Pressure-induced two-step spin transition with structural symmetry breaking: X-ray diffraction, magnetic, and Raman studies

Physical Review B - Condensed Matter and Materials Physics

Volumn 84, Issue 14, 2011, Pages

  Shepherd, Helena J ^a,b   Bonnet, Sylvestre ^c   Guionneau, Philippe ^b   Bedoui, Salma ^a   Garbarino, Gaston ^d   Nicolazzi, William ^a   Bousseksou, Azzedine ^a   Molnár, Gábor ^a  

^a LCC LABORATOIRE DE CHIMIE DE COORDINATION   (France)

^b UNIVERSITÉ DE BORDEAUX   (France)

^c LEIDEN UNIVERSITY   (Netherlands)

^d EUROPEAN SYNCHROTRON RADIATION FACILITY   (France)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 80155211251     PISSN: 10980121     EISSN: 1550235X     Source Type: Journal    
DOI: 10.1103/PhysRevB.84.144107     Document Type: Article

References (60)

1. Y. Garcia, O. Kahn, L. Rabardel, B. Chansou, L. Salmon, and J.-P. Tuchagues, Inorg. Chem. INOCAJ 0020-1669 10.1021/ic990511q 38, 4663 (1999).
2. J. A. Real, H. Bolvin, A. Bousseksou, A. Dworkin, O. Kahn, F. Varret, and J. Zarembowitch, J. Am. Chem. Soc. JACSAT 0002-7863 10.1021/ja00038a031 114, 4650 (1992).
3. J. A. Real, A. B. Gaspar, M. C. Muñoz, P. Gütlich, V. Ksenofontov, and H. Spiering, Top. Curr. Chem. 233, 167 (2004).
4. V. Ksenofontov, A. B. Gaspar, V. Niel, S. Reiman, J. A. Real, and P. Gütlich, Chem. Eur. J. CEUJED 0947-6539 10.1002/chem.200305275 10, 1291 (2004).
5. S. M. Neville, B. A. Leita, G. J. Halder, C. J. Kepert, B. Moubaraki, J.-F. Létard, and K. S. Murray, Chem. Eur. J. CEUJED 0947-6539 10.1002/chem.200800886 14, 10123 (2008).
6. G. J. Halder, K. W. Chapman, S. M. Neville, B. Moubaraki, K. S. Murray, J.-F. Létard, and C. J. Kepert, J. Am. Chem. Soc. JACSAT 0002-7863 10.1021/ja8068038 130, 17552 (2008).
7. M. Nihei, M. Ui, M. Yokota, L. Han, A. Maeda, H. Kishida, H. Okamoto, and H. Oshio, Angew. Chem. Int. Ed. 1433-7851 10.1002/anie.200502216 44, 6484 (2005). (Pubitemid 41509130)
8. A. Kaiba, H. J. Shepherd, D. Fedaoui, P. Rosa, A. E. Goeta, N. Rebbani, J.-F. Létard, and P. Guionneau, Dalton Trans. 1477-9226 10.1039/b914841h 39, 2910 (2010).
9. D. Chernyshov, M. Hostettler, K. W. Törnroos, and H.-B. Bürgi, Angew. Chem. Int. Ed. 1433-7851 10.1002/anie.200351834 42, 3825 (2003). (Pubitemid 37051533)
10. N. Bréfuel, E. Collet, H. Watanabe, M. Kojima, N. Matsumoto, L. Toupet, K. Tanaka, and J.-P. Tuchagues, Chem. Eur. J. CEUJED 0947-6539 10.1002/chem.201001264 16, 14060 (2010).
11. K. Nakano, S. Kawata, K. Yoneda, A. Fuyuhiro, T. Yagi, S. Nasu, S. Morimoto, and S. Kaizaki, Chem. Commun. 10.1039/b411190g 2892 (2004). (Pubitemid 40064839)
12. K. W. Törnroos, M. Hostettler, D. Chernyshov, B. Vangdal, and H.-B. Bürgi, Chem. Eur. J. CEUJED 0947-6539 10.1002/chem.200600547 12, 6207 (2006). (Pubitemid 44325277)
13. M. Yamada, H. Hagiwara, H. Torigoe, N. Matsumoto, M. Kojima, F. Dahan, J.-P. Tuchagues, N. Re, and S. Iijima, Chem. Eur. J. CEUJED 0947-6539 10.1002/chem.200500972 12, 4536 (2006). (Pubitemid 43898301)
14. N. Bréfuel, H. Watanabe, L. Toupet, J. Come, N. Matsumoto, E. Collet, K. Tanaka, and J.-P. Tuchagues, Angew. Chem. Int. Ed. 1433-7851 10.1002/anie.200904190 48, 9304 (2009).
