A 2H nuclear magnetic resonance study of the state of water in neat silica and zwitterionic stationary phases and its influence on the chromatographic retention characteristics in hydrophilic interaction high-performance liquid chromatography

Journal of Chromatography A

Volumn 1218, Issue 38, 2011, Pages 6630-6638

  Wikberg, Erika ^a   Sparrman, Tobias ^a   Viklund, Camilla ^b,c   Jonsson, Tobias ^b   Irgum, Knut ^a  

^a UMEÅ UNIVERSITY   (Sweden)

^b Merck SeQuant AB   (Sweden)

^c Uminova Innovation   (Sweden)

Author keywords

HPLC; Hydrophilic interaction chromatography; Retention mechanisms

Indexed keywords

CHROMATOGRAPHIC RETENTION; FREEZING-POINT DEPRESSION; GIBBS-THOMSON; HPLC; HYDROPHILIC INTERACTION; HYDROPHILIC INTERACTION CHROMATOGRAPHY; IMMOBILIZED LAYERS; MODIFIED SILICA; NUCLEAR MAGNETIC RESONANCE STUDIES; PARTITIONING MECHANISM; POLAR COMPOUNDS; POLYMERIC STATIONARY PHASIS; POROUS PROPERTIES; RETENTION CHARACTERISTICS; RETENTION MECHANISM; STATIONARY PHASE; STATIONARY PHASIS; STRUCTURAL EFFECT; WATER LAYERS; WATER STRUCTURE; ZWITTERIONIC STATIONARY PHASIS;

FUNCTIONAL POLYMERS; HYDROPHILICITY; LIQUIDS; NUCLEAR MAGNETIC RESONANCE; PHASE TRANSITIONS; PORE SIZE; RESONANCE; SILICA; SURFACE STRUCTURE;

LIQUID CHROMATOGRAPHY;

AMPHOLYTE; BETAINE DERIVATIVE; SILICON DIOXIDE; SULFOBETAINE; SURFACE WATER; UNCLASSIFIED DRUG; WATER;

ARTICLE; CHEMICAL MODIFICATION; CHEMICAL STRUCTURE; CHROMATOGRAPHIC RETENTION; CONTROLLED STUDY; DEUTERON NUCLEAR MAGNETIC RESONANCE; FREEZING; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; HYDROPHILIC INTERACTION CHROMATOGRAPHY; HYDROPHILIC INTERACTION HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; IMMOBILIZATION; PHASE TRANSITION; PHYSICAL PARAMETERS; PHYSICAL PHASE; POROSITY; PRIORITY JOURNAL; SIGNAL PROCESSING; STATIONARY PHASE; SURFACE PROPERTY; TEMPERATURE; THAWING; CHEMICAL PHENOMENA; CHEMISTRY; INSTRUMENTATION; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY;

CHROMATOGRAPHY, HIGH PRESSURE LIQUID; HYDROPHOBIC AND HYDROPHILIC INTERACTIONS; MAGNETIC RESONANCE SPECTROSCOPY; PHASE TRANSITION; SILICON DIOXIDE; WATER;

EID: 80052099865     PISSN: 00219673     EISSN: 18733778     Source Type: Journal    
DOI: 10.1016/j.chroma.2011.04.056     Document Type: Article

References (42)

