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Volumn 42, Issue 8, 2011, Pages 891-902

Characterization of humic substances by advanced solid state NMR spectroscopy: Demonstration of a systematic approach

Author keywords

[No Author keywords available]

Indexed keywords

ANGLE SPINNING; DIPOLAR DEPHASING; HETERONUCLEAR CORRELATION; HUMIC ACID; HUMIC SUBSTANCES; NATURAL ORGANIC MATTERS; NEW NMR TECHNIQUES; NMR SPECTRUM; NMR TECHNIQUES; SOLID STATE NMR; SOLID-STATE NMR SPECTROSCOPY; SOLID-STATE NUCLEAR MAGNETIC RESONANCE; SPECIFIC FUNCTIONAL GROUPS; SPECTRAL EDITING; SPIN DIFFUSIONS; STEP-BY-STEP; STRUCTURAL COMPLEXITY; TECHNICAL DEVELOPMENT;

EID: 80051665635     PISSN: 01466380     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.orggeochem.2011.03.023     Document Type: Article
Times cited : (90)

References (68)
  • 1
    • 0042340664 scopus 로고    scopus 로고
    • Fossil fuels
    • John Wiley & Sons, Inc., New York, D.M. Grant, R.K. Harris (Eds.)
    • Botto R.E. Fossil fuels. Encyclopedia of Nuclear Magnetic Resonance 1996, 2101-2118. John Wiley & Sons, Inc., New York. D.M. Grant, R.K. Harris (Eds.).
    • (1996) Encyclopedia of Nuclear Magnetic Resonance , pp. 2101-2118
    • Botto, R.E.1
  • 3
    • 85097344588 scopus 로고    scopus 로고
    • The chemistry of soil organic matter
    • SSSA, Madison, WI. M.A. Tabatabai, D.L. Sparks (Eds.)
    • Clapp C.E., Hayes M.H.B., Simpson A.J., Kingery W.L. The chemistry of soil organic matter. Chemical Processes in Soils 2005, 1-150. SSSA, Madison, WI. M.A. Tabatabai, D.L. Sparks (Eds.).
    • (2005) Chemical Processes in Soils , pp. 1-150
    • Clapp, C.E.1    Hayes, M.H.B.2    Simpson, A.J.3    Kingery, W.L.4
  • 4
    • 0036557814 scopus 로고    scopus 로고
    • Elemental quantitation of natural organic matter by CPMAS C-13 NMR spectroscopy
    • Conte P., Piccolo A., van Lagen B., Buurman O., Hemminga M.A. Elemental quantitation of natural organic matter by CPMAS C-13 NMR spectroscopy. Solid State NMR 2002, 21:158-170.
    • (2002) Solid State NMR , vol.21 , pp. 158-170
    • Conte, P.1    Piccolo, A.2    van Lagen, B.3    Buurman, O.4    Hemminga, M.A.5
  • 5
    • 0033562863 scopus 로고    scopus 로고
    • Conformational arrangement of dissolved humic substances. Influence of solution composition on association of humic molecules
    • Conte P., Piccolo A. Conformational arrangement of dissolved humic substances. Influence of solution composition on association of humic molecules. Environmental Science Technology 1999, 33:1682-1690.
    • (1999) Environmental Science Technology , vol.33 , pp. 1682-1690
    • Conte, P.1    Piccolo, A.2
  • 7
    • 51849085786 scopus 로고    scopus 로고
    • Dynamics of cross polarization in solid state nuclear magnetic resonance experiments of amorphous and heterogeneous natural organic substances
    • Conte P., Berns A.E. Dynamics of cross polarization in solid state nuclear magnetic resonance experiments of amorphous and heterogeneous natural organic substances. Analytical Sciences 2008, 24:1183-1188.
