Low-to-medium-frequency AC impedance spectroscopy investigations of nanocrystalline calcium silicate hydrate dried powders

Journal of the American Ceramic Society

Volumn 94, Issue 8, 2011, Pages 2680-2687

  Leroux, Fabrice ^a,b   Russias, Julie ^c   Cau Dit Coumes, Celine ^c   Frizon, Fabien ^c   Renaudin, Guillaume ^a,b  

^a UNIVERSITÉ CLERMONT AUVERGNE   (France)

^b CNRS   (France)

^c DIF   (France)

Author keywords

[No Author keywords available]

Indexed keywords

ADDITIVES; DEHYDRATION; EQUIVALENT CIRCUITS; FRACTAL DIMENSION; GRAIN BOUNDARIES; HYDRATES; HYDRATION; NANOCRYSTALS; SILICATE MINERALS; SPECTROSCOPY;

AC IMPEDANCE SPECTROSCOPY; CALCIUM SILICATE HYDRATE; CHARGE ACCUMULATION; CONSTANT PHASE ELEMENT; DEHYDRATION PROCESS; DIELECTRIC POLARIZATION; IMPEDANCE SPECTROSCOPY; MEDIUM-FREQUENCY RANGE;

CALCIUM SILICATE;

EID: 80051548989     PISSN: 00027820     EISSN: 15512916     Source Type: Journal    
DOI: 10.1111/j.1551-2916.2011.04429.x     Document Type: Article

References (49)

