, D. Gajan, M.A. Caporini, V. Vitzthum, P. Miéville, J. Alauzun, A. Roussey, C. Thieuleux, A. Mehdi, G. Bodenhausen, C. Copéret, and L. Emsley J. Am. Chem. Soc. 132 2010 15459 15461