    • (2008) Analytical Sciences , vol.24 , pp. 1183-1188
    • Conte, P.1    Berns, A.E.2
  • 9
    • 0001042105 scopus 로고    scopus 로고
    • Principles of centerband-only detection of exchange in solid-state nuclear magnetic resonance, and extension to four-time centerband-only detection of exchange
    • DeAzevedo E.R., Hu W.-G., Bonagamba T.J., Schmidt-Rohr K. Principles of centerband-only detection of exchange in solid-state nuclear magnetic resonance, and extension to four-time centerband-only detection of exchange. Journal of Chemical Physics 2000, 112:8988-9001.
    • (2000) Journal of Chemical Physics , vol.112 , pp. 8988-9001
    • DeAzevedo, E.R.1    Hu, W.-G.2    Bonagamba, T.J.3    Schmidt-Rohr, K.4
  • 15
    • 0024567455 scopus 로고
    • The chemical structure of highly aromatic humic acids in three volcanic ash soils as determined by dipolar dephasing NMR studies
    • Hatcher P.G., Schnitzer M., Vassallo A.M., Wilson M.A. The chemical structure of highly aromatic humic acids in three volcanic ash soils as determined by dipolar dephasing NMR studies. Geochimica et Cosmochimica Acta 1989, 53:125-130.
    • (1989) Geochimica et Cosmochimica Acta , vol.53 , pp. 125-130
    • Hatcher, P.G.1    Schnitzer, M.2    Vassallo, A.M.3    Wilson, M.A.4
  • 17
    • 77956697860 scopus 로고    scopus 로고
    • Chemical structure and heterogeneity differences of two lignins from Loblolly pine as investigated by advanced solid-state NMR spectroscopy
    • Holtman K.M., Chen N., Chappell M.A., Kadla J.F., Xu L., Mao J.-D. Chemical structure and heterogeneity differences of two lignins from Loblolly pine as investigated by advanced solid-state NMR spectroscopy. Journal of Agricultural and Food Chemistry 2010, 58:9882-9892.
    • (2010) Journal of Agricultural and Food Chemistry , vol.58 , pp. 9882-9892
    • Holtman, K.M.1    Chen, N.2    Chappell, M.A.3    Kadla, J.F.4    Xu, L.5    Mao, J.-D.6
  • 18
    • 0034141179 scopus 로고    scopus 로고
    • Poly(methylene) crystallites in humic substances detected by nuclear magnetic resonance
    • Hu W.-G., Mao J.-D., Xing B., Schmidt-Rohr K. Poly(methylene) crystallites in humic substances detected by nuclear magnetic resonance. Environmental Science and Technology 2000, 34:530-534.
    • (2000) Environmental Science and Technology , vol.34 , pp. 530-534
    • Hu, W.-G.1    Mao, J.-D.2    Xing, B.3    Schmidt-Rohr, K.4
  • 19
    • 0342980931 scopus 로고    scopus 로고
    • Characterization of ultradrawn polyethylene fibers by NMR: crystallinity, domain sizes and a highly mobile second amorphous phase
    • Hu W.-G., Schmidt-Rohr K. Characterization of ultradrawn polyethylene fibers by NMR: crystallinity, domain sizes and a highly mobile second amorphous phase. Polymer 2000, 41:2979-2987.
    • (2000) Polymer , vol.41 , pp. 2979-2987
    • Hu, W.-G.1    Schmidt-Rohr, K.2
  • 20
    • 0001222666 scopus 로고    scopus 로고
    • Polarization transfer dynamics in Lee-Goldburg cross polarization nuclear magnetic resonance experiments on rotating solids
    • Ladizhansky V., Vega S. Polarization transfer dynamics in Lee-Goldburg cross polarization nuclear magnetic resonance experiments on rotating solids. Journal of Chemical Physics 2000, 112:7158-7168.
