Residue dynamics studies of aluminum phosphide and magnesium phosphide in stored rice utilizing a sulfuric acid-toluene extraction coupled with gas chromatography analysis

Cereal Chemistry

Volumn 88, Issue 5, 2011, Pages 441-444

  Zhang, Fengzu ^a   Jiang, Yaping ^a   Wang, Lei ^a   Kang, Shu ^a   Pan, Canping ^a  

^a CHINA AGRICULTURAL UNIVERSITY   (China)

Author keywords

[No Author keywords available]

Indexed keywords

ALUMINUM COMPOUNDS; DYNAMICS; GAS CHROMATOGRAPHY; MAGNESIUM COMPOUNDS; SULFUR DETERMINATION; SULFURIC ACID; TOLUENE;

CALIBRATION CURVES; CORRELATION COEFFICIENT; DYNAMIC STUDIES; FLAME PHOTOMETRIC DETECTORS; GAS CHROMATOGRAPHY ANALYSIS; LABORATORY PRACTICES; LIMIT OF DETECTION; LINEAR RELATIONSHIPS; ORGANIC LAYERS; RICE SAMPLES;

PHOSPHORUS COMPOUNDS;

EID: 80054990181     PISSN: 00090352     EISSN: None     Source Type: Journal    
DOI: 10.1094/CCHEM-06-10-0093     Document Type: Article

References (15)

1. Berck, B., Westlake, W. E., and Gunther, F. A. 1970. Microdetermination of phosphine by gas-liquid chromatography with microcoulometric, thermionic, and flame photometric detection. J. Agric. Food Chem. 18:143-147.
2. Banks H. J. 1986. Sorption and desorption of fumigants on grains: Mathematical descriptions. Pages 179-194 in: Pesticides and Humid Tropical Grain Storage Systems. B. R. Champ and E. Highley, eds. ACIAR Proceedings: Canberra, Australia.
3. Bruce, R. B., Robbins, A. J., and Tuft, T. O. 1962. Phosphine residues from Phostoxin treated grain. J. Agric. Food Chem. 10:18-21.
4. Calzolai, S. G. 1990. Problema dei residui nella disinfestazione dei cereali. Tec. Molitoria 41:272-275.
5. Corley, J., Kahl, J., Burkhart, D., Diaz, E., and Möller, G. 1998. Rapid zinc phosphide trace analysis in agricultural commodities by phosphine generation, toluene trapping, and gas chromatography. J. Agric. Food Chem. 46:999-1004. (Pubitemid 128488104)
6. Food and Agricultural Organization (FAO) and World Health Organization (WHO). 1983. Codex alimentarius: Maximum limits for pesticide residues, 2nd Ed., vol. 13. FAO/WHO: Rome.
7. Longobardi, F., Pascale, M., Silvestri, M., and Visconti, A. 2008. Rapid method for determination of phosphine residues in wheat. Food Anal. Methods 1:220-225.
8. Mauldin, R. E., Goldade, D. A., Engeman, R. M., Goodall, M. J., Carver, R. K., and Johnson, J. J. 1996. Determination of zinc phosphide residues in the California ground squirrel (Spermophilus beecheyi) by gas chromatography flame photometric detection. J. Agric. Food Chem. 44:189-194. (Pubitemid 126458563)
9. Ministry of Agriculture of the People's Republic of China. 2004. Guideline on Pesticide Residue Trials. NY/T 788-2004.
10. Nowicki, T. W. 1978. Gas-liquid chromatography and flame photometric detection of phosphine in wheat. J. AOAC Int. 61:829-836. (Pubitemid 9057390)
11. Rangaswamy, J. R. 1984. Simple spectrophotometric method for determination of phosphine residues in wheat. J. AOAC Int. 67:117-122. (Pubitemid 16223972)
12. Ren, Y. L., and Desmarchelier, J. M. 1998. Release of fumigant residues from grain by microwave irradiation. J. AOAC Int. 81:673-678. (Pubitemid 128441681)
13. Shang, Y. D. 1996. Determination of phosphide residue in grain with molybdenum blues colorimetry. Grain Storage 2(25):41-43.
14. Visconti, A., Pascale, M., Longobardi, F., Ranieri, R., and Silvestri, M. 2006. European patent application 06425533.4-1524.
15. Working Party on Pesticide Residues. 1998. Annual Report of the Working Party on Pesticide Residues. MAFF: London.