FTIR spectroscopy study of polyamide-6 irradiated by electron and proton beams

Polymer Degradation and Stability

Volumn 97, Issue 4, 2012, Pages 523-531

  Porubská, Mária ^a   Szöllös, Ondrej ^b   Kóňová, Alena ^c   Janigová, Ivica ^d   Jašková, Miloslava ^c   Jomová, Klaudia ^a   Chodák, Ivan ^d  

^a Faculty of Natural Sciences ^*  (Slovakia)

^b Biont as   (Slovakia)

^c VUSAPL As   (Slovakia)

^d POLYMER INSTITUTE   (Slovakia)

Author keywords

Crystallinity; Electron beam; FTIR spectroscopy; Gel; Irradiated PA 6; Proton beam

Indexed keywords

AMINE GROUPS; AMORPHOUS PHASE; CROSSLINKED; CRYSTALLINE PHASE; CRYSTALLINITIES; FT-IR SPECTRUM; FTIR ANALYSIS; FTIR SPECTROSCOPY; GEL FRACTION; IRRADIATED PA-6; NEW COMPONENTS; PLANAR CONFORMATIONS; POLYAMIDE 6; STRUCTURAL CHANGE; UNSATURATED STRUCTURES; YOUNG MODULUS;

CRYSTALLINE MATERIALS; ELECTRON BEAMS; ETHYLENE; GELS; IRRADIATION; MACROMOLECULES; PROTON BEAMS;

FOURIER TRANSFORM INFRARED SPECTROSCOPY;

EID: 84857633508     PISSN: 01413910     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.polymdegradstab.2012.01.017     Document Type: Article

References (27)

1. Arkema Technical Information Peroxide selection based on HALF-LIFE 2006 http://www.arkema.com/sites/group/en/home.page
2. M. Lazár, R. Rado, and J. Rychlý Crosslinking of polyolefins Adv Polym Sci 95 1990 149 197
3. I. Chodák Properties of crosslinked polyolefin-based materials Prog Polym Sci 20 1995 1165 1199
4. M.C. Evora, L.D. Machado, V.L. Loureno, O.L. Gonalez, H. Wiebeck, and L.G. de Andrade e Silva Thermal analysis of ionizing radiation effects on recycled polyamide-6 J Therm Anal Calorim 67 2 2002 327 333 (Pubitemid 34199842)
5. S. Dadbin, M. Frounchi, and D. Goudarzi Electron beam induced crosslinking of nylon 6 with and without the presence of TAC Polym Degrad Stab 89 2005 436 441 (Pubitemid 40785698)
6. L. Pan, T. Inoue, H. Hayami, and S. Nishikawa Reactive blending of polyamide with polyethylene: pull-out of in situ-formed graft copolymers and its application for high-temperature materials Polymer 43 2002 337 343
7. N.K. Pramanik, R.S. Haldar, Y.K. Bhardwaj, S. Sabharwal, U.K. Niyogi, and R.K. Khandal Radiation processing of Nylon 6 by e-beam for improved properties and performance Radiat Phys Chem 78 3 2009 199 205
8. D.W. Lee Permanently crosslinked - electron-beam crosslinking of PA and PBTP Kunst Plast Eur 91 6 2001 78 80
9. Z. Brocka, and G.W. Ehrenstein Crosslinked PA 6 for circuit carriers Kunst Plast Eur 94 11 2004 88 94
10. J. Zimmerman Spectra of irradiated polyamides J Polym Sci 2 5 1959 181 185
11. M.C. Gupta, and R.R. Pandey Gamma -irradiation of nylon 6 J Polym Sci Part A: Polym Chem 26 2 1988 491 502
12. G. Spadaro, D. Acierno, E. Calderaro, and A. Valenza Structural induced modifications in blends of polyamide with gamma irradiated low density polyethylene Radiat Phys Chem 40 3 1992 249 254
13. M.M. Hassan Mechanical, thermal, and morphological behavior of the polyamide 6/acrylonitrile-butadiene-styrene blends irradiated with gamma rays Polym Eng Sci 48 2 2008 373 380 (Pubitemid 351262323)
14. M. Porubská, D. Škerliková, and I. Chodák Optimization of the method of crosslinked portion determination in irradiated polyamide-6 Polym Test 29 2010 196 199
15. S.M. Aharoni n-Nylons 1997 John Wiley & Sons New York
16. R. Sengupta, V.K. Tikku, A.K. Somani, T.K. Chaki, and A.K. Bhownick Electron-beam irradiatied polyamid-6,6 films - II: mechanical and dynamic mechanical properties and water absorption behaviour Radiat Phys Chem 72 6 2005 751 757 (Pubitemid 39574186)
17. M. Horák, and D. Papoušek Infračervená spektra a struktura molekul Infra-red spectra and structure of molecules; in Czech 1st ed. 1976 Academia Praha Prague pp. 656-659
18. J. Maillo, P. Pages, E. Vallejo, T. Lacorte, and J. Gacén FTIR spectroscopy study of the interaction between fibre of polyamide 6 and iodine Eur Polym J 41 4 2005 753 759 (Pubitemid 40183351)
19. G. Socrates Infrared and Raman characteristic group frequencies: tables and charts p.349 3rd ed. 2001 John Wiley&Sohns Chichester Available on: http://books.google.sk/books?id=LDoAAjMnwEIC&printsec=frontcover#v= onepage&q&f=true [7.6.2010]
20. Pockett P. Crystallinity in linear polyamides: a study using melt blending with small-molecule diluents. Thesis. University of South Australia 2004. Appendix C, p.335-337. Available on: http://www.johnpockett.com/Thesis/ Appx-C.pdf [7.6.2010].
21. I.K. Melvin Nylon plastics 1973 John Wiley & Sons New York 683
22. N. Vasanthan, and D.R. Salem FTIR spectroscopic characterization of structural changes in polyamide-6 fibers during annealing and drawing J Polym Sci Part B Polym Phys 39 5 2001 536 547 (Pubitemid 32227255)
23. A.D. Cross, and R.A. Jones An introduction to practical infra-red spectroscopy 3rd ed. 1969 Butterworths & Co. Ltd London
24. V. Milata, P. Segľa, A. Gatiaľ, J. Šima, and V. Kováčik Spektrálne tabuľky pre riešenie úloh a problémov z molekulovej spektroskopie Spectral tables for solution of molecular spectroscopy problems; in Slovak STU Bratislava, pp. 44-54. Available on: 2009 http://www.chtf.stuba.sk/∼milata/SMKTP/ Spektralne%20tabulky.pdf [September 2010].
25. J.T. Edward, H.S. Chang, and K. Yates Can J Chem 38 1960 2271 (Cited from [17])
26. A.R. Katritzky, and R.A.Y. Jones Chem Ind (London) 1961 722 (Cited from [17])
27. H.V. Drushel, J.S. Ellerbe, R.C. Cox, and L.H. Lane Monomer sequence distribution in ethylene-propylene copolymers by computer analysis of infrared spectra Anal Chem 40 2 1968 370 379