메뉴 건너뛰기




Volumn , Issue , 2011, Pages 105-125

Modeling Chromatographic Band Broadening in Monolithic Columns

Author keywords

[No Author keywords available]

Indexed keywords


EID: 84856597652     PISSN: None     EISSN: None     Source Type: Book    
DOI: 10.1002/9783527633241.ch6     Document Type: Chapter
Times cited : (3)

References (51)
  • 1
    • 84859338859 scopus 로고
    • Continuous rods of macroporous polymer as high -performance liquid chromatography separation media
    • Svec, F., and Frechet, J.M. (1992) Continuous rods of macroporous polymer as high -performance liquid chromatography separation media. Anal. Chem., 64, 820-822.
    • (1992) Anal. Chem. , vol.64 , pp. 820-822
    • Svec, F.1    Frechet, J.M.2
  • 2
    • 0004547564 scopus 로고    scopus 로고
    • Octadecylsilylated porous silica rods as separation media for reversed -phase liquid chromatography
    • Minakuchi, H., Nakanishi, K., Soga, N., Ishizuka, N., and Tanaka, N. (1996) Octadecylsilylated porous silica rods as separation media for reversed -phase liquid chromatography. Anal. Chem., 68, 3498-3501.
    • (1996) Anal. Chem. , vol.68 , pp. 3498-3501
    • Minakuchi, H.1    Nakanishi, K.2    Soga, N.3    Ishizuka, N.4    Tanaka, N.5
  • 3
    • 0000651036 scopus 로고
    • High -performance liquid -chromatography on continuous polymer beds
    • Hjerten, S., Liao, L.J., and Zhang, R. (1989) High -performance liquid -chromatography on continuous polymer beds. J. Chromatogr., 473, 273-275.
    • (1989) J. Chromatogr. , vol.473 , pp. 273-275
    • Hjerten, S.1    Liao, L.J.2    Zhang, R.3
  • 4
    • 61349154252 scopus 로고    scopus 로고
    • Flow -through pore characteristics of monolithic silicas and their impact on column performance in high -performance liquid chromatography
    • Skudas, R., Grimes, B.A., Thommes, M., and Unger, K.K. (2009) Flow -through pore characteristics of monolithic silicas and their impact on column performance in high -performance liquid chromatography. J. Chromatogr. A, 1216, 2625-2636.
    • (2009) J. Chromatogr. A , vol.1216 , pp. 2625-2636
    • Skudas, R.1    Grimes, B.A.2    Thommes, M.3    Unger, K.K.4
  • 5
    • 33747802798 scopus 로고    scopus 로고
    • About the C term in the van Deemter ' s equation of plate height in monoliths
    • Siouffi, A.M. (2006) About the C term in the van Deemter ' s equation of plate height in monoliths. J. Chromatogr. A, 1126, 86-94.
    • (2006) J. Chromatogr. A , vol.1126 , pp. 86-94
    • Siouffi, A.M.1
  • 6
    • 0032944605 scopus 로고    scopus 로고
    • Band dispersion in chromatography -a new view of A -term dispersion
    • Knox, J.H. (1999) Band dispersion in chromatography -a new view of A -term dispersion. J. Chromatogr. A, 831, 3-15.
    • (1999) J. Chromatogr. A , vol.831 , pp. 3-15
    • Knox, J.H.1
  • 7
    • 0032785691 scopus 로고    scopus 로고
    • Network modeling of the convective flow and diffusion of molecules adsorbing in monoliths and in porous particles packed in a chromatographic column
    • Meyers, J.J., and Liapis, A.I. (1999) Network modeling of the convective flow and diffusion of molecules adsorbing in monoliths and in porous particles packed in a chromatographic column. J. Chromatogr. A, 852, 3-23.