    • (2000) Journal of Chemical Physics , vol.112 , pp. 7158-7168
    • Ladizhansky, V.1    Vega, S.2
  • 21
    • 77954600357 scopus 로고    scopus 로고
    • Systematic approaches to comprehensive analyses of natural organic matter
    • Leenheer J. Systematic approaches to comprehensive analyses of natural organic matter. Annals of Environmental Science 2009, 3:1-130.
    • (2009) Annals of Environmental Science , vol.3 , pp. 1-130
    • Leenheer, J.1
  • 22
    • 34247625470 scopus 로고    scopus 로고
    • Effect of magnetic particles on NMR spectra of Murchison meteorite organic matter and a polymer-based model system
    • Levin E.M., Bud'ko S.L., Mao J.-D., Huang Y., Schmidt-Rohr K. Effect of magnetic particles on NMR spectra of Murchison meteorite organic matter and a polymer-based model system. Solid State NMR 2007, 31:63-71.
    • (2007) Solid State NMR , vol.31 , pp. 63-71
    • Levin, E.M.1    Bud'ko, S.L.2    Mao, J.-D.3    Huang, Y.4    Schmidt-Rohr, K.5
  • 23
    • 0036298936 scopus 로고    scopus 로고
    • A robust technique for two-dimensional separation of undistorted chemical-shift anisotropy powder patterns in magic-angle-spinning NMR
    • Liu S.-F., Mao J.-D., Schmidt-Rohr K. A robust technique for two-dimensional separation of undistorted chemical-shift anisotropy powder patterns in magic-angle-spinning NMR. Journal of Magnetic Resonance 2002, 155:15-28.
    • (2002) Journal of Magnetic Resonance , vol.155 , pp. 15-28
    • Liu, S.-F.1    Mao, J.-D.2    Schmidt-Rohr, K.3
  • 26
    • 0036275655 scopus 로고    scopus 로고
    • The segmental mobility of humic acids investigated with solid-state NMR: support for dual-mode sorption of hydrophobic organic contaminants
    • Mao J.-D., Ding G., Xing B. The segmental mobility of humic acids investigated with solid-state NMR: support for dual-mode sorption of hydrophobic organic contaminants. Communications in Soil Science and Plant Analysis 2002, 33:1679-1688.
    • (2002) Communications in Soil Science and Plant Analysis , vol.33 , pp. 1679-1688
    • Mao, J.-D.1    Ding, G.2    Xing, B.3
  • 27
    • 0036497155 scopus 로고    scopus 로고
    • Correlation of poly(methylene)-rich aliphatic domains in humic substances with sorption of a nonpolar organic contaminant, phenanthrene
    • Mao J.-D., Hundal L.S., Thompson M.L., Schmidt-Rohr K. Correlation of poly(methylene)-rich aliphatic domains in humic substances with sorption of a nonpolar organic contaminant, phenanthrene. Environmental Science and Technology 2002, 36:929-936.
    • (2002) Environmental Science and Technology , vol.36 , pp. 929-936
    • Mao, J.-D.1    Hundal, L.S.2    Thompson, M.L.3    Schmidt-Rohr, K.4
  • 28
    • 0037660479 scopus 로고    scopus 로고
    • Nuclear magnetic resonance and diffuse-reflectance infrared Fourier transform spectroscopy of biosolids-derived biocolloidal organic matter
    • Mao J.-D., Hundal L.S., Schmidt-Rohr K., Thompson M.L. Nuclear magnetic resonance and diffuse-reflectance infrared Fourier transform spectroscopy of biosolids-derived biocolloidal organic matter. Environmental Science and Technology 2003, 37:1751-1757.
    • (2003) Environmental Science and Technology , vol.37 , pp. 1751-1757
    • Mao, J.-D.1    Hundal, L.S.2    Schmidt-Rohr, K.3    Thompson, M.L.4
  • 29
    • 0042709985 scopus 로고    scopus 로고
    • Recoupled long-range C-H dipolar dephasing in solid-state NMR, and its use for spectral selection of fused aromatic rings
    • Mao J.-D., Schmidt-Rohr K. Recoupled long-range C-H dipolar dephasing in solid-state NMR, and its use for spectral selection of fused aromatic rings. Journal of Magnetic Resonance 2003, 162:217-227.
