GC separation of amino acid enantiomers via derivatization with heptafluorobutyl chloroformate and Chirasil-L-Val column

Journal of Separation Science

Volumn 32, Issue 22, 2009, Pages 3919-3924

  Ková, Helena Zahradníč ^a   Hušek, Petr ^a   Šimek, Petr ^a  

^a INSTITUTE OF MATHEMATICS   (Czech Republic)

Author keywords

Chiral separation; D,L AAs; Derivatization; GC; HFBCF

Indexed keywords

AMINO ACID ENANTIOMERS; CAPILLARY COLUMNS; CHIRAL SEPARATIONS; CHLOROFORMATES; DERIVATIZATION REAGENT; DERIVATIZATIONS; ELUTION TEMPERATURE; ENANTIOSEPARATIONS; GC SEPARATIONS; INTERNAL STANDARDS; ONE-STEP REACTIONS; ORGANIC MEDIUM; PROTEINOGENIC; SEPARATION PROPERTY;

AMINO ACIDS; CHIRALITY; ENANTIOMERS; ORGANIC ACIDS;

SEPARATION;

4 FLUOROPHENYLALANINE; ALANINE; AMINO ACID; ARGININE; ASPARAGINE; ASPARTIC ACID; CYSTEINE; CYSTINE; FORMIC ACID; GLUTAMIC ACID; GLUTAMINE; GLYCINE; HEPTAFLUOROBUTYL CHLOROFORMATE; HISTIDINE; ISOLEUCINE; LEUCINE; LYSINE; METHIONINE; ORGANIC COMPOUND; ORNITHINE; PHENYLALANINE; PROLINE; SERINE; THREONINE; TRYPTOPHAN; TYROSINE; UNCLASSIFIED DRUG; VALINE;

AQUEOUS SOLUTION; ARTICLE; CAPILLARY CHROMATOGRAPHY; CHIRALITY; CONTROLLED STUDY; DERIVATIZATION; ELUTION; ENANTIOMER; EXTRACTION; GAS CHROMATOGRAPHY; PRIORITY JOURNAL; SEPARATION TECHNIQUE; STANDARD; TEMPERATURE;

CHROMATOGRAPHY, GAS; FLUOROCARBONS; FORMIC ACIDS; LIMIT OF DETECTION; REPRODUCIBILITY OF RESULTS;

EID: 76649130546     PISSN: 16159306     EISSN: 16159314     Source Type: Journal    
DOI: 10.1002/jssc.200900400     Document Type: Article

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