    • (1999) J. Chromatogr. A , vol.852 , pp. 3-23
    • Meyers, J.J.1    Liapis, A.I.2
  • 8
    • 0031581827 scopus 로고    scopus 로고
    • Effect of skeleton size on the performance of octadecylsilylated continuous porous silica columns in reversed -phase liquid chromatography
    • Minakuchi, H., Nakanishi, K., Soga, N., Ishizuka, N., and Tanaka, N. (1997) Effect of skeleton size on the performance of octadecylsilylated continuous porous silica columns in reversed -phase liquid chromatography. J. Chromatogr. A, 762, 135-146.
    • (1997) J. Chromatogr. A , vol.762 , pp. 135-146
    • Minakuchi, H.1    Nakanishi, K.2    Soga, N.3    Ishizuka, N.4    Tanaka, N.5
  • 9
    • 0032570914 scopus 로고    scopus 로고
    • Effect of domain size on the performance of octadecylsilylated continuous porous silica columns in reversed -phase liquid chromatography
    • Minakuchi, H., Nakanishi, K., Soga, N., Ishizuka, N., and Tanaka, N. (1998) Effect of domain size on the performance of octadecylsilylated continuous porous silica columns in reversed -phase liquid chromatography. J. Chromatogr. A, 797, 121-132.
    • (1998) J. Chromatogr. A , vol.797 , pp. 121-132
    • Minakuchi, H.1    Nakanishi, K.2    Soga, N.3    Ishizuka, N.4    Tanaka, N.5
  • 12
    • 0037194962 scopus 로고    scopus 로고
    • The moment equations of chromatography for monolithic stationary phases
    • Miyabe, K., and Guiochon, G. (2002) The moment equations of chromatography for monolithic stationary phases. J. Phys. Chem. B, 106, 8898-8909.
    • (2002) J. Phys. Chem. B , vol.106 , pp. 8898-8909
    • Miyabe, K.1    Guiochon, G.2
  • 13
    • 0346753671 scopus 로고    scopus 로고
    • Moment analysis of mass -transfer kinetics in C -18 -silica monolithic columns
    • Miyabe, K., Cavazzini, A., Gritti, F., Kele, M., and Guiochon, G. (2003) Moment analysis of mass -transfer kinetics in C -18 -silica monolithic columns. Anal. Chem., 75, 6975-6986.
    • (2003) Anal. Chem. , vol.75 , pp. 6975-6986
    • Miyabe, K.1    Cavazzini, A.2    Gritti, F.3    Kele, M.4    Guiochon, G.5
  • 14
    • 0036883295 scopus 로고    scopus 로고
    • Fluid dynamics in monolithic adsorbents: Phenomenological approach to equivalent particle dimensions
    • Tallarek, U., Leinweber, F.C., and Seidel -Morgenstern, A. (2002) Fluid dynamics in monolithic adsorbents: Phenomenological approach to equivalent particle dimensions. Chem. Eng. Technol., 25, 1177-1182.
    • (2002) Chem. Eng. Technol. , vol.25 , pp. 1177-1182
    • Tallarek, U.1    Leinweber, F.C.2    Seidel -Morgenstern, A.3
  • 15
    • 0036606582 scopus 로고    scopus 로고
    • Characterization of silica -based monoliths with bimodal pore size distribution
    • Leinweber, F.C., Lubda, D., Cabrera, K., and Tallarek, U. (2002) Characterization of silica -based monoliths with bimodal pore size distribution. Anal. Chem., 74, 2470-2477.
    • (2002) Anal. Chem. , vol.74 , pp. 2470-2477
    • Leinweber, F.C.1    Lubda, D.2    Cabrera, K.3    Tallarek, U.4
  • 16
    • 0042347638 scopus 로고    scopus 로고
    • Chromatographic performance of monolithic and particulate stationary phases -hydrodynamics and adsorption capacity
    • Leinweber, F.C., and Tallarek, U. (2003) Chromatographic performance of monolithic and particulate stationary phases -hydrodynamics and adsorption capacity. J. Chromatogr. A, 1006, 207-228.
