An inexpensive electrodeposition device and its use in a quantitative analysis laboratory exercise

Journal of Chemical Education

Volumn 88, Issue 10, 2011, Pages 1428-1430

  Parker, Richard H ^a  

^a LAGRANGE COLLEGE   (United States)

Author keywords

Analytical chemistry; Electrochemistry; Electrolytic galvanic cells potentials; Gravimetric analysis; Hands on learning manipulatives; High school introductory chemistry; Instrumental methods; Laboratory instruction; Second year undergraduate

Indexed keywords

EID: 80052857436     PISSN: 00219584     EISSN: None     Source Type: Journal    
DOI: 10.1021/ed101202t     Document Type: Article

References (15)

1. (a) Ayres, G. H.; Quantitative Chemical Analysis, 2nd ed.; Harper & Row: New York, 1968; pp 652-654.
2. (b) Day, R A.; Underwood, A. L. Laboratory Manual Quantitative Analysis, 6th ed.; Prentice Hall: Engle-wood Cliffs, NJ, 1991; p 149.
3. A solution of this type for electrolysis is described in Dale, J. M.; Banks, C. V. Nickel. In Treatise on Analytical Chemistry, Part II; Kolthoff, I. M.; Elving, P. J.; Sandell, E. B., Eds.; Interscience Publishers: New York, 1962; Vol. 2; p 408.
4. Information regarding the construction of other electrochemical devices and electrodeposition of both copper and nickel can be found in the following articles: (a) King, D.; Friend, J.; Kariuki, J. J. Chem. Educ. 2010, 87, 507 and references therein.
5. (b) Elving, P. J.; Hayes, J. R.; Mellon, M. G. J. Chem. Educ. 1953, 30, 254.
6. (c) Anderson, G. E. J. Chem. Educ. 1996, 73, A173.
7. (d) Manjkow, J.; Levine, D. J. Chem. Educ. 1986, 63, 809.
8. (a) Kern, E. F.; Fabian, F. G. Sch. Mines Q. 1907, 29, 342.
9. (b) Laitinen, H. A.; Chemical Analysis; Mc GrawHill: New York, 1960; p 248.
10. Barrett, E. C. H. Electrodeposition of Nickel. U.S. Patent 3, 671, 409, June 20, 1972.
11. (a) Hargis, L. G. Analytical Chemistry, Principles and Techniques; Prentice Hall: Englewood Cliffs, NJ, 1988; p 752.
12. Mendham, J.; Denney, R. C.; Barnes, J. D.; Thomas, M. Vogel's Textbook of (Quantitative Chemical Analysis, 6th ed.;, Pearson Education Limited: Essex, England, 2000; p 470.
13. Harris, D. C.; Quantitative Chemical Analysis, 7th ed.; W.H. Freeman and Company: New York, 2007; pp 60-61.
14. Miller, J. N.; Miller, J. C.; Statistics and Chemometrics for Analytical Chemistry, 4th ed.; Prentice Hall: Dorchester, England, 2000; pp 58-64.
15. Kolthoff, I. M.; Sandell, E. B.; Meehan, E. J.; Bruckenstein, S.; Quantitative Analysis, 4th ed.; Macmillian, London, 1969; p 936.