Electrochemical study of ceftazidime-copper (II) complex: Synthesis, characterization, biological activity and analytical application to pharmaceutical dosage forms

Current Analytical Chemistry

Volumn 6, Issue 4, 2010, Pages 299-309

  Muslu, Harun ^a   Golcu, Aysegul ^a   Ozkan, Sibel A ^b  

^a KAHRAMANMARAS SUTCU IMAM UNIVERSITY   (Turkey)

^b ANKARA UNIVERSITY   (Turkey)

Author keywords

Biological activity; Ceftazidime; Copper complex; Electrochemistry; Spectral properties

Indexed keywords

ANTIBIOTICS; BACILLUS CEREUS; BACTERIOLOGY; COPPER COMPOUNDS; ELECTROCHEMISTRY; ESCHERICHIA COLI; GLASS MEMBRANE ELECTRODES; MASS SPECTROMETRY; SPECTROSCOPIC ANALYSIS; YEAST;

CEFTAZIDIME; COPPER COMPLEXES; DIFFERENTIAL PULSE; ELECTROCHEMICAL STUDIES; PULSE-WAVE; SPECTRAL PROPERTIES; SQUARE-WAVE; SYNTHESISED; THIRD GENERATION; VOLTAMMETRIC TECHNIQUES;

BIOACTIVITY;

EID: 80051656299     PISSN: 15734110     EISSN: None     Source Type: Journal    
DOI: 10.2174/1573411011006040299     Document Type: Article

References (53)