    • (2003) J. Chromatogr. A , vol.1006 , pp. 207-228
    • Leinweber, F.C.1    Tallarek, U.2
  • 18
    • 85010246622 scopus 로고
    • Longitudinal diffusion and resistance to mass transfer as causes of non ideality in chromatography
    • van Deemter, J.J., Zuiderweg, F.J., and Klinkenberg, A. (1956) Longitudinal diffusion and resistance to mass transfer as causes of non ideality in chromatography. Chem. Eng. Sci., 5, 271-289.
    • (1956) Chem. Eng. Sci. , vol.5 , pp. 271-289
    • van Deemter, J.J.1    Zuiderweg, F.J.2    Klinkenberg, A.3
  • 19
    • 0002442533 scopus 로고
    • Role of lateral diffusion as a rate -controlling mechanism in chromatography
    • Giddings, J.C. (1961) Role of lateral diffusion as a rate -controlling mechanism in chromatography. J. Chromatogr., 5, 46-60.
    • (1961) J. Chromatogr. , vol.5 , pp. 46-60
    • Giddings, J.C.1
  • 20
    • 0003842710 scopus 로고
    • Dynamics of Chromatography Part 1
    • Marcel Dekker, New York
    • Giddings, J.C. (1965) Dynamics of Chromatography Part 1, Marcel Dekker, New York.
    • (1965)
    • Giddings, J.C.1
  • 21
    • 0034329655 scopus 로고    scopus 로고
    • A kinetic study of mass transfer in reversed -phase liquid chromatography on a C18 -silica gel
    • Miyabe, K., and Guiochon, G. (2000) A kinetic study of mass transfer in reversed -phase liquid chromatography on a C18 -silica gel. Anal. Chem., 72, 5162-5171.
    • (2000) Anal. Chem. , vol.72 , pp. 5162-5171
    • Miyabe, K.1    Guiochon, G.2
  • 22
    • 55549094435 scopus 로고    scopus 로고
    • Equivalence of the Different C m -and C s -term expressions used in liquid chromatography and a geometrical model uniting them
    • Desmet, G., and Broeckhoven, K. (2008) Equivalence of the Different C m -and C s -term expressions used in liquid chromatography and a geometrical model uniting them. Anal. Chem., 80, 8076-8088.
    • (2008) Anal. Chem. , vol.80 , pp. 8076-8088
    • Desmet, G.1    Broeckhoven, K.2
  • 23
    • 33746852389 scopus 로고    scopus 로고
    • General HETP equation for the study of mass -transfer mechanisms in RPLC
    • Gritti, F., and Guiochon, G. (2006) General HETP equation for the study of mass -transfer mechanisms in RPLC. Anal. Chem., 78, 5329-5347.
    • (2006) Anal. Chem. , vol.78 , pp. 5329-5347
    • Gritti, F.1    Guiochon, G.2
  • 24
    • 84954000171 scopus 로고
    • Model for application of gas -chromatography to measurements of diffusion in bidisperse structured catalysts
    • Haynes, H.W., and Sarma, P.N. (1973) Model for application of gas -chromatography to measurements of diffusion in bidisperse structured catalysts. AIChE J., 19, 1043-1046.
    • (1973) AIChE J. , vol.19 , pp. 1043-1046
    • Haynes, H.W.1    Sarma, P.N.2
  • 25
    • 85008726847 scopus 로고
    • High efficiency high speed liquid chromatography in columns
    • Huber, J. (1969) High efficiency high speed liquid chromatography in columns. J. Chromatogr. Sci., 7, 85-90.
    • (1969) J. Chromatogr. Sci. , vol.7 , pp. 85-90
    • Huber, J.1
  • 26
    • 0000913121 scopus 로고
    • Movement and band spreading of unsorbed solutes in liquid -chromatography
    • Horvath, C., and Lin, H. -J. (1976) Movement and band spreading of unsorbed solutes in liquid -chromatography. J. Chromatogr., 126, 401-420.
