On the relationship between band broadening and the particle-size distribution of the packing material in liquid chromatography: Theory and practice

Journal of Chromatography A

Volumn 1218, Issue 45, 2011, Pages 8209-8221

  Gritti, Fabrice ^a   Farkas, Tivadar ^a   Heng, Josuah ^a   Guiochon, Georges ^a  

^a UNIVERSITY OF TENNESSEE   (United States)

Author keywords

Column efficiency; Column technology; Luna C18(2); Mass transfer kinetics; Particle size distribution

Indexed keywords

ANALYTES; BAND-BROADENING; BEST MODEL; COLUMN EFFICIENCY; COLUMN TECHNOLOGY; COULTER COUNTERS; EDDY DIFFUSIONS; EFFECTIVE DIFFUSION COEFFICIENTS; EXTERNAL SURFACES; FINE PARTICLES; LARGE PARTICLES; LONGITUDINAL DIFFUSIONS; LUNA-C18(2); MASS TRANSFER KINETICS; NUMERICAL INTEGRATIONS; PACKED COLUMN; PACKING MATERIALS; PARTICLE MIXTURES; PEAK PARKING; PEAK PROFILES; SMALL PARTICLES; SOLID-LIQUID MASS TRANSFER; THEORY AND PRACTICE; TWO-MATERIALS; VAN DEEMTER EQUATION; WALL EFFECTS;

ACETONITRILE; COLUMN CHROMATOGRAPHY; DIFFUSION; EFFICIENCY; LIQUID CHROMATOGRAPHY; MIXTURES; PARTICLE SIZE; PARTICLE SIZE ANALYSIS; SIZE DISTRIBUTION;

LIQUIDS;

ACETONITRILE; WATER;

ARTICLE; DIFFUSION; DIFFUSION COEFFICIENT; DISPERSION; LIQUID CHROMATOGRAPHY; MATERIALS; PACKING MATERIAL; PARTICLE SIZE; PRIORITY JOURNAL; THEORY;

CHROMATOGRAPHY, LIQUID; DIFFUSION; KINETICS; LINEAR MODELS; MODELS, CHEMICAL; NAPHTHALENES; PARTICLE SIZE; PERMEABILITY; POROSITY; URACIL;

EID: 80054714624     PISSN: 00219673     EISSN: 18733778     Source Type: Journal    
DOI: 10.1016/j.chroma.2011.09.034     Document Type: Article

References (62)

