Determination of fat-soluble vitamins and carotenoids in standard reference material 3280 multivitamin/multielement tablets by liquid chromatography with absorbance detection

Journal of AOAC International

Volumn 94, Issue 3, 2011, Pages 815-822

  Thomas, Jeanice B ^a   Sharpless, Katherine E ^a   Yen, James H ^b   Rimmer, Catherine A ^a  

^a NATIONAL INSTITUTE OF STANDARDS AND TECHNOLOGY   (United States)

^b NATIONAL INSTITUTE OF STANDARDS AND TECHNOLOGY   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

DIETARY SUPPLEMENTS; DISTRIBUTED COMPUTER SYSTEMS; FOOD ADDITIVES; LIQUID CHROMATOGRAPHY; NUTRITION; PIGMENTS;

ABSORBANCE DETECTION; ANALYTICAL METHOD; CONCENTRATION LEVELS; FAT SOLUBLE VITAMINS; NATIONAL INSTITUTE OF STANDARDS AND TECHNOLOGY; NATIONAL INSTITUTES OF HEALTH; STANDARD REFERENCE MATERIAL; U.S. DEPARTMENT OF AGRICULTURES;

VITAMINS;

CAROTENOID; FAT; VITAMIN;

ARTICLE; CHEMISTRY; DIET SUPPLEMENTATION; LIQUID CHROMATOGRAPHY; METHODOLOGY; PHOTON ABSORPTIOMETRY; SENSITIVITY AND SPECIFICITY; STANDARD; TABLET;

ABSORPTIOMETRY, PHOTON; CAROTENOIDS; CHROMATOGRAPHY, LIQUID; DIETARY SUPPLEMENTS; FATS; REFERENCE STANDARDS; SENSITIVITY AND SPECIFICITY; TABLETS; VITAMINS;

EID: 80051937128     PISSN: 10603271     EISSN: None     Source Type: Journal    
DOI: 10.1093/jaoac/94.3.815     Document Type: Article

References (39)