    • (1976) J. Chromatogr. , vol.126 , pp. 401-420
    • Horvath, C.1    Lin, H.-J.2
  • 27
    • 0003017403 scopus 로고
    • Band spreading in liquid -chromatography -general plate height equation and a method for evaluation of individual plate height contributions
    • Horvath, C., and Lin, H. -J. (1978) Band spreading in liquid -chromatography -general plate height equation and a method for evaluation of individual plate height contributions. J. Chromatogr., 149, 43-70.
    • (1978) J. Chromatogr. , vol.149 , pp. 43-70
    • Horvath, C.1    Lin, H.-J.2
  • 28
    • 0013792568 scopus 로고
    • Contribution to theory of chromatography linear non -equilibrium elution chromatography
    • Kucera, E. (1965) Contribution to theory of chromatography linear non -equilibrium elution chromatography. J. Chromatogr., 19, 237-248.
    • (1965) J. Chromatogr. , vol.19 , pp. 237-248
    • Kucera, E.1
  • 29
    • 0003563262 scopus 로고
    • Fundamentals of Preparative and Nonlinear Chromatography
    • Academic Press, Boston
    • Guiochon, G., Golshan -Shirazi, S., and Katti, A.M. (1994) Fundamentals of Preparative and Nonlinear Chromatography, Academic Press, Boston.
    • (1994)
    • Guiochon, G.1    Golshan -Shirazi, S.2    Katti, A.M.3
  • 30
    • 3242769785 scopus 로고    scopus 로고
    • Measurement of intraparticle diffusion in reversed phase liquid chromatography
    • Hong, L., Felinger, A., Kaczmarski, K., and Guiochon, G. (2004) Measurement of intraparticle diffusion in reversed phase liquid chromatography. Chem. Eng. Sci., 59, 3399-3412.
    • (2004) Chem. Eng. Sci. , vol.59 , pp. 3399-3412
    • Hong, L.1    Felinger, A.2    Kaczmarski, K.3    Guiochon, G.4
  • 31
    • 34347240027 scopus 로고    scopus 로고
    • Modeling of the mass -transfer kinetics in chromatographic columns packed with shell and pellicular particles
    • Kaczmarski, K., and Guiochon, G. (2007) Modeling of the mass -transfer kinetics in chromatographic columns packed with shell and pellicular particles. A nal. Chem., 79, 4648-4656.
    • (2007) A nal. Chem. , vol.79 , pp. 4648-4656
    • Kaczmarski, K.1    Guiochon, G.2
  • 32
    • 39149138429 scopus 로고    scopus 로고
    • Evaluation of chromatographic performance of various packing materials having different structural characteristics as stationary phase for fast high performance liquid chromatography by new moment equations
    • Miyabe, K. (2008) Evaluation of chromatographic performance of various packing materials having different structural characteristics as stationary phase for fast high performance liquid chromatography by new moment equations. J. Chromatogr. A, 1183, 49-64.
    • (2008) J. Chromatogr. A , vol.1183 , pp. 49-64
    • Miyabe, K.1
  • 33
    • 0037032671 scopus 로고    scopus 로고
    • Novel general expressions that describe the behavior of the height equivalent of a theoretical plate in chromatographic systems involving electrically -driven and pressure -driven flows
    • Grimes, B.A., Lüdtke, S., Unger, K.K., and Liapis, A.I. (2002) Novel general expressions that describe the behavior of the height equivalent of a theoretical plate in chromatographic systems involving electrically -driven and pressure -driven flows. J. Chromatogr. A, 979, 447-466.
    • (2002) J. Chromatogr. A , vol.979 , pp. 447-466
    • Grimes, B.A.1    Lüdtke, S.2    Unger, K.K.3    Liapis, A.I.4
  • 34
    • 17744369361 scopus 로고
    • Liquid mass transfer at very low Reynolds numbers in packed beds
    • Wilson, E.J., and Geankoplis, C.J. (1966) Liquid mass transfer at very low Reynolds numbers in packed beds. Ind. Eng. Chem. Fundam., 5, 9-14.