1. Halasz I., Naefe M. Anal. Chem 1972, 44:76.
2. Done J., Knox J. J. Chromatogr. Sci. 1972, 10:606.
3. Endele R., Halasz I., Unger K. J. Chromatogr. 1974, 99:377.
4. Dewaele C., Verzele M. J. Chromatogr. 1983, 260:13.
5. Billen J., Guillarme D., Rudaz S., Veuthey J.-L., Ritchie H., Grady B., Desmet G. J. Chromatogr. A 2007, 1161:224.
6. Kirkland J.J., Langlois T.J., DeStefano J. J. Am. Lab. 2007, 39(8):18.
7. Schuster S.A., Wagner B., Boyes B., Kirkland J. J. Chromatogr. Sci. 2010, 48:566.
8. Gritti F., Guiochon G. J. Chromatogr. A 2007, 1157:289.
9. Cavazzini A., Gritti F., Kaczmarski K., Marchetti N., Guiochon G. Anal. Chem. 2007, 79:5972.
10. Marchetti N., Cavazzini A., Gritti F., Guiochon G. J. Chromatogr. A 2007, 1163:203.
11. Gritti F., Leonardis I., Shock D., Stevenson P., Shalliker A., Guiochon G. J. Chromatogr. A 2010, 1217:1589.
12. Gritti F., Guiochon G. J. Chromatogr. A 2010, 1217:5069.
13. Gritti F., Guiochon G. Chem. Eng. Sci. 2010, 65:6310.
14. Gritti F., Guiochon G. J. Chromatogr. A 2010, 1217:1604.
15. Gritti F., Sanchez C.A., Farkas T., Guiochon G. J. Chromatogr. A 2010, 1217:3000.
16. Gritti F., Leonardis I., Abia J., Guiochon G. J. Chromatogr. A 2010, 1217:3819.
17. Olah E., Fekete S., Fekete J., Ganzler K. J. Chromatogr. A 2010, 1217:3642.
18. Gritti F., Guiochon G. J. Chromatogr. A 2011, 1218:907.
19. Gritti F., Guiochon G. Chem. Eng. Sci 2010, 65:6327.
20. Gritti F., Guiochon G. J. Chromatogr. A 2010, 1217:8167.
21. McCalley D.V. J. Chromatogr. A 2010, 1217:4561.
22. Omamogho J., Glennon J., Hanrahan J., Tobin J. J. Chromatogr. A 2011, 1218:1942.
23. J.W. Jorgenson, L.E. Blue, E. Franklin, R.A. Lieberman, in: Presented at the Pittcon 2010 Conference, Orlando, FL, February 28-March 5, 2010 Paper 350-3, 2010.
24. Gritti F., Guiochon G. J. Chromatogr. A 2011, 1218:1592.
25. Gritti F., Guiochon G. J. Chromatogr. A 2011, 1218:1915.
26. Gritti F., Guiochon G. J. Chromatogr. A 2010, 1217:5137.
27. Cabooter D., Fanigliulo A., Bellazzi G., Allieri B., Rottigni A., Desmet G. J. Chromatogr. A 2010, 1217:7074.
28. Daneyko A., Höltzel A., Tallarek S.K.U. Anal. Chem. 2011, 83:3903.
29. Giddings J.C. Dynamics of Chromatography 1960, Marcel Dekker, New York, NY.
30. Gritti F., Guiochon G. J. Chromatogr. A 2007, 1166:30.
31. Yew B.G., Ureta J., Shalliker R.A., Drumm E.C., Guiochon G. AIChE J. 2003, 49:642.
32. Gritti F., Guiochon G. J. Chromatogr. A 2011, 1218:4452.
33. G. Guiochon, A. Felinger, A.M. Katti, D.G. Shirazi, Fundamentals of Preparative and Nonlinear Chromatography, Elsevier, Amsterdam, The Netherlands, 2006.
34. Lightfoot E., Gibbs S., Karrila S. Chem. Eng. J. 1987, 36:B29.
35. Sircar K. Chem. Eng. Sci. 1974, 29:863.
36. Schlichting H. Boundary-layer Theory 1979, McGraw-Hill, Inc., New York.
37. F. Gritti, G. Guiochon, J. Chromatogr. A (2011) doi:10.1016/j.chroma.2011.04.058.
38. Kucera E. J. Chromatogr. 1965, 19:237.
39. Dougharty N. AIChE J. 1972, 18:657.
40. Gritti F., Guiochon G. Anal. Chem. 2006, 78:5329.
41. Gritti F., Guiochon G. J. Chromatogr. A 2011, 1218:3476.
42. Gritti F., Guiochon G. Chem. Eng. Sci. 2011, 66:3773.
43. Deridder S., Desmet G. J. Chromatogr. A 2011, 1218:46.
44. Gritti F., Guiochon G. AIChE J. 2011, 57:346.
45. Gritti F., Guiochon G. AIChE J. 2011, 57:333.
46. Gritti F., Guiochon G. AIChE J. 2010, 56:1495.
47. Khirevich S., Daneyko A., Höltzel A., Seidel-Morgenstern A., Tallarek U. J. Chromatogr. A 2010, 1217:4713.
48. Gritti F., Guiochon G. Anal. Chem. 2007, 79:3188.
49. Knox J.H., McLaren L. Anal. Chem. 1964, 36:1477.
50. Knox J., Scott H. J. Chromatogr. 1983, 282:297.
51. Gritti F., Guiochon G. Chem. Eng. Sci. 2006, 61:7636.
52. Miyabe K., Ando N., Guiochon G. J. Chromatogr. A 2009, 1216:4377.
53. Miyabe K., Matsumoto Y., Guiochon G. Anal. Chem. 2010, 6:3859.
54. Ludlum D., Warner R., Smith H. J. Phys. Chem. 1962, 66:1540.
55. Dunlop P., Pepela C., Steel B. J. Am. Chem. Soc. 1970, 92:6743.
56. Li J., Carr P. Anal. Chem. 1997, 69:2530.
57. Li J., Carr P. Anal. Chem. 1997, 69:2550.
58. F. Gritti, G. Guiochon, Chem. Eng. Sci. 66 (2011) 6168.
59. Mitzithras A., Coveney F., Strange J. J. Mol. Liq. 1992, 260:273.
60. Renkin E. J. Gen. Physiol. 1954, 38:225.
61. Brenner H., Gaydos L. J. Colloid Interface Sci. 1977, 58:312.
62. Gritti F., Guiochon G. J. Chromatogr. A 2010, 1217:6350.