15. M. Griffin, S. Shakespeare, H. J. Shepherd, C. J. Harding, J.-F. Létard, C. Desplanches, A. E. Goeta, J. A. K. Howard, A. K. Powell, V. Mereacre, Y. Garcia, A. D. Naik, H. Müller-Bunz, and G. G. Morgan, Angew. Chem. Int. Ed. 1433-7851 10.1002/anie.201005545 50, 896 (2011).
16. M. Nihei, H. Tahira, N. Takahashi, Y. Otake, Y. Yamamura, Kazuya Saito, and H. Oshio, J. Am. Chem. Soc. JACSAT 0002-7863 10.1021/ja910122r 132, 3553 (2010).
17. M. Buron-Le Cointe, N. Ould Moussa, E. Trzop, A. Moréac, G. Molnár, L. Toupet, A. Bousseksou, J.-F. Létard, and G. S. Matouzenko, Phys. Rev. B PLRBAQ 1098-0121 10.1103/PhysRevB.82.214106 82, 214106 (2010).
18. S. Bonnet, M. A. Siegler, J. Sánchez Costa, G. Molnár, A. Bousseksou, A. L. Spek, P. Gamez, and J. Reedijk, Chem. Commun. 10.1039/b811746b 5619 (2008).
19. S. Bonnet, G. Molnár, J. Sánchez Costa, M. A. Siegler, A. L. Spek, A. Bousseksou, W.-T. Fu, P. Gamez, and J. Reedijk, Chem. Mater. CMATEX 0897-4756 10.1021/cm803414q 21, 1123 (2009).
20. T. Sato, K. Nishi, S. Iijima, M. Kojima, and N. Matsumoto, Inorg. Chem. INOCAJ 0020-1669 10.1021/ic9006197 48, 7211 (2009).
21. A. Bousseksou, F. Varret, and J. Nasser, J. Phys. I (France) 1155-4304 10.1051/jp1:1993191 3, 1463 (1993).
22. V. Ksenofontov, A. B. Gaspar, and P. Gütlich, Top. Curr. Chem. 0340-1022 10.1007/b95421 235, 23 (2004).
23. C. P. Köhler, R. Jakobi, E. Meissner, L. Wiehl, H. Spiering, and P. Gütlich, J. Phys. Chem. Solids JPCSAW 0022-3697 10.1016/0022-3697(90)90052- H 51, 239 (1990).
24. P. Gütlich, A. Hauser, and H. Spiering, Angew. Chem. Int. Ed. Engl. 0570-0833 10.1002/anie.199420241 33, 2024 (1994).
25. P. Guionneau, M. Marchivie, G. Bravic, J.-F. Létard, and D. Chasseau, Top. Curr. Chem. 234, 97 (2004).
26. P. Gütlich, A. B. Gaspar, Y. Garcia, and V. Ksenofontov, C. R. Chimie 1631-0748 10.1016/j.crci.2006.09.011 10, 21 (2007).
27. P. Guionneau, C. Brigouleix, Y. Barrans, A. E. Goeta, J.-F. Létard, J. A. K. Howard, J. Gaultier, and D. Chasseau, C. R. Acad. Sci. IIC 4, 161 (2001).
28. T. Granier, B. Gallois, J. Gaultier, J. A. Real, and J. Zarembowitch, Inorg. Chem. INOCAJ 0020-1669 10.1021/ic00075a058 32, 5305 (1993).
29. P. Guionneau, M. Marchivie, Y. Garcia, J. A. K. Howard, and D. Chasseau, Phys. Rev. B PLRBAQ 1098-0121 10.1103/PhysRevB.72.214408 72, 214408 (2005). (Pubitemid 43033206)
30. V. Legrand, F. Le Gac, P. Guionneau, and J.-F. Létard, J. Appl. Crystallogr. 0021-8898 10.1107/S0021889808006481 41, 637 (2008). (Pubitemid 351693894)
31. S. Bedoui, G. Molnár, S. Bonnet, C. Quintero, H. J. Shepherd, W. Nicolazzi, L. Salmon, and A. Bousseksou, Chem. Phys. Lett. CHPLBC 0009-2614 10.1016/j.cplett.2010.09.027 499, 94 (2010).
32. See Supplemental Material at http://link.aps.org/supplemental/10.1103/ PhysRevB.84.144107 for additional magnetic, crystallographic and Raman spectral data as well as for details on the Ising-like model with three sublattices.
33. Detailed structural analysis and cell parameter evolution as a function of temperature are given in the electronic supplementary material of S. Bonnet, M. A. Siegler, J. Sánchez Costa, G. Molnár, A. Bousseksou, A. L. Spek, P. Gamez, and J. Reedijk, Chem. Commun. 10.1039/b811746b 5619 (2008).
34. R. Boehler and K. De Hantsetters, High Press. Res. 0895-7959 10.1080/08957950412331323924 24, 391 (2004). (Pubitemid 40079237)