    • (1966) Ind. Eng. Chem. Fundam. , vol.5 , pp. 9-14
    • Wilson, E.J.1    Geankoplis, C.J.2
  • 35
    • 4344717022 scopus 로고    scopus 로고
    • A computational study of the porosity effects in silica monolithic columns
    • Gzil, P., Vervoort, N., Baron, G.V., and Desmet, G. (2004) A computational study of the porosity effects in silica monolithic columns. J. Sep. Sci., 27, 887-896.
    • (2004) J. Sep. Sci. , vol.27 , pp. 887-896
    • Gzil, P.1    Vervoort, N.2    Baron, G.V.3    Desmet, G.4
  • 36
    • 41549162315 scopus 로고    scopus 로고
    • Errors involved in the existing B -term expressions for the longitudinal diffusion in fully porous chromatographic media -part I: computational data in ordered pillar arrays and effective medium theory
    • Desmet, G., Broeckhoven, K., De Smet, J., Deridder, S., Baron, G.V., and Gzil, P. (2008) Errors involved in the existing B -term expressions for the longitudinal diffusion in fully porous chromatographic media -part I: computational data in ordered pillar arrays and effective medium theory. J. Chromatogr. A, 1188, 171-188.
    • (2008) J. Chromatogr. A , vol.1188 , pp. 171-188
    • Desmet, G.1    Broeckhoven, K.2    De Smet, J.3    Deridder, S.4    Baron, G.V.5    Gzil, P.6
  • 37
    • 41549111387 scopus 로고    scopus 로고
    • Errors involved in the existing B -term expressions for the longitudinal diffusion in fully porous chromatographic media -Part II: Experimental data in packed columns and surface diffusion measurements
    • Broeckhoven, K., Cabooter, D., Lynen, F., Sandra, P., and Desmet, G. (2008) Errors involved in the existing B -term expressions for the longitudinal diffusion in fully porous chromatographic media -Part II: Experimental data in packed columns and surface diffusion measurements. J. Chromatogr. A, 1188, 189-198.
    • (2008) J. Chromatogr. A , vol.1188 , pp. 189-198
    • Broeckhoven, K.1    Cabooter, D.2    Lynen, F.3    Sandra, P.4    Desmet, G.5
  • 38
    • 84984085862 scopus 로고
    • Correlation of diffusion coefficients in dilute solutions
    • Wilke, C.R., and Chang, P. (1955) Correlation of diffusion coefficients in dilute solutions. AICHE J., 1, 264-270.
    • (1955) AICHE J. , vol.1 , pp. 264-270
    • Wilke, C.R.1    Chang, P.2
  • 39
    • 0000306011 scopus 로고
    • Liquid diffusivities
    • Scheibel, E.G. (1954) Liquid diffusivities. Ind. Eng. Chem., 46, 2007-2008.
    • (1954) Ind. Eng. Chem. , vol.46 , pp. 2007-2008
    • Scheibel, E.G.1
  • 40
    • 0031182013 scopus 로고    scopus 로고
    • Accuracy of empirical correlations for estimating diffusion coefficients in aqueous organic mixtures
    • Li, J., and Carr, P.W. (1997) Accuracy of empirical correlations for estimating diffusion coefficients in aqueous organic mixtures. Anal. Chem., 69, 2530-2536.
    • (1997) Anal. Chem. , vol.69 , pp. 2530-2536
    • Li, J.1    Carr, P.W.2
  • 41
    • 57149102554 scopus 로고    scopus 로고
    • Experimental study of porous silicon shell pillars under retentive conditions
    • De Malsche, W., Gardeniers, H., and Desmet, G. (2008) Experimental study of porous silicon shell pillars under retentive conditions. Anal. Chem., 80, 5391-5400.
    • (2008) Anal. Chem. , vol.80 , pp. 5391-5400
    • De Malsche, W.1    Gardeniers, H.2    Desmet, G.3
  • 42
    • 0003804374 scopus 로고
    • Fundamentals of Heat and Mass Transfer
    • 2nd edn, John Wiley & Sons, Inc., New York
    • Incropera, F.P., and De Witt, D.P. (1985) Fundamentals of Heat and Mass Transfer, 2nd edn, John Wiley & Sons, Inc., New York.