    • (2003) Journal of Magnetic Resonance , vol.162 , pp. 217-227
    • Mao, J.-D.1    Schmidt-Rohr, K.2
  • 30
    • 2442501190 scopus 로고    scopus 로고
    • 13C NMR signals from di-oxygenated alkyl bands by a chemical-shift-anisotropy filter
    • 13C NMR signals from di-oxygenated alkyl bands by a chemical-shift-anisotropy filter. Solid State Nuclear Magnetic Resonance 2004, 26:36-45.
    • (2004) Solid State Nuclear Magnetic Resonance , vol.26 , pp. 36-45
    • Mao, J.-D.1    Schmidt-Rohr, K.2
  • 32
    • 23844547603 scopus 로고    scopus 로고
    • Methylene spectral editing in solid-state NMR by three-spin coherence selection
    • Mao J.-D., Schmidt-Rohr K. Methylene spectral editing in solid-state NMR by three-spin coherence selection. Journal of Magnetic Resonance 2005, 176:1-6.
    • (2005) Journal of Magnetic Resonance , vol.176 , pp. 1-6
    • Mao, J.-D.1    Schmidt-Rohr, K.2
  • 34
    • 33645234667 scopus 로고    scopus 로고
    • Absence of mobile carbohydrate domains in dry humic substances proven by NMR, and implications for organic-contaminant sorption models
    • Mao J.-D., Schmidt-Rohr K. Absence of mobile carbohydrate domains in dry humic substances proven by NMR, and implications for organic-contaminant sorption models. Environmental Science and Technology 2006, 40:1751-1756.
    • (2006) Environmental Science and Technology , vol.40 , pp. 1751-1756
    • Mao, J.-D.1    Schmidt-Rohr, K.2
  • 35
    • 34547135200 scopus 로고    scopus 로고
    • Characterization of a nitrogen-rich fulvic acid and its precursor algae by solid-state NMR
    • Mao J.-D., Cory R.M., McKnight D.M., Schmidt-Rohr K. Characterization of a nitrogen-rich fulvic acid and its precursor algae by solid-state NMR. Organic Geochemistry 2007, 38:1277-1292.
    • (2007) Organic Geochemistry , vol.38 , pp. 1277-1292
    • Mao, J.-D.1    Cory, R.M.2    McKnight, D.M.3    Schmidt-Rohr, K.4
  • 36
    • 35648935844 scopus 로고    scopus 로고
    • Humic acids from particulate organic matter in the Saguenay Fjord and the St. Lawrence Estuary investigated by advanced solid-state NMR
    • Mao J.-D., Tremblay L., Gagné J.-P., Kohl S., Rice J., Schmidt-Rohr K. Humic acids from particulate organic matter in the Saguenay Fjord and the St. Lawrence Estuary investigated by advanced solid-state NMR. Geochimica et Cosmochimica Acta 2007, 71:5483-5499.
    • (2007) Geochimica et Cosmochimica Acta , vol.71 , pp. 5483-5499
    • Mao, J.-D.1    Tremblay, L.2    Gagné, J.-P.3    Kohl, S.4    Rice, J.5    Schmidt-Rohr, K.6
  • 37
    • 48349089921 scopus 로고    scopus 로고
    • Influence of animal manure application on the chemical structures of soil organic matter as investigated by advanced solid-state NMR and FT-IR spectroscopy
    • Mao J.-D., Olk D.C., Fang X., He Z., Schmidt-Rohr K. Influence of animal manure application on the chemical structures of soil organic matter as investigated by advanced solid-state NMR and FT-IR spectroscopy. Geoderma 2008, 146:353-362.
