Fast-liquid chromatography using columns of different internal diameters packed with sub-2μm silica particles

Journal of Chromatography A

Volumn 1228, Issue , 2012, Pages 213-220

  D'Orazio, Giovanni ^a   Rocco, Anna ^a   Fanali, Salvatore ^a  

^a CNR   (Italy)

Author keywords

Drug analysis; Fast liquid chromatography; Nano liquid chromatography; Sub 2micron particles

Indexed keywords

ANALYSIS TIME; CAPILLARY COLUMNS; CHROMATOGRAPHIC SEPARATIONS; CONCENTRATION LEVELS; CONCENTRATION RANGES; CORRELATION COEFFICIENT; DEXAMETHASONES; DRUG ANALYSIS; INTERNAL DIAMETERS; INTERNAL STANDARDS; LINEAR VELOCITY; MICRO-LIQUID CHROMATOGRAPHY; MOBILE PHASE; NANO-LC; NANO-LIQUID CHROMATOGRAPHY; NONSTEROIDAL ANTI-INFLAMMATORY DRUGS; PEAK AREA; REAL SAMPLES; RELATIVE STANDARD DEVIATIONS; RETENTION FACTORS; RETENTION TIME; SILICA PARTICLES;

DRUG PRODUCTS; FORMIC ACID; HIGH PRESSURE LIQUID CHROMATOGRAPHY; LIPIDS; MIXTURES; SEPARATION; SILICA;

CHROMATOGRAPHY;

11ALPHA HYDROXYPROGESTERONE; 2 (3' CARBOSSIPHENYL)PROPIONIC ACID; 2 (3' CARBOSSIPHENYL)PROPIONITRILE; 2 [(4' BENZOYLOXY 2' HYDROXY)PHENYL]PROPIONIC ACID; ACETONITRILE; CICLOPROFEN; CORTICOSTERONE; CORTISONE; CORTISONE ACETATE; DEXAMETHASONE; DF 1770Y; DF 2008Y; DF 2107Y; FENOPROFEN; FLURBIPROFEN; FORMIC ACID; IBUPROFEN; INDOPROFEN; KETOPROFEN; NONSTEROID ANTIINFLAMMATORY AGENT; PREDNISOLONE; SILICON DIOXIDE; STEROID; TRIAMCINOLONE; TRIAMCINOLONE ACETONIDE; UNCLASSIFIED DRUG; WATER;

ANALYSIS TIME; ANALYTICAL PARAMETERS; ARTICLE; CAPILLARY COLUMN; CONCENTRATION RESPONSE; CONTROLLED STUDY; DRUG DETERMINATION; DRUG FORMULATION; DRUG STRUCTURE; LABORATORY DEVICE; LIMIT OF DETECTION; LIQUID CHROMATOGRAPHY; MICRO LIQUID CHROMATOGRAPHY; NANO LIQUID CHROMATOGRAPHY; PARTICLE SIZE; PLOTS AND CURVES; PRIORITY JOURNAL; PROCESS OPTIMIZATION; PRODUCTIVITY; RETENTION FACTOR; SELECTIVITY; TIME; ULTRA PERFORMANCE LIQUID CHROMATOGRAPHY; VALIDATION PROCESS; VAN DEEMTER CURVE; VELOCITY;

ANTI-INFLAMMATORY AGENTS, NON-STEROIDAL; CHROMATOGRAPHY, LIQUID; LIMIT OF DETECTION; PARTICLE SIZE; PRESSURE; REPRODUCIBILITY OF RESULTS; SILICON DIOXIDE; STEROIDS;

EID: 84857055883     PISSN: 00219673     EISSN: 18733778     Source Type: Journal    
DOI: 10.1016/j.chroma.2011.05.053     Document Type: Article

References (36)

