The use of 1H-31P GHMBC and covariance NMR to unambiguously determine phosphate ester linkages in complex polysaccharide mixtures

Journal of Biomolecular NMR

Volumn 51, Issue 3, 2011, Pages 357-367

  Zartler, Edward R ^a   Martin, Gary E ^a  

^a MERCK RESEARCH LABORATORIES   (United States)

Author keywords

Carbon phosphorus spectrum; Generalized indirect covariance; Multiple bond coupling; Phosphorus; Unsymmetrical indirect covariance

Indexed keywords

CARBON; ORGANOPHOSPHATE; PHOSPHORUS; POLYSACCHARIDE;

ARTICLE; CALCULATION; CARBON NUCLEAR MAGNETIC RESONANCE; COVARIANCE; GRADIENT HETERONUCLEAR MULTIPLE BOND CORRELATION; HETERONUCLEAR MULTIPLE BOND CORRELATION; NUCLEAR MAGNETIC RESONANCE; PHOSPHORUS NUCLEAR MAGNETIC RESONANCE; PRIORITY JOURNAL; PROTON NUCLEAR MAGNETIC RESONANCE; SIGNAL NOISE RATIO; CHEMISTRY; METHODOLOGY;

NUCLEAR MAGNETIC RESONANCE, BIOMOLECULAR; PHOSPHORIC ACID ESTERS; POLYSACCHARIDES;

EID: 80755132303     PISSN: 09252738     EISSN: 15735001     Source Type: Journal    
DOI: 10.1007/s10858-011-9563-8     Document Type: Article

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