    • (2008) Geoderma , vol.146 , pp. 353-362
    • Mao, J.-D.1    Olk, D.C.2    Fang, X.3    He, Z.4    Schmidt-Rohr, K.5
  • 40
    • 77951098412 scopus 로고    scopus 로고
    • Structural features of a bituminous coal and their changes during low-temperature oxidation and loss of volatiles investigated by advanced solid-state NMR spectroscopy
    • Mao J.-D., Schimmelmann A., Mastalerz M., Hatcher P.G., Li Y. Structural features of a bituminous coal and their changes during low-temperature oxidation and loss of volatiles investigated by advanced solid-state NMR spectroscopy. Energy & Fuels 2010, 24:2536-2544.
    • (2010) Energy & Fuels , vol.24 , pp. 2536-2544
    • Mao, J.-D.1    Schimmelmann, A.2    Mastalerz, M.3    Hatcher, P.G.4    Li, Y.5
  • 41
    • 77954738639 scopus 로고    scopus 로고
    • Chemical structure of soil organic matter in slickspots as investigated by advanced solid-state NMR
    • Mao J.-D., Palazzo A.J., Olk D.C., Clapp C.E., Senesi N., Bashore T.L., Cao X.-Y. Chemical structure of soil organic matter in slickspots as investigated by advanced solid-state NMR. Soil Science 2010, 175:329-338.
    • (2010) Soil Science , vol.175 , pp. 329-338
    • Mao, J.-D.1    Palazzo, A.J.2    Olk, D.C.3    Clapp, C.E.4    Senesi, N.5    Bashore, T.L.6    Cao, X.-Y.7
  • 42
    • 79952308228 scopus 로고    scopus 로고
    • Chemical structures of corn stover and its residue after dilute acid prehydrolysis and enzymatic hydrolysis: Insight into factors limiting enzymatic hydrolysis
    • Mao J.-D., Holtman K.M., Franqui-Villanueva D. Chemical structures of corn stover and its residue after dilute acid prehydrolysis and enzymatic hydrolysis: Insight into factors limiting enzymatic hydrolysis. Journal of Agricultural and Food Chemistry 2010, 58:11680-11687.
    • (2010) Journal of Agricultural and Food Chemistry , vol.58 , pp. 11680-11687
    • Mao, J.-D.1    Holtman, K.M.2    Franqui-Villanueva, D.3
  • 44
    • 33847700459 scopus 로고    scopus 로고
    • Advanced instrumental approaches for characterization of marine dissolved organic matter: extraction techniques, mass spectrometry, and nuclear magnetic resonance spectroscopy
    • Mopper K., Stubbins A., Ritchie J.D., Bialk H.M., Hatcher P.G. Advanced instrumental approaches for characterization of marine dissolved organic matter: extraction techniques, mass spectrometry, and nuclear magnetic resonance spectroscopy. Chemical Reviews 2007, 107:419-442.
    • (2007) Chemical Reviews , vol.107 , pp. 419-442
    • Mopper, K.1    Stubbins, A.2    Ritchie, J.D.3    Bialk, H.M.4    Hatcher, P.G.5
  • 46
    • 33845560961 scopus 로고
    • Selection of nonprotonated carbon resonances in solid-state nuclear magnetic resonance
    • Opella S.J., Frey M.H. Selection of nonprotonated carbon resonances in solid-state nuclear magnetic resonance. Journal of the American Chemical Society 1979, 101:5854-5856.
    • (1979) Journal of the American Chemical Society , vol.101 , pp. 5854-5856
    • Opella, S.J.1    Frey, M.H.2
  • 48
    • 0028995620 scopus 로고
    • 13C CPMAS NMR off de-ashed soil humin in a 2nd-growth Douglas-fir stand of coastal British-Columbia
    • 13C CPMAS NMR off de-ashed soil humin in a 2nd-growth Douglas-fir stand of coastal British-Columbia. Geoderma 1995, 68:229-241.