35. G. J. Piermarini, S. Block, J. D. Barnett, and R. A. Foremann, J. Appl. Phys. JAPIAU 0021-8979 10.1063/1.321957 46, 2774 (1975).
36. CrysAlisPro, Oxford Diffraction Ltd., Version 1.171.33.66.
37. G. M. Sheldrick, Acta Crystallogr. A64, 112 (2008).
38. O. V. Dolomanov, L. J. Bourhis, R. J. Gildea, J. A. K. Howard, and H. Puschmann, J. Appl. Crystallogr. 0021-8898 10.1107/S0021889808042726 42, 339 (2009).
39. R. J. Angel, J. Appl. Crystallogr. 0021-8898 10.1107/S0021889804005229 37, 486, (2004).
40. A. Katrusiak, Acta Crystallogr. A64, 135 (2008).
41. G. Molnár, T. Guillon, N. Ould Moussa, L. Rechignat, T. Kitazawa, M. Nardone, and A. Bousseksou, Chem. Phys. Lett. CHPLBC 0009-2614 10.1016/j.cplett.2006.03.053 423, 152 (2006). (Pubitemid 44287795)
42. A. Eiling and J. S. Schilling, J. Phys. F 0305-4608 10.1088/0305-4608/11/ 3/010 11, 623 (1981).
43. A. Bousseksou, G. Molnár, and G. Matouzenko, Eur. J. Inorg. Chem. 10.1002/ejic.200400571 4353 (2004).
44. V. Ksenofontov, H. Spiering, A. Schreiner, G. Levchenko, H. A. Goodwin and P. Gütlich, J. Phys. Chem. Solids JPCSAW 0022-3697 10.1016/S0022- 3697(98)00259-5 60, 393 (1999).
45. E. König, G. Ritter, J. Waigel, and H. A. Goodwin, J. Chem. Phys. JCPSA6 0021-9606 10.1063/1.449209 83, 3055 (1985).
46. V. Ksenofontov, G. Levchenko, H. Spiering, P. Gütlich, J.-F. Létard, Y. Bouhedja, and O. Kahn, Chem. Phys. Lett. CHPLBC 0009-2614 10.1016/S0009-2614(98)00901-4 294, 545 (1998).
47. P. Gütlich, V. Ksenofontov, and A. B. Gaspar, Coord. Chem. Rev. 0010-8545 10.1016/j.ccr.2005.01.022 249, 1811 (2005). (Pubitemid 41121956)
48. E. König, G. Ritter, W. Irler, and H. A. Goodwin, J. Am. Chem. Soc. JACSAT 0002-7863 10.1021/ja00534a021 102, 4681 (1980).
49. A. Bousseksou, J. Nasser, J. Linares, K. Boukheddaden, and F. Varret, J. Phys. I (France) 1155-4304 10.1051/jp1:1992217 2, 1381 (1992).
50. M. Nishino, K. Boukheddaden, S. Miyashita, and F. Varret, Phys. Rev. B 1098-0121 10.1103/PhysRevB.68.224402 68, 224402 (2003).
51. B. Hôo, K. Boukheddaden, and F. Varret, Eur. Phys. J. B EPJBFY 1434-6028 10.1007/s100510070124 17, 449 (2000).
52. K. Boukheddaden, J. Linares, R. Tamasa, and C. Chong, J. Phys.: Cond. Matter. 0953-8984 10.1088/0953-8984/19/10/106201 19, 106201 (2006).
53. K. Boukheddaden, S. Miyashita, and M. Nishino, Phys. Rev. B 1098-0121 10.1103/PhysRevB.75.094112 75, 094112 (2007).
54. J. A. Nassa, K. Boukheddaden, and J. Linares, Eur. Phys. J. B EPJBFY 1434-6028 10.1140/epjb/e2004-00184-y 39, 219 (2004).
55. W. Nicolazzi, S. Pillet, and C. Lecomte, Phys. Rev. B 1098-0121 10.1103/PhysRevB.78.174401 78, 174401 (2008).
56. H. Spiering, K. Boukheddaden, J. Linares, and F. Varret, Phys. Rev. B 1098-0121 10.1103/PhysRevB.70.184106 70, 184106 (2004). (Pubitemid 40123235)
57. T. Kohlhaas, H. Spiering, and P. Gütlich, Z. Phys. B ZPBBDJ 0722-3277 10.1007/s002570050311 102, 455 (1997).
58. H. Spiering, T. Kohlhaas, H. Romstedt, A. Hauser, C. Bruns-Yilmaz, J. Kusz, and P. Gütlich, Coord. Chem. Rev. 0010-8545 10.1016/S0010-8545(99) 00109-5 190-192, 629 (1999).
59. D. Chernyshov, H.-B. Bürgi, M. Hostettler, and K. W. Törnroos, Phys. Rev. B PLRBAQ 1098-0121 10.1103/PhysRevB.70.094116 70, 094116 (2004).
60. A. Das and B. Ghosh, J. Phys. C JPSOAW 0022-3719 10.1088/0022-3719/16/10/ 011 16, 1799 (1983).