Low temperature nanocasting of hematite nanoparticles using mesoporous silica molds

Powder Technology

Volumn 217, Issue , 2012, Pages 269-273

  Ballem, Mohamed A ^a   Zhang, Xuanjun ^a   Johansson, Emma M ^a   Córdoba, José M ^a   Odén, Magnus ^a  

^a LINKÖPING UNIVERSITY   (Sweden)

Author keywords

Fe 2O 3; Mesoporous silica; Nanocasting; Nanoparticles; SBA 15; SBA 16

Indexed keywords

AVERAGE DIAMETER; HEMATITE NANOPARTICLES; HIGH CRYSTALLINITY; HYDROTHERMAL TREATMENTS; LOW TEMPERATURES; MESOPOROUS SILICA; NANOCASTING; NARROW SIZE DISTRIBUTIONS; OXIDE PRECURSORS; SBA-15; SBA-16; SILICA PORES; SMALL SIZE; WELL-DISPERSED; WET-IMPREGNATION;

IRON ORES; IRON OXIDES; MESOPOROUS MATERIALS; MOLDS; NANOPARTICLES; SILICA;

HIGH RESOLUTION TRANSMISSION ELECTRON MICROSCOPY;

FERRIC OXIDE; MESOPOROUS SILICA; NANOPARTICLE; SILICON DIOXIDE; SODIUM HYDROXIDE; UNCLASSIFIED DRUG;

ARTICLE; DISPERSION; DISSOLUTION; LOW TEMPERATURE; NANOCASTING; NANOTECHNOLOGY; PARTICLE SIZE; TRANSMISSION ELECTRON MICROSCOPY;

EID: 84855214820     PISSN: 00325910     EISSN: 1873328X     Source Type: Journal    
DOI: 10.1016/j.powtec.2011.10.037     Document Type: Article

References (35)