1. Zaki, A.; Schreiber, E.C.; Weliky, I.; Knill, J.R.; Hubsher, H.J. Clinical pharmacology of oral cephradine. J. Clin. Pharmacol., 1974, 14, 118-126.
2. Klostersky, J.; Danean, D.; Weerts, D. Cephradine Antibacterial activity and clinical effectiveness. Chemotherapy, 1973, 18, 191-196.
3. Anacona, J.R. Synthesis and antibacterial activity of some metal complexes of beta-lactamic antibiotics. J. Coord. Chem., 2001, 54, 355-365.
4. Lozano, J.; Borras, J. Antibiotic as ligand. Coordinating behavior of the cephalexin towards Zn(II) and Cd(II) ions. J. Inorg. Biochem., 1987, 31, 187-195.
5. Abou-Attia, F.M.; YIssa, M.; Abdel-Gawad, F.M.; Abdel-Hamid, S.M. Quantitative determination of some pharmaceutical piperazine derivatives through complexation with iron(III) chloride. II Farmaco, 2003, 58, 573-579.
6. Helaleh, M.I.H.; Nameh, E.S.M. Selective kinetic study for the degradation of cephalexin in alkaline aqueous media. Anal. Quim. Intern. Ed., 1998, 94, 160-165.
7. Sorenson, J.R.J. Copper chelates as possible active forms of antiarthritic agents. J. Med. Chem., 1976, 19, 135-148.
8. Brown, D.H.; Lewis, A.E.; Smith, W.E.; Teape, J.W. Antiinflammatory effects of some copper complexes. J. Med. Chem., 1980, 23, 729-734.
9. Williams, D.R. The Metals of Life, Van Nostrand Reinhold, London, 1971.
10. Ruiz, M.; Perello, L.; Ortiz, R.; Castineiras, A.; Maichlemossmer, C.; Can-ton E. Synthesis, characterization, and crystal structure of [Cu(cinoxacinate)2]cntdot.2H2O complex: a square-planar CuO4 chromophore, Antibacterial studies. J. Inorg. Biochem., 1995, 59, 801-810.
11. Castillo-Blum, S.E.; Barba-Behrens N. Coordination chemistry of some biologically active ligands. Coord. Chem. Rev., 2000, 196, 3-30.
12. United States Pharmacopoeia XXIII, United States Pharmacopoeia Convection, Rockville, MD, 1993.
13. Fabre, H.; Blanchin, M.D.; Kok W.T. Liquid chromatography with amperometric detection for the determination of cephalosporins in biological fluids. Analyst, 1988, 113, 651-655.
14. El-Gindy, A.; El Walily, A.F.; Bedair M.F. First-derivative spectrophotometric and LC determination of cefuroxime and cefadroxil in urine. J. Pharmaceut. Biomed. Anal., 2000, 23, 341-352.
15. Al-Rawithi, S.; Hussien, R.; Raines, D.A.; AlShowaier, I.; Kurdi W. Sensitive assay for the determination of cefazolin or ceftriaxone in plasma utilizing LC. J. Pharmaceut. Biomed. Anal., 2000, 22, 281-286.
16. Shin, Y.S.; Kruis, B.; Heininger, U.; Endres, W. Radioisotopic methods for assay of the enzymes in the urea cycle: First trimester diagnostic possibilities for urea cycle disorders using chorionic villi sampling. J. Inherit. Metab. Dis., 1987, 10, 314-316.
17. Rani, A.S.; Jayaraman, A.; Sharma, L.D.; Murali Dhar, G.; Prasada Rao T.S.R. Cyclic voltammetric studies of alumina supported monometallic Pt and bimetallic Pt---Sn catalysts using carbon paste electrodes. J. Electroanal. Chem., 2000, 495, 62-70.
18. Reddy, G.V.S.; Reddy S.J. Estimation of cephalosporin antibiotics by differential pulse polarography. Talanta, 1997, 44, 627-631.
19. Altinöz, S.; Ozer, D.; Temizer A. Determination of ceftriaxone in aqueous-humor and serum samples by differential-pulse adsorptive stripping voltammetry. Analyst, 1994, 119, 1575-1577.
20. Ozkan, S.A.; Erk, N.; Uslu, B.; Yilmaz, N.; Biryol I. Study on electrooxidation of cefadroxil monohydrate and its determination by differential pulse voltammetry. J. Pharm. Biomed. Anal., 2000, 23, 263-273.
21. Yang, J.; Zhou, G.; Zhang, G.; Su, Z.; Hu J. Determination of some cephalosporins in pharmaceutical formulations by a fluorescence quenching method. Anal. Commun., 1996, 33, 167-169.
22. Agbaba, D.; Eric, S.; Karljikovic-Rajic, K.; Zivanov, S.; Stakic D. Spectrophotometric Determination of Certain Cephalosporins Using Ferrihydroxamate Method. Spectrosc. Lett., 1997, 30, 309-319.
23. Zakhari, N.A.; Walash, M.I.; Rizk, M.S., Toubar, S.S.; Brooks, C.J.W.; Cole, W.J. Gas chromatographic assay of methyltestosterone in tablets. J. Pharm. Biomed. Analysis., 1991, 9, 705-709.
24. Ayad, M.M.; Shalaby, A.A.; Abdellatef, H.E.; Elsaid, H.M. Spectrophotometric determination of certain cephalosporins through oxidation with cerium(IV) and 1-chlorobenzotriazole. J. Pharm. Biomed. Analysis, 1999, 20, 557-564.
25. Issopoulos, P.B.; Sofia, S.E. Analytical investigation of β-lactam antibiotics in pharmaceutical preparations IX. Colorimetric determination of six cephalosporins of second and third generation in the range of micromolar concentrations. Acta Pharm. Hung., 1996, 66, 89-94.
26. Ayad, M.; Shalaby, A.A.; Abdellatef, H.E.; Elsaid, H.M. Spectrophotometric and atomic absorption spectrometric determination of certain cephalosporins. J. Pharm. Biomed. Anal., 1999, 18, 975-983.
27. El-Gindy, A.; El Walily, A.F.; Bedair, M.F. First-derivative spectrophotometric and LC determination of cefuroxime and cefadroxil in urine. J. Pharm. Biomed. Anal., 2000, 23, 341-352.
