Design and performance of a high pressure insert for use in a standard magic angle spinning NMR probe

Journal of Magnetic Resonance

Volumn 183, Issue 2, 2006, Pages 178-182

  Deuchande, Teresa ^a   Breton, Olivier ^b   Haedelt, Josefin ^b   Hughes, Eric ^b  

^a CBQF CENTRO DE BIOTECNOLOGIA E QUÍMICA FINA LABORATÓRIO ASSOCIADO   (Portugal)

^b NESTLÉ RESEARCH CENTER   (Switzerland)

Author keywords

Gas; High pressure; MAS; Nitrogen; Nitrous oxide; NMR

Indexed keywords

HIGH PRESSURE EFFECTS; MAGNETIC PERMEABILITY; NITROGEN; NITROGEN OXIDES; POLYETHER ETHER KETONES; ROTORS;

COMPLEX FOOD MATERIALS; GAS LOADING CHAMBER; HIGH PRESSURE; MAS; NITROUS OXIDE;

NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY;

ARTICLE; CHEMISTRY; EQUIPMENT; EQUIPMENT DESIGN; GAS; INSTRUMENTATION; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; PRESSURE; REPRODUCIBILITY; SENSITIVITY AND SPECIFICITY; SPIN LABELING; TRANSDUCER;

EQUIPMENT DESIGN; EQUIPMENT FAILURE ANALYSIS; GASES; MAGNETIC RESONANCE SPECTROSCOPY; PRESSURE; REPRODUCIBILITY OF RESULTS; SENSITIVITY AND SPECIFICITY; SPIN LABELS; TRANSDUCERS;

EID: 33750938488     PISSN: 10907807     EISSN: 10960856     Source Type: Journal    
DOI: 10.1016/j.jmr.2006.08.007     Document Type: Article

References (9)

1. Andrew E.R., Bradbury A., and Eades R.G. Removal of dipolar broadening of nuclear magnetic resonance spectra of solids by specimen rotation. Nature 183 (1959) 1802-1803
2. Lowe I.J. Free induction decays of rotating solids. Phys. Rev. Lett. 2 (1959) 285-287
3. Schaefer J., and Stejskal E.O. Carbon-13 nuclear magnetic resonance of polymers spinning at the magic angle. J. Am. Chem. Soc. 98 (1976) 1031-1032
4. Miyoshi T., Takegoshi K., and Terao T. A simple method for 13C CPMAS NMR measurements under high gas pressures. J. Magn. Reson. 125 (1997) 383-384
5. Ehrhardt M.R., Flynn P.F., and Wand A.J. Preparation of encapsulated proteins dissolved in low viscosity fluids. J. Biomol. NMR 14 (1999) 75-78
6. Flynn P.F. Multidimensional multinuclear solution NMR studies of encapsulated macromolecules. Prog. Nucl. Mag. Res. Sp. 45 (2004) 31-51
7. Wallen S.L., Schoenbachler L.K., Dawson E.D., and Blatchford M.A. A polymer NMR cell for the study of high-pressure and supercritical fluid solutions. Anal. Chem. 72 (2000) 4230-4234
8. Yonker C.R., and Lineham J.C. The use of supercritical fluids as solvents for NMR spectroscopy. Prog. Nucl. Mag. Res. Sp. 47 (2005) 95-109
9. Martin G.J., Martin M.L., and Gouesnard J.P. 15N NMR Spectroscopy (1981), Springer-Verlag, New York