Multistep crystallization process involving sequential formations of density fluctuations, "intermediate structures", and lamellar crystallites: Poly(3-hydroxybutyrate) As investigated by time-resolved synchrotron SAXS and WAXD

Macromolecules

Volumn 45, Issue 1, 2012, Pages 313-328

  Guo, Longhai ^a   Spegazzini, Nicolas ^a   Sato, Harumi ^a   Hashimoto, Takeji ^a,b,e   Masunaga, Hiroyasu ^c   Sasaki, Sono ^c,d   Takata, Masaki ^c   Ozaki, Yukihiro ^a  

^a KWANSEI GAKUIN UNIVERSITY   (Japan)

^b KYOTO UNIVERSITY   (Japan)

^c JAPAN SYNCHROTRON RADIATION RESEARCH INSTITUTE   (Japan)

^d KYOTO INSTITUTE OF TECHNOLOGY   (Japan)

^e NATIONAL TSING HUA UNIVERSITY   (Taiwan)

Author keywords

[No Author keywords available]

Indexed keywords

AMORPHOUS MATRICES; CORRELATION FUNCTION; CRYSTALLIZATION PROCESS; DENSITY FLUCTUATION; HYDROXYBUTYRATE; INTERMEDIATE STRUCTURES; ISOTHERMAL CRYSTALLIZATION; MULTI-STEP; MULTIVARIATE CURVE RESOLUTION-ALTERNATING LEAST SQUARES; POLY(3-HYDROXYBUTYRATE); PRECISE ANALYSIS; PURE CRYSTALS; SIMULTANEOUS MEASUREMENT; SMALL ANGLE X-RAY SCATTERING; TIME-RESOLVED; TWO-DIMENSIONAL CORRELATION SPECTROSCOPY; WEIGHT FRACTIONS; WIDE-ANGLE X-RAY DIFFRACTION;

CRYSTALLITES; LAMELLAR STRUCTURES; X RAY DIFFRACTION; X RAY SCATTERING;

X RAY DIFFRACTION ANALYSIS;

EID: 84855696534     PISSN: 00249297     EISSN: None     Source Type: Journal    
DOI: 10.1021/ma201475t     Document Type: Article

References (55)