28. Martinez, L.G.; Cabeza, A.S.; Falco, P.C.; Reig, F.B. A new derivatization procedure for the determination of cephalexin with 1,2-naphthoquinone 4-sulphonate in pharmaceutical and urine samples using solid-phase extraction cartridges and UV-visible detection. Anal. Chim. Acta, 1983, 70, 115-123.
29. Alwarthan, A.A.; Metwally, F.H.; Al-Tamimi, S.A. Determination of Promethazine by Its Inhibition of the Chmiluminescence of the Luminol-Hydrogen Peroxide-Chromiun(III) System. Anal. Lett., 1993, 26, 2619-2635.
30. Anacona, J.R.; Patino, C. Metalloantibiotics: synthesis and antibacterial activity of ceftazidime metal complexes. J. Coord. Chem., 2009, 62, 613-621.
31. Zhang, X.; Zhai, S.; Zhao, R.; Ouyang R.G. Willy, J.; Li, X. Determination of cilnidipine, a new calcium antagonist, in human plasma using high performance liquid chromatography with tandem mass spectrometric detection. Anal. Chim. Acta, 2007, 600, 142-146.
32. El-Maali, N.A.; Osman, A.H.; Aly, A.M.M.; Al-Hazmi, G.A.A. Voltammetric analysis of Cu (II), Cd (II) and Zn (II) complexes and their cyclic voltammetry with several cephalosporin antibiotics. Bioelectrochemistry, 2005, 65, 95-104.
33. Saxena, K.B.C.; Aly, A.M.M. Information technology support for reengineering public administration: A conceptual framework. Int. J. Inform. Manag., 1995, 15, 271-293.
34. Osman, A.H.; Aly, A.M.M.; El-Maali, N.A.; Al-Hazmi, G.A.A. An investigation of the cu(ii) complexes of certain cephalosporin antibiotics: spectral, thermal, and photochemical studies. Synth. React. Inorg. Metalo-Org. Chem., 2002, 32, 1289-1300.
35. Osman, A.H.; El-Maali, N.A.; Aly, A.M.M.; Al-Hazmi, G.A.A. Synthesis and reactivity in inorganic, metal-organic, and nanometal chemistry. Synth. React. Inorg. Metalo-Org. Chem., 2002, 32, 763-781.
36. Ozkan, S.A.; Uslu, B.; Zuman, P. Electrochemical reduction and oxidation of the antibiotic cefepime at a carbon electrode. Anal. Chim. Acta, 2002, 457, 265-274.
37. Golcu, A.; Dogan, B.; Ozkan, S.A. Electrochemical reduction and oxidation of the antibiotic cefepime at a carbon electrode. Talanta, 2005, 67, 703-712.
38. Dogan, B.; Golcu, A.; Dolaz, M.; Ozkan, S.A. electrochemical behaviour of the bactericidal cefoperazone and its selective voltammetric determination in pharmaceutical dosage forms and human serum. Curr. Pharm. Anal., 2009, 5, 179-189.
39. Dogan, B.; Golcu, A.; Dolaz, M.; Ozkan, S.A. Anodic oxidation of antibacterial drug cefotaxime sodium and its square wave and differential pulse voltammetric determination in pharmaceuticals and human serum. Curr. Pharm. Anal., 2009, 5, 197-207.
40. Wang, J. Electroanalytical techniques in clinical chemistry and laboratory medicine, VCH Publishers: New York, 1988.
41. Zengin, H.; Dolaz, M.; Golcu, A. preparation, photoluminescence and antimicrobial activity of loracarbef and its various complexes. Curr. Anal. Chem., 2009, 5, 358-362.
42. Golcu, A.; Dolaz, M.; Kocak B.; Kavak N.; Demirelli, H. Spectrophotometric determination of levofloxacin in pharmaceutical formulations. Asian J. Chem., 2009, 21, 528-540.
43. Golcu, A.; Yavuz, P. Spectral, analytical, thermal, and antimicrobial studies of novel sodium 2-[4(2-hydroxy-3-izopropylaminopropoxy) phenyl]acetamide (atenolol) dithiocarbamate and its divalent transition metal complexes. Russian J. Coord. Chem., 2008, 34, 106-114.
44. Golcu, A. New, simple, and validated UV-spectrophotometric method for the estimation of some beta blockers in bulk and formulations. J. Anal. Chem., 2008, 63, 538-543.
45. Gölcü, A.; Dolaz, M.; Demirelli, H.; Diǧak, M.; Serin, S. Spectroscopic and analytic properties of new copper(II) complex of antiviral drug valacyclovir. Trans. Metal Chem., 2006, 31, 658-665.
46. Gölcü, A. Transition metal complexes of propranolol dithiocarbamate: synthesis, characterization, analytical properties and biological activity. Trans. Metal Chem., 2006, 31, 405-412.
47. Tumer, M.; Deligonul, N.; Golcu, A. Mixed-ligand copper(II) complexes: Investigation of their spectroscopic, catalysis, antimicrobial and potentiometric properties. Trans. Metal Chem., 2006, 31, 1-12.
48. Kissenger, P. T., Heineman, W. R. Laboratory Techiques in Electroanalytical Chemistry, 2nd ed., Marcel Dekker: New York, 1996.
49. Gosser, D.K. Cyclic Voltammetry, VCH: New York, 1994.
50. Laviron, E.; Rouillier, L.; Degrand, C. A multilayer model for the study of space distributed redox modified electrodes: Part II. Theory and application of linear potential sweep voltammetry for a simple reaction. J. Electroanal. Chem., 1980, 112, 11-23.
51. Riley, C.M.; Rosanske, T.W. Development and Validation of Analytical Methods, Elsevier Science Ltd.: New York, 1996.
52. Ermer, J.; Miller, J.H. McB. Method validation in pharmaceutical analysis, 1st ed. Wiley-VCH Pub.: Germany, 2005.
53. Swartz, M.E.; Krull, I.S. Analytical Method Development and Validation, Marcel, Dekker: New York, 1997.