    • (1985)
    • Incropera, F.P.1    De Witt, D.P.2
  • 43
    • 85007999849 scopus 로고
    • Mass transfer in laminar region between liquid and packing material surface in the packed bed
    • Kataoka, T., Yoshida, H., and Ueyama, K. (1972) Mass transfer in laminar region between liquid and packing material surface in the packed bed. J. Chem. Eng. Jpn., 5, 132-136.
    • (1972) J. Chem. Eng. Jpn. , vol.5 , pp. 132-136
    • Kataoka, T.1    Yoshida, H.2    Ueyama, K.3
  • 44
    • 7944235657 scopus 로고
    • Transport Phenomena
    • John Wiley & Sons, Inc., New York
    • Bird, R.B., Stewart, W.E., and Lightfoot, E.N. (1962) Transport Phenomena, John Wiley & Sons, Inc., New York.
    • (1962)
    • Bird, R.B.1    Stewart, W.E.2    Lightfoot, E.N.3
  • 45
    • 0004111751 scopus 로고    scopus 로고
    • Coulson & Richardson ' s Chemical Engineering
    • 5th edn, Elsevier Butterworth -Heinemann, Oxford
    • Richardson, J.F., Harker, J.H., and Backhurst, J.R. (2002) Coulson & Richardson ' s Chemical Engineering, vol. 2, 5th edn, Elsevier Butterworth -Heinemann, Oxford.
    • (2002) , vol.2
    • Richardson, J.F.1    Harker, J.H.2    Backhurst, J.R.3
  • 47
    • 0037442324 scopus 로고    scopus 로고
    • A correlation for the pressure drop in monolithic silica columns
    • Vervoort, N., Gzil, P., Baron, G.V., and Desmet, G. (2003) A correlation for the pressure drop in monolithic silica columns. Anal. Chem., 75, 843-850.
    • (2003) Anal. Chem. , vol.75 , pp. 843-850
    • Vervoort, N.1    Gzil, P.2    Baron, G.V.3    Desmet, G.4
  • 48
    • 1242293003 scopus 로고    scopus 로고
    • Model column structure for the analysis of the flow and band -broadening characteristics of silica monoliths
    • Vervoort, N., Gzil, P., Baron, G.V., and Desmet, G. (2004) Model column structure for the analysis of the flow and band -broadening characteristics of silica monoliths. J. Chromatogr. A, 1030, 177-186.
    • (2004) J. Chromatogr. A , vol.1030 , pp. 177-186
    • Vervoort, N.1    Gzil, P.2    Baron, G.V.3    Desmet, G.4
  • 49
    • 65449154301 scopus 로고    scopus 로고
    • Mass transfer kinetic mechanism in monolithic columns and application to the characterization of new research monolithic samples with different average pore sizes
    • Gritti, F., and Guiochon, G. (2009) Mass transfer kinetic mechanism in monolithic columns and application to the characterization of new research monolithic samples with different average pore sizes. J. Chromatogr. A, 1216, 4752-4767.
    • (2009) J. Chromatogr. A , vol.1216 , pp. 4752-4767
    • Gritti, F.1    Guiochon, G.2
  • 50
    • 0037414678 scopus 로고    scopus 로고
    • Study of the mass transfer kinetics in a monolithic column
    • Gritti, F., Piatkowski, W., and Guiochon, G. (2003) Study of the mass transfer kinetics in a monolithic column. J. Chromatogr. A, 983, 51-71.
    • (2003) J. Chromatogr. A , vol.983 , pp. 51-71
    • Gritti, F.1    Piatkowski, W.2    Guiochon, G.3
  • 51
    • 34748882992 scopus 로고    scopus 로고
    • Monolithic columns in high -performance liquid chromatography
    • Guiochon, G. (2007) Monolithic columns in high -performance liquid chromatography. J. Chromatogr. A, 1168, 101-168.
    • (2007) J. Chromatogr. A , vol.1168 , pp. 101-168
    • Guiochon, G.1


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.