    • (1995) Geoderma , vol.68 , pp. 229-241
    • Preston, C.M.1    Newman, R.H.2
  • 49
    • 0029752805 scopus 로고    scopus 로고
    • Applications of NMR to soil organic matter analysis: history and prospects
    • Preston C.M. Applications of NMR to soil organic matter analysis: history and prospects. Soil Science 1996, 161:144-166.
    • (1996) Soil Science , vol.161 , pp. 144-166
    • Preston, C.M.1
  • 50
    • 0001102779 scopus 로고    scopus 로고
    • Carbon-13 solid-state NMR of soil organic matter - using the technique effectively
    • Preston C.M. Carbon-13 solid-state NMR of soil organic matter - using the technique effectively. Canadian Journal of Soil Science 2001, 81:255-270.
    • (2001) Canadian Journal of Soil Science , vol.81 , pp. 255-270
    • Preston, C.M.1
  • 51
    • 0035743666 scopus 로고    scopus 로고
    • Spectral editing in solid-state NMR using scalar multiple quantum filters
    • Sakellariou D., Lesage A., Emsley L. Spectral editing in solid-state NMR using scalar multiple quantum filters. Jounal of Magnetic Resonance 2001, 151:41-47.
    • (2001) Jounal of Magnetic Resonance , vol.151 , pp. 41-47
    • Sakellariou, D.1    Lesage, A.2    Emsley, L.3
  • 55
    • 0037182956 scopus 로고    scopus 로고
    • Selective observation of nitrogen-bonded carbons in solid-state NMR by saturation-pulse induced dipolar exchange with recoupling
    • Schmidt-Rohr K., Mao J.-D. Selective observation of nitrogen-bonded carbons in solid-state NMR by saturation-pulse induced dipolar exchange with recoupling. Chemical Physics Letters 2002, 359:403-411.
    • (2002) Chemical Physics Letters , vol.359 , pp. 403-411
    • Schmidt-Rohr, K.1    Mao, J.-D.2
  • 62
    • 0346938543 scopus 로고    scopus 로고
    • High-field and high-speed CP-MAS C-13 NMR heteronuclear dipolar-correlation spectroscopy of solids with frequency-switched Lee-Goldburg homonuclear decoupling
    • vanRossum B.J., Forster H., deGroot H.J.M. High-field and high-speed CP-MAS C-13 NMR heteronuclear dipolar-correlation spectroscopy of solids with frequency-switched Lee-Goldburg homonuclear decoupling. Journal of Magnetic Resonance 1997, 124:516-519.
    • (1997) Journal of Magnetic Resonance , vol.124 , pp. 516-519
    • vanRossum, B.J.1    Forster, H.2    deGroot, H.J.M.3
  • 66
    • 43949157887 scopus 로고
    • Spectral editing in CPMAS NMR. Generating subspectra based on proton multiplicities
    • Wu X., Burns S.T., Zilm K.W. Spectral editing in CPMAS NMR. Generating subspectra based on proton multiplicities. Journal of Magnetic Resonance, Series A 1994, 111:29-36.
    • (1994) Journal of Magnetic Resonance, Series A , vol.111 , pp. 29-36
    • Wu, X.1    Burns, S.T.2    Zilm, K.W.3
  • 67
    • 0022715174 scopus 로고
    • 13C proton shift correlation spectroscopy of a whole coal
    • 13C proton shift correlation spectroscopy of a whole coal. Fuel 1986, 65:721-724.
    • (1986) Fuel , vol.65 , pp. 721-724
    • Zilm, K.W.1    Webb, G.G.2
  • 68
    • 0024000859 scopus 로고
    • Applications of zero field and 2-dimensional NMR methods to fossil fuels
    • Zilm K.W., Webb G.G. Applications of zero field and 2-dimensional NMR methods to fossil fuels. Fuel 1988, 67:707-713.
    • (1988) Fuel , vol.67 , pp. 707-713
    • Zilm, K.W.1    Webb, G.G.2


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