1. Jiang W., Irgum K. Anal. Chem. 2002, 74:4682.
2. Jiang W., Irgum K. Anal. Chem. 2001, 73:1993.
3. Jiang W., Irgum K. Anal. Chem. 1999, 71:333.
4. Viklund C., Sjögren A., Irgum K., Nes I. Anal. Chem. 2001, 73:444.
5. Viklund C., Irgum K. Macromolecules 2000, 33:2539.
6. Hemström P., Irgum K. J. Sep. Sci. 2006, 29:1784.
7. Lee W.-F., Tsai C.-C. Polymer 1995, 36:357.
8. Konak C., Rathi R.C., Kopeckova P., Kopecek J. Macromolecules 1994, 27:1992.
9. Laughlin R.G. Langmuir 1991, 7:842.
10. Dunlop I.E., Briscoe W.H., Titmuss S., Sakellariou G., Hadjichristidis N., Klein J. Macromol. Chem. Phys. 2004, 205:2250.
11. Zhang Z., Chao T., Jiang S. J. Phys. Chem. B 2008, 112:5327. and references cited therein.
12. Jiang W., Awasum J.N., Irgum K. Anal. Chem. 2003, 75:2768.
13. Cho W.K., Kong B., Choi I.S. Langmuir 2007, 23:5678.
14. Zhang Z., Chao T., Chen S., Jiang S. Langmuir 2006, 22:10072.
15. Kitano H., Kawasaki A., Kawasaki H., Morokoshi S. J. Colloid Interface Sci. 2005, 282:340.
16. Zhang Z., Chen S., Chang Y., Jiang S. J. Phys. Chem. B 2006, 110:10799.
17. Chang Y., Chen S., Zhang Z., Jiang S. Langmuir 2006, 22:2222.
18. Jönsson B., Lindman B., Holmberg K., Kronberg B. Surfactants and Polymers in Aqueous Solution 1998, Wiley, Chichester, UK, pp. 21-23.
19. Baba T., Sakamoto R., Shibukawa M., Oguma K. J. Chromatogr. A 2004, 1040:45.
20. Liu W.G., Yao K.D. Polymer 2001, 42:3943.
21. Alekseva T.A., Lebovka N.I., Mikhailovsky S.V. Colloid J. 2003, 65:275278.
22. Carenza M., Cojazzi G., Bracci B., Lendinara L., Vitali L., Zincani M., Yoshida M., Katakai R., Takacs E., Higa O.Z., Martellini F. Radiat. Phys. Chem. 1999, 55:209.
23. Capitani D., Crescenzi V., De Angelis A.A., Segre A.L. Macromolecules 2001, 34:4136.
24. Hodge R.M., Edward G.H., Simon G.P. Polymer 1996, 37:1371.
25. Kitano H., Mori T., Takeuchi Y., Tada S., Gemmei-Ide M., Yokoyama Y., Tanaka M. Macromol. Biosci. 2005, 5:314.
26. Kitano H., Sudo K., Ichikawa K., Ide M., Ishihara K. J. Phys. Chem. B 2000, 104:11425.
27. Kitano H., Imai M., Sudo K., Ide M. J. Phys. Chem. B 2002, 106:11391.
28. Gemmei-Ide M., Motonaga T., Kitano H. Langmuir 2006, 22:2422.
29. Kitano H., Nagaoka K., Tada S., Gemmei-Ide M., Tanaka M. Macromol. Biosci. 2008, 8:77.
30. Sagidullin A.I., Furo I. Langmuir 2008, 24:4470.
31. Gane P.A.C., Ridgway C.J., Lehtinen E., Valiullin R., Furo I., Schoelkopf J., Paulapuro H., Daicic J. Ind. Eng. Chem. Res. 2004, 43:7920.
32. Sparrman T., Öquist M.G., Schleucher J., Klemetdsson L., Nilsson M. Environ. Sci. Technol. 2004, 38:5420.
33. Wikberg E., Verhage J.J., Viklund C., Irgum K. J. Sep. Sci. 2009, 32:2008.
34. LaMer V.K., Baker W.N. J. Am. Chem. Soc. 1934, 56:2641.
35. Brunauer S., Emmett P.H., Teller E. J. Am. Chem. Soc. 1938, 60:309.
36. Barrett E.P., Joyner L.G., Halenda P.P. J. Am. Chem. Soc. 1951, 73:373.
37. Halle B. Progr. NMR Spectrosc. 1996, 28:137.
38. Chavez F.V., Halle B. Magn. Reson. Med. 2006, 56:73.
39. Jackson J.A., Rabideau S.W. J. Chem. Phys. 1964, 41:4008.
40. Jackson C.L., McKenna G.B. J. Chem. Phys. 1990, 93:9002.
41. Strange J.H., Rahman M., Smith E.G. Phys. Rev. Lett. 1993, 71:3589.
42. Strange J.H., Mitchell J., Webber J.B.W. Magn. Reson. Imaging 2003, 21:221.