1. Strobl, G. R. The Physics of Polymers; Springer-Verlag: Berlin, 1997.
2. Lotz, B. Eur. Phys. J. E 2000, 3, 185-1894
3. Wunderlich, B. Prog. Polym. Sci. 2003, 28, 383-450
4. Cornibert, J.; Marchessault, R. H. J. Mol. Biol. 1972, 71, 735-756
5. Yokouchi, M.; Chatani, Y.; Tadokoro, H.; Teranishi, K.; Tani, H. Polymer 1973, 14, 267-272
6. Doi, Y. Microbial Polyester; VCH Publishers: New York, 1990.
7. Anderson, A. J.; Dawes, E. A. Mirobiol. Rev. 1990, 54, 450-472
8. Lara, M. L.; Gjalt, H. W. Microbiol. Mol. Biol. Rev. 1999, 63, 21-53
9. Iwata, T.; Doi, Y. Macromol. Chem. Phys. 1999, 200, 2429-2442
10. Sato, H.; Nakamura, M.; Padermshoke, A.; Yamaguchi, H.; Terauchi, H.; Ekgasit, S.; Noda, I.; Ozaki, Y. Macromolecules 2004, 37, 3763-3769
11. Sato, H.; Murakami, R.; Padermshoke, A.; Hirose, F.; Senda, K.; Noda, I.; Ozaki, Y. Macromolecules 2004, 37, 7203-7213
12. Sato, H.; Murakami, R.; Zhang, J.; Mori, K.; Takahashi, I.; Terauchi, H.; Noda, I.; Ozaki, Y. Macromol. Symp. 2005, 230, 158-166
13. Sato, H.; Mori, K.; Murakami, R.; Ando, Y.; Takahashi, I.; Zhang, J.; Terauchi, H.; Hirose, F.; Senda, K.; Tashiro, K.; Noda, I.; Ozaki, Y. Macromolecules 2006, 39, 1525-1531
14. Sato, H.; Ando, Y.; Dybal, J.; Iwata, T.; Noda, I.; Ozaki, Y. Macromolecules 2008, 41, 4305-4312
15. Guo, L. H.; Sato, H.; Hashimoto, T.; Ozaki, Y. Macromolecules 2010, 43, 3897-3902
16. Guo, L. H.; Sato, H.; Hashimoto, T.; Ozaki, Y. Macromolecules 2011, 44, 2229-2239
17. Suttiwijitpukdee, N.; Sato, H.; Zhang, J.; Hashimoto, T.; Ozaki, Y. Polymer 2011, 52, 461-471
18. An, Y.; Dong, L.; Li, L.; Mo, Z.; Feng, Z. Eur. Polym. J. 1999, 35, 365-369
19. Androsch, R. Polymer 2008, 49, 4673-4679
20. Zhang, J.; Sato, H.; Noda, I.; Ozaki, Y. Macromolecules 2005, 38, 4274-4281
21. Suttiwijitpukdee, N.; Sato, H.; Zhang, J.; Hashimoto, T. Macromolecules 2011, 44, 3467-3477
22. Tashiro, K.; Sasaki, S.; Gose, N.; Kobayashi, M. Polym. J. 1998, 30, 485-491
23. Kanig, G. Colloid Polym. Sci. 1991, 269, 1118-1125
24. Saijo, K.; Hashimoto, T. Mater. Res. Soc. Symp. Proc. 1986, 79, 267-276
25. Saijo, K.; Zhu, Y. P.; Hashimoto, T.; Wasiak, A.; Brzostowski, N. J. Appl. Polym. Sci. 2007, 105, 137-157
26. Okada, T.; Saito, H.; Inoue, T. Macromolecules 1992, 25, 1908-1911
27. Pogodina, N. V.; Siddiquee, S. K.; van Egmond, J. W.; Winter, H. H. Macromolecules 1999, 32, 1167-1174
28. Matsuba, G.; Kaji, K.; Nishida, K.; Kanaya, T.; Imai, M. Polym. J. 1999, 31, 722-727
29. Strobl, G. R. Eur. Phys. J. E 2000, 3, 165-183
30. Sajkiewicz, P.; Hashimoto, T.; Saijo, K.; Gradys, A. Polymer 2005, 46, 513-521
31. Noda, I. Appl. Spectrosc. 1993, 47, 1329-1336
32. Noda, I.; Dowrey, A. E.; Marott, C.; Story, G. M.; Ozaki, Y. Appl. Spectrosc. 2000, 54, 236A-248A
33. Noda, I.; Ozaki, Y. Two-Dimensional Correlation Spectroscopy; John Wiley & Sons: Chichester, UK, 2004.
34. Marquez-Alvarez, C.; Rodriguez-Ramos, I.; Guerrero-Ruiz, A.; Haller, G. L.; Fernandez-Garcia, M. J. Am. Chem. Soc. 1997, 119, 2905-2914
35. Larrechi, S. M.; Rius, X. F. Appl. Spectrosc. 2004, 58, 47-53
36. Garrido, M.; Lazaro, I.; Larrechi, S. M.; Rius, X. F. Anal. Chim. Acta 2004, 515, 65-73
37. Spegazzini, N.; Ruisanchez, I.; Larrechi, S. M.; Cadiz, V.; Canadell, J. Analyst 2008, 133, 1028-1035
38. Perera, P.; Wyche, M.; Loethen, Y.; Ben-Amotz, D. J. Am. Chem. Soc. 2008, 130, 4576-4577
39. Spegazzini, N.; Ruisanchez, I.; Larrechi, S. M. Anal. Chim. Acta 2009, 642, 155-162
40. Blobel, J.; Bernado, P.; Svergun, I. D.; Tauler, R.; Pons, M. J. Am. Chem. Soc. 2009, 131, 4378-4386
41. Iglesias-Juez, A.; Kubacka, A.; Fernandez-Garcia, M.; Michiel, M. D.; Newton, M. A. J. Am. Chem. Soc. 2011, 133, 4484-4489
42. Sasaki, S.; Sato, H.; Funatsu, R.; Yoshimoto, J.; Masunaga, H.; Ogawa, H. SPring-8 User Experiment Report 2008B, 2026
43. Masunaga, H.; Ogawa, H.; Sasaki, S. SPring-8 User Experiment Report 2010B, 1068
44. Strobl, G. R.; Schneider, M. J. Polym. Sci., Polym. Phys. Ed. 1980, 18, 1343-1359
45. Guinier, A. Ann. Phys. 1939, 12, 161-237
46. Guinier, A.; Fournet, G. Small Angle X-ray Scattering; John Wiley & Sons, Inc.: London, 1955.
47. Porod, G. Kolloidn. Zh. 1951, 124, 83-111
48. Porod, G. Kolloidn. Zh. 1952, 125, 51-57
49. Hsiao, B. S.; Wang, Z.; Yeh, F.; Gao, Y.; Sheth, C. K. Polymer 1999, 40, 3515-3523
50. Sasaki, S.; Tashiro, K.; Kobayashi, M.; Izumi, Y.; Kobayashi, K. Polymer 1999, 40, 7125-7135
51. Lisowski, S. M.; Liu, Q.; Cho, J.; Runt, J.; Yeh, F.; Hsiao, B. S. Macromolecules 2000, 33, 4842-4849
52. Hama, H.; Tashiro, K. Polymer 2003, 44, 6973-6988
53. Reddy, R. K.; Tashiro, K.; Sakurai, T.; Yamaguchi, N.; Sasaki, S.; Masunaga, H.; Takata, M. Macromolecules 2009, 42, 4191-4199
54. Maeder, M. Anal. Chem. 1987, 59, 527-530
55. II'ichev, Y. V.; Schworer, M. A.; Wirz, J. J. Am. Chem. Soc. 2004, 126, 4581-4595