1. Nguyen D.T.-T., Guillarme D., Rudaz S., Veuthey J.-L. J. Sep. Sci. 2006, 29:1836.
2. Mutton I.M. Chromatographia 1998, 47:291.
3. Van Deemter J.J., Zuiderweg F.J., Kinkenberg A. Chem. Eng. Sci. 1956, 5:271.
4. Knox J.H., Saleem M. J. Chromatogr. Sci. 1969, 7:614.
5. Knox J.H. J. Chromatogr. Sci. 1977, 15:352.
6. Wu N., Clausen A.M. J. Sep. Sci. 2007, 30:1167.
7. Gritti F., Guiochon G. J. Chromatogr. A 2010, 1217:7677.
8. Gritti F., Guiochon G. J. Chromatogr. A 2010, 1217:5069.
9. Gritti F., Guiochon G. Chem. Eng. Sci. 2010, 65:6327.
10. Cunliffe J.M., Adams-Hall S.B., Maloney T.D. J. Sep. Sci. 2007, 30:1214.
11. de Villiers A., Lauer H., Szucs R., Goodall S., Sandra P. J. Chromatogr. A 2006, 1113:84.
12. Colon L.A., Cintron J.M., Anspach J.A., Fermier A.M., Swinney K.A. Analyst 2004, 129:503.
13. Karlsson K.E., Novotny M. Anal. Chem. 1988, 60:1662.
14. Anspach J.A., Maloney T.D., Colon L.A. J. Sep. Sci. 2007, 30:1207.
15. Lestremau F., Wu D., Sucz R. J. Chromatogr. A 2010, 1217:4925.
16. Thomas A., Kohler M., Schänzer W., Kamber M., Delahaut P., Thevis M. Rapid Commun. Mass Spectrom. 2009, 23:2669.
17. Wu N., Lippert J.A., Lee M.L. J. Chromatogr. A 2001, 911:1.
18. Patel K.D., Jerkovich A.D., Link J.C., Jorgenson J.W. Anal. Chem. 2004, 76:5777.
19. Fekete S., Fekete J., Ganzler K. J. Pharm. Biomed. Anal. 2009, 49:833.
20. http://bioszeparacio.hu/_user/browser/File/Thermo/GOLD%25201_9%2520Method%2520Optimisation%2520(TG20338_E%25201006M_L).pdf.
21. Baranowska I., Kowalski B. Water Air Soil Pollut. 2011, 211:417.
22. Petrovic M., Gros M., Bacelo D. J. Chromatogr. A 2006, 1124:68.
23. Brombacher S., Owen S.J., Volmer D.A. Anal. Bioanal. Chem. 2003, 376:773.
24. Pesek J.J., Matyska M.T., Sukul D. J. Chromatogr. A 2008, 1191:136.
25. Saevels J., Wuyts M., Van Schepdael A., Roets E., Hoogmartens J. J. Pharm. Biomed. Anal. 1999, 3:513.
26. Stead D.A., Reid R.G., Taylor R.B. J. Chromatogr. A. 1998, 798:259.
27. Fanali S., D'Orazio G., Quaglia M.G. Chromatographia 2004, 60:S239.
28. http://userpages.xfoneusa.net/~dhyams/cftp.htm.
29. Fanali S., Arturki Z., D'Orazio G., Rocco A. J. Chromatogr. A 2007, 1150:252.
30. Rocco A., Fanali S. J. Chromatogr. A 2009, 1216:7173.
31. Heinisch S., Desmet G., Clicq D., Rocca J.-L. J. Chromatogr. A 2008, 1203:124.
32. Kennedy R.T., Jorgenson J.W. Anal. Chem. 1989, 61:1128.
33. Hsieh S., Jorgenson J.W. Anal. Chem. 1996, 68:1212.
34. Mills M.J., Maltas J., Lough W.J. J. Chromatogr. A 1997, 759:1.
35. Vissers J.P.C., de Ru A.H., Ursem M., Chervet J.-P. J. Chromatogr. A 1996, 746:1.
36. Arthur K.E., Wolff J.-C., Carrier D.J. Rapid Commun. Mass Spectrom. 2004, 18:678.