Heptafluorobutyl chloroformate-based sample preparation protocol for chiral and nonchiral amino acid analysis by gas chromatography

Methods in Molecular Biology

Volumn 828, Issue , 2012, Pages 137-152

  Šimek, Petr ^a   Hušek, Petr ^a   Zahradníčková, Helena ^a  

^a INSTITUTE OF MATHEMATICS   (Czech Republic)

Author keywords

2,3 Dimercapto 1 propanesulfonic acid; Amino acid; Amino acid analysis; Chiral analysis; Derivatization; Enantiomer; Gas chromatography; Heptafluorobutyl chloroformate; Mass spectrometry; Plasma; Serum

Indexed keywords

AMINO ACID; FLUOROCARBON; FORMIC ACID DERIVATIVE; HEPTAFLUOROBUTYL CHLOROFORMATE;

ANALYSIS; ANIMAL; ARTICLE; CHEMISTRY; GAS CHROMATOGRAPHY; HUMAN; MASS FRAGMENTOGRAPHY; METHODOLOGY; STANDARD; STEREOISOMERISM;

AMINO ACIDS; ANALYTIC SAMPLE PREPARATION METHODS; ANIMALS; CHROMATOGRAPHY, GAS; FLUOROCARBONS; FORMATES; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; HUMANS; REFERENCE STANDARDS; STEREOISOMERISM;

EID: 84555187417     PISSN: 10643745     EISSN: None     Source Type: Book Series    
DOI: 10.1007/978-1-61779-445-2_13     Document Type: Article

References (9)

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9. Zahradní?kov H, Huek P and Åimek P (2009) GC separation of amino acid enantiomers via derivatization with heptafl uorobutyl chloroformate and Chirasil-L-Val column. J Sep Sci 25:3919-3924