1. U.S. Food and Drug Administration (1994) Dietary Supplement Health and Education Act, Washington, DC
2. U.S. Food and Drug Administration (2003) Fed. Regist. 68, 12157-12263
3. U.S. Food and Drug Administration (2006) Code of Federal Regulations, Title 2, Part 110, U.S. Government Printing Office, pp 216-217
4. U.S. Department of Agriculture, Agricultural Research Service, Nutrient Data Laboratory (2006) USDA Nutrient Database for Standard Reference, Release 18, in Nutrient Data Laboratory, http://www.nal.usda.gov/fnic/foodcomp/search or http://www.ars.usda.gov/nutrientdata, cited March 9, 2007
5. Dwyer, J.T., Picciano, M.F., Betz, J.M., Fisher, K.D., Saldanha, L.G., Yetley, E.A., Coates, P.M., Milner, J.A., Whitted, J., Burt, V., Radimer, K., Wilger, J., Sharpless, K.E., Holden, J.M., Andrews, K., Roseland, J., Zhao, C., Schweitzer, A., Harnly, J., Wolf, W.R., & Perry, C.R. (2008) J. Food Comp. Anal. 21, S83-S93
6. Dwyer, J.T., Holden, J., Andrews, K., Roseland, J., Zhao, C., Schweitzer, A., Perry, C.R., Harnly, J., Wolf, W.R., Picciano, M.F., Fosjer, K. D., Saldanha, L.G., Yetley, E.A., Betz, J.M., Coates, P.M., Milner, J.A., Whitted, J., Burt, V., Radimer, K., Wilger, J., Sharpless, K.E., & Hardy, C.J. (2007) Anal. Bioanal. Chem. 389, 37-46
7. Certificate of Analysis, Standard Reference Material 3280 Multivitamin/Multielement Tablets (2008) Standard Reference Materials Program, National Institute of Standards and Technology, Gaithersburg, MD, http://www.nist.gov/srm
8. Sander, L.C., Sharpless, K.E., Wise, S.A., Nelson, B.C., Phinney, K.W., Porter, B.J., Rimmer, C.A., Thomas, J.B., Wood, L.J., Yen, J. H., Duewer, D.L., Atkinson, R., Chen, P., Goldschmidt, R., Wolf, W.R., Ho, I-P., & Betz, J.M. (2011) Anal. Chem. 83, 99-108
9. U.S. Pharmacopeia, 29th Rev. (1975) The U.S. Pharmacopeial Convention, Rockville, MD, pp 2407-2413
10. Eriksson, M., Eriksson, T., & Sorensen, B. (1978) Acta Pharm. Suecica 15, 274-281
11. Barnett, S.A., & Frick, L.W. (1979) Anal. Chem. 51, 641-645
12. Burns, D.T., & Mackay, C. (1980) J. Chromatogr. 200, 300-304
13. Sun, J. (1999) J. AOAC Int. 82, 68-72
14. Moreno, P., & Salvado, V. (2000) J. Chromatogr. A 870, 207-215
15. Luque-Garcia, J.L., & Luque de Castro, M.D. (2001) J. Chromatogr. A 935, 3-11
16. Kozhanova, L.A., Fedorova, G.A., & Baram, G.I. (2002) J. Anal. Chem. 57, 40-45
17. Kozlov, É. I., Solunina, I. A., Lyubareva, M.L., & Nadtochii, M.A. (2003) Pharm. Chem. J. 37, 560-562
18. Breithaupt, D.E., & Kraut, S. (2006) Eur. Food Res. Technol. 222, 643-649
19. Sharpless, K.E., & Brown Thomas, J. (1997) in Laboratory Medicine: a Scientific and Managerial Infobase, Version 2.1, A.J. Pesce & L.A. Kaplan (Eds), Pesce Kaplan Publishers, Cincinnati, OH
20. Brown Thomas, J., Kline, M.C., Gill, L.M., Yen, J.H., Duewer, D.L., Sniegoski, L.T., & Sharpless, K.E. (2001) Clin. Chim. Acta 305, 141-155
21. Groenendijk, G.W.T., De Grip, W.J., & Daemen, F.J.M. (1980) Biochim. Biophys. Acta 617, 430-438
22. Handelman, G.J., Shen, B., & Krinsky, N.I. (1992) Methods Enzymol. 213, 336-346
23. Epler, K.S., Ziegler, R.G., & Craft, N.E. (1993) J. Chromatogr. B 619, 37-48
24. The Merck Index, 9th Ed. (1976) Merck & Co., Inc., Rahway, NJ, p. 3250
25. Rimmer, C.A. (2008) Nutrient Data Quality: Fat Soluble Vitamins, Vitamin Methodology Workshop, Office of Dietary Supplements, National Institutes of Health, Gaithersburg, MD
26. Certificate of Analysis, Standard Reference Material 1849 Infant/Adult Nutritional formula (2010) Standard Reference Materials Program, National Institute of Standards and Technology, Gaithersburg, MD, http://www.nist.gov/srm
27. Sharpless, K.E., Lindstrom, R.M., Nelson, B.C., Phinney, K.W., Rimmer, C.A., Sander, L.C., Schantz, M.M., Spatz, R.O., Thomas, J.B., Wise, S.A., Wood, L.J., & Yen, J.H. (2010) J. AOAC Int. 93, 1262-1274
28. Andrews, K.W. (2008) Status of Vitamin Methodology in Adult MVM Matrices Based on SRM 3280 Results, Vitamin Methodology Workshop, Office of Dietary Supplements, National Institutes of Health, Gaithersburg, MD
29. Craft, N.E. (2008) Vitamin a and Beta-Carotene: The Good, the Bad, and the Ugly, Vitamin Methodology Workshop, Office of Dietary Supplements, National Institutes of Health, Gaithersburg, MD
30. Sander, L.C., & Wise, S.A. (1990) LC·GC 5, 378-390
31. Sander, L.C., Epler Sharpless, K.S., Craft, N.E., & Wise, S.A. (1994) Anal. Chem. 66, 1667-1674
32. Sharpless, K.E., Brown Thomas, J., Sander, L.C., & Wise, S.A. (1996) J. Chromatogr. B 678, 187-195
33. Phinney, K.W., Rimmer, C.A., Thomas, J.B., Sander, L.C., Sharpless, K.E., & Wise, S.A. (2011) Anal. Chem. 83, 92-98
34. May, W., Parris, R., Beck, C., Fassett, J., Greenberg, R., Guenther, F., Kramer, G., Wise, S., Gills, T., Colbert, J., Gettings, R., & MacDonald, B. (2000) Definitions of Terms and Modes Used at NIST for Value-Assignment of Reference Materials for Chemical Measurements, NIST Special Publication 260-136, U.S. Government Printing Office, Washington, DC
35. Levenson, M.S., Banks, D.L., Eberhardt, K.R., Gill, L.M., Guthrie, W.F., Liu, H.K., Vangel, M.G., Yen, J.H., & Zhang, N.F. (2000) J. Res. Natl. Inst. Stand. Technol. 105, 571-579
36. Guide to the Expression of Uncertainty in Measurement, 1st Ed., ISO, Geneva, Switzerland, 1993; ISBN 92-67-10188-9.
37. See also: Taylor, B.N. & Kuyatt, C.E. (1994) Guidelines for Evaluating and Expressing the Uncertainty of NIST Measurement Results, NIST Technical Note 1297, U.S. Government Printing Office, Washington, DC, http://www.physics.nist.gov/Pubs/guidelines/contents.html
38. Accuracy (Trueness and Precision) of Measurement Results, Part 2: Basic Method of Repeatability and Reproducibility of a Standard Measurement Method, ISO 5725 (1997) International Organization for Standardization, Geneva, Switzerland, http://www.itl.nist.gov/div898/handbook
39. Taylor, B.N. (2005) Guide for the Use of the International System of Units (SI), NIST Special Publication 811, U.S. Government Printing Office, Washington, DC, http://www.physics.nist.gov/Pubs