1. Beek W., Wienk M., Janssen R. Efficient hybrid solar cells from zinc oxide nanoparticles and a conjugated polymer. Advanced Materials 2004, 16(12):1009-1013.
2. Oskam G. Metal oxide nanoparticles: synthesis, characterization and application. Journal Sol-Gel Science Technololgy 2006, 37(3):161-164.
3. Chen J., Xu L., Li W., Gou X. α-Fe2O3 nanotubes in gas sensor and lithium-ion battery applications. Advanced Materials 2005, 17(5):582-586.
4. Xinglong G., et al. Monodisperse hematite porous nanospheres: synthesis, characterization, and applications for gas sensors. Nanotechnol 2008, 19(12):125606.
5. Wu C., Yin P., Zhu X., OuYang C., Xie Y. Synthesis of hematite (α-Fe2O3) nanorods: diameter-size and shape effects on their applications in magnetism, lithium ion battery, and gas sensors. The Journal of Physical Chemistry. B 2006, 110(36):17806-17812.
6. Raming T.P., Winnubst A.J.A., van Kats C.M., Philipse A.P. The synthesis and magnetic properties of nanosized hematite ([alpha]-Fe2O3) particles. Journal of Colloid and Interface Science 2002, 249(2):346-350.
7. Reddy M.V., Yu T., Sow C.H., Shen Z.X., Lim C.T., Subba Rao G.V., et al. α-Fe2O3 nanoflakes as an anode material for Li-ion batteries. Advanced Functional Materials 2007, 17(15):2792-2799.
8. Katsuki H., Komarneni S. Role of α-Fe2O3 morphology on the color of red pigment for porcelain. Journal of the American Ceramic Society 2003, 86(1):183-185.
9. Pailhé N., Wattiaux A., Gaudon M., Demourgues A. Impact of structural features on pigment properties of [alpha]-Fe2O3 haematite. Journal Solid State Chemistry 2008, 181(10):2697-2704.
10. Feng J., Hu X., Yue P.L. Discoloration and mineralization of Orange II using different heterogeneous catalysts containing Fe: a comparative study. Environmental Science and Technology 2004, 38(21):5773-5778.
11. 3 as a highly active heterogeneous Fenton-like catalyst towards the degradation of acid orange 7 and phenol. Applied Catalysis B 2010, 96(1-2):162-168.
12. Turner J.E., Hendewerk M., Parmeter J., Neiman D., Somorjai G.A. The characterization of doped iron oxide electrodes for the photodissociation of water. Journal of the Electrochemical Society 1984, 131(8):1777-1783.
13. Lindgren T., Wang H., Beermann N., Vayssieres L., Hagfeldt A., Lindquist S.-E. Aqueous photoelectrochemistry of hematite nanorod array. Solid Energy Material Solid Cells 2002, 71(2):231-243.
14. Liu X.Q., Tao S.W., Shen Y.S. Preparation and characterization of nanocrystalline [alpha]-Fe2O3 by a sol-gel process. Sensors and Actuators B: Chemical 1997, 40(2-3):161-165.
15. Dong W., Zhu C. Use of ethylene oxide in the sol-gel synthesis of [small alpha]-Fe2O3 nanoparticles from Fe(III) salts. Journal of Materials Chemistry 2002, 12(6):1676-1683.
16. Li Q., Wei Y. Study on preparing monodispersed hematite nanoparticles by microwave-induced hydrolysis of ferric salts solution. Materials Research Bulletin 1998, 33(5):779-782.
17. Wang W., Howe J.Y., Gu B. Structure and morphology evolution of hematite (α-Fe2O3) nanoparticles in forced hydrolysis of ferric chloride. Journal Physical Chemistry C 2008, 112(25):9203-9208.
18. Yener D.O., Giesche H. Synthesis of pure and manganese-, nickel-, and zinc-doped ferrite particles in water-in-oil. Journal of the American Ceramic Society 2001, 84(9):1987.
19. Han L.-H., Liu H., Wei Y. In situ synthesis of hematite nanoparticles using a low-temperature microemulsion method. Powder Technology 2011, 207(1-3):42-46.
20. Zysler R.D., Vasquez-Mansilla M., Arciprete C., Dimitrijewits M., Rodriguez-Sierra D., Saragovi C. Structure and magnetic properties of thermally treated nanohematite. Journal of Magnetism and Magnetic Materials 2001, 224(1):39-48.
21. Fan H., Song B., Liu J., Yang Z., Li Q. Thermal formation mechanism and size control of spherical hematite nanoparticles. Materials Chemistry and Physics 2005, 89(2-3):321-325.
22. Almeida T.P., Fay M., Zhu Y., Brown P.D. Process map for the hydrothermal synthesis of α-Fe2O3 nanorods. Journal of Physical Chemistry C 2009, 113(43):18689-18698.
23. Liu X., Qiu G., Yan A., Wang Z., Li X. Hydrothermal synthesis and characterization of [alpha]-FeOOH and [alpha]-Fe2O3 uniform nanocrystallines. Journal of Alloys and Compounds 2007, 433(1-2):216-220.
24. Zhang H., Wang W., Li H., Meng S., Li D. A strategy to prepare ultrafine dispersed Fe2O3 nanoparticles. Materials Letters 2008, 62(8-9):1230-1233.
25. Ni S., Lin S., Pan Q., Yang F., Huang K., Wang X., et al. Synthesis of core-shell [alpha]-Fe2O3 hollow micro-spheres by a simple two-step process. Journal of Alloys and Compounds 2009, 478(1-2):876-879.
26. Ballem M., Córdoba J., Odén M. Mesoporous silica templated zirconia nanoparticles. Journal of Nanoparticle Research 2011, 13(7):2743-2748.
27. Tsai H.T., Córdoba J.M., Johansson E.M., Ballem M.A., Odén M. Silica SBA-15 template assisted synthesis of ultrasmall and homogeneously sized copper nanoparticles. Journal of Nanoscience and Nanotechnology 2011, 11(4):3493-3498.
28. Ryoo R., Joo S.H., Jun S. Synthesis of highly ordered carbon molecular sieves via template-mediated structural transformation. The Journal of Physical Chemistry. B 1999 Sep 16, 103(37):7743-7746.
29. Sayari A., Han B.H., Yang Y. Simple synthesis route to monodispersed SBA-15 silica rods. Journal of the American Chemical Society 2004 Nov 10, 126(44):14348-14349.
30. Ballem M.A., Cordoba J.M., Oden M. Influence of synthesis temperature on morphology of SBA-16 mesoporous materials with a three-dimensional pore system. Microporous and Mesoporous Materials 2010 Apr 1, 129(1-2):106-111.
31. Brunauer S., Emmett P.H., Teller E. Adsorption of gases in multimolecular layers. Journal of the American Chemical Society 1938, 60:309-319.
32. Kruk M., Jaroniec M., Sayari A. Application of large pore MCM-41 molecular sieves to improve pore size analysis using nitrogen adsorption measurements. Langmuir 1997, 13(23):6267-6273.
33. Broekhoff J.C.P., de Boer J.H. Studies on pore systems in catalysts: IX. Calculation of pore distributions from the adsorption branch of nitrogen sorption isotherms in the case of open cylindrical pores A. Fundamental equations. Journal of Catalysis 1967, 9(1):8-14.
34. Sing K.S.W., Everett D.H., Haul R.A.W., Moscou L., Pierotti R.A., Rouquerol J., et al. Reporting physisorption data for gas solid systems with special reference to the determination of surface-area and porosity (recommendations 1984). Pure and Applied Chemistry 1985, 57(4):603-619.
35. Inoue S., Hanzawa Y., Kaneko K. Prediction of hysteresis disappearance in the adsorption isotherm of N2 on regular mesoporous silica. Langmuir 1998, 14(11):3079-3081.