1. H. F. W. Taylor, " Hydration of Portland cement "; pp. 187-226 in Cement Chemistry. Chapter 7, 2nd edition, Edited by, T. Telford,. Thomas Telford Publishing, London, 1997.
2. M. D. Andersen, H. J. Jakobsen, and, J. Skibsted, " Incorporation of Aluminum in the Calcium Silicate Hydrate (C-S-H) of Hydrated Portland Cements: A High-Field 27Al and 29Si MAS NMR Investigation," Inorg. Chem., 42 [7] 2280-7 (2003).
3. 27Al NMR and EELS," J. Am. Ceram. Soc., 76 [9] 2285-8 (1993).
4. 29Si MAS NMR Spectroscopy," Cem. Concr. Res., 34 [5] 857-68 (2004).
5. P. Faucon, A. Delagrave, J. C. Petit, C. Richet, J. M. Marchand, and, H. Zanni, " Aluminum Incorporation in Calcium Silicate Hydrates (C-S-H) Depending on their Ca/Si Ratio," J. Phys. Chem. B, 103 [37] 7796-802 (1999).
6. G. K. Sun, J. F. Young, and, R. J. Kirkpatrick, " The Role of Al in C-S-H: NMR, XRD, and Compositional Results for Precipitated Samples," Cem. Concr. Res., 36 [1] 18-29 (2006).
7. X. Pardal, I. Pochard, and, A. Nonat, " Experimental Study of Si-Al Substitution in Calcium-Silicate-Hydrate (C-S-H) Prepared Under Equilibrium Conditions," Cem. Concr. Res., 39 [8] 637-43 (2009).
8. H. M. Jennings, " Refinements to Colloid Model of CSH in Cement: CM-II," Cem. Concr. Res., 38 [3] 275-89 (2008).
9. P. R. Camp, and, S. Bilotta, " Dielectric Properties of Portland Cement Paste as a Function of Time Since Mixing," J. Appl. Phys., 66 [12] 6007-13 (1989).
10. P. Gu, and, J. J. Beaudoin, " Dielectric Behavior of Hardened Cement Paste Systems," J. Mater. Sci. Lett., 15 [2] 182-4 (1996). (Pubitemid 126739238)
11. D. Buerchler, B. Elsener, and, H. Boehni, " Electrical Resistivity and Dielectric Properties of Hardened Cement Paste and Mortar," Mater. Res. Soc. Symp. Proc., 411, 407-12 (1996).
12. P. Gu, P. Xie, J. J. Beaudoin, and, R. Brousseau, " A.C. Impedance Spectroscopy (II): Microstructural Characterization of Hydrating Cement-Silica Fume Systems," Cem. Concr. Res., 23 [1] 157-68 (1993).
13. W. J. McCarter, G. Starrs, and, T. M. Chrisp, " The Complex Impedance Response of Fly-Ash Cements Revisited," Cem. Concr. Res., 34 [10] 1837-43 (2004).
14. F. D. Tamas, E. Farkas, M. Voros, and, D. M. Roy, " Low-Frequency Electrical Conductivity of Cement, Clinker and Clinker Mineral Pastes," Cem. Concr. Res., 17 [2] 340-8 (1987). (Pubitemid 17530946)
15. G. Levita, A. Marchetti, G. Gallone, A. Princigallo, and, G. L. Guerrini, " Electrical Properties of Fluidified Portland Cement Mixes in the Early Stage of Hydration," Cem. Concr. Res., 30 [6] 923-30 (2000).
16. M. Moukwa, M. Brodwin, S. Christo, J. Chang, and, S. P. Shah, " The Influence of the Hydration Process Upon Microwave Properties of Cements," Cem. Concr. Res., 21 [5] 863-72 (1991). (Pubitemid 21698424)
17. J. M. Torrents, J. Roncero, and, R. Gettu, " Utilization of Impedance Spectroscopy for Studying the Retarding Effect of a Superplasticizer on the Setting of Cement," Cem. Concr. Res., 28 [9] 1325-33 (1998). (Pubitemid 128634293)
18. T. O. Mason, M. A. Campo, A. D. Hixon, and, L. Y. Woo, " Impedance Spectroscopy of Fiber-Reinforced Cement Composites," Cem. Concr. Compos., 24 [5] 457-66 (2002).
19. B. Jönsson, H. Wennerström, A. Nonat, and, B. Cabane, " Onset of Cohesion in Cement Paste," Langmuir, 20 [16] 6702-9 (2004).
20. L. Nachbaur, J. C. Mutin, A. Nonat, and, L. Choplin, " Dynamic Mode Rheology of Cement and Tricalcium Silicate Pastes from Mixing to Setting," Cem. Concr. Res., 31 [2] 183-92 (2001). (Pubitemid 33763338)
21. C. Labbez, B. Jönsson, I. Pochard, A. Nonat, and, B. Cabane, " Surface Charge Density and Electrokinetic Potential of Highly Charged Minerals: Experiments and Monte Carlo Simulations on Calcium Silicate Hydrate," J. Phys. Chem. B, 110 [18] 9219-30 (2006).
22. C. Labbez, A. Nonat, I. Pochard, and, B. Jönsson, " Experimental and Theoretical Evidence of Overcharging of Calcium Silicate Hydrate," J. Colloid Interface Sci., 309 [2] 303-7 (2007). (Pubitemid 46551124)
23. C. Labbez, B. Jönsson, M. Skarba, and, M. Borkovec, " Ion-Ion Correlation and Charge Reversal at Titrating Solid Interfaces," Langmuir, 25 [13] 7209-13 (2009).
24. M. Keddam, H. Takenouti, X. R. Novoa, and, C. Andrade, " Impedance Measurements on Cement Paste," Cem. Conc. Res., 27 [8] 1191-201 (1997). (Pubitemid 127407836)
25. B. J. Christensen, R. T. Coverdale, R. A. Olson, S. J. Ford, E. J. Garboczi, H. M. Jennings, and, T. O. Mason, " Impedance Spectroscopy of Hydrating Cement-Based Materials: Measurement, Interpretation, and Application," J. Am. Ceram. Soc., 77 [11] 2789-804 (1994).
26. B. J. Christensen, T. O. Mason, and, H. M. Jennings, " Influence of Silica Fume on the Early Hydration of Portland Cements Using Impedance Spectroscopy," J. Am. Ceram. Soc., 75 [4] 939-45 (1992).
27. P. Gu, P. Xie, Y. Fu, and, J. J. Beaudoin, " A.C Impedance Phenomena in Hydrating Cement Systems: Frequency Dispersion Angle and Pore Size Distribution," Cem. Concr. Res., 24 [1] 86-8 (1994).
28. R. T. Coverdale, B. J. Christensen, T. O. Mason, H. M. Jennings, and, E. J. Garboczi, " Interpretation of the Impedance Spectroscopy of Cement Paste via Computer Modelling, Part II Dielectric Response," J. Mater. Sci., 29 [19] 4984-92 (1994).
29. C. Andrade, V. M. Blanco, A. Collazo, M. Keddam, X. R. Novoa, and, H. Takenouti, " Cement Paste Hardening Process Studied by Impedance Spectroscopy," Electrochim. Acta, 44 [24] 4313-8 (1999).
30. C. Alonso, C. Andrade, M. Keddam, X. R. Novoa, and, H. Takenouti, " Study of the Dielectric Characteristics of Cement Paste," Mater. Sci. Forum, 289-292, 15-28 (1998). (Pubitemid 128565839)
31. Y. El Hafiane, A. Smith, J. P. Bonnet, P. Abélard, and, P. Blanchart, " Electrical Characterization of Aluminous Cement at the Early Age in the 10 Hz-1 GHz Frequency Range," Cem. Conc. Res., 30 [7] 1057-62 (2000).
32. L. Y. Woo, N. J. Kidner, S. Wansom, and, T. O. Mason, " Combined Time Domain Reflectometry and AC-Impedance Spectroscopy of Fiber-Reinforced Fresh-Cement Composites," Cem. Concr. Res., 37 [1] 89-95 (2007). (Pubitemid 44838564)
33. G. Renaudin, J. Russias, F. Leroux, F. Frizon, and, C. Cau-dit-Coumes, " Structural Characterization of C-S-H and C-A-S-H Samplesa - Part I: Long-Range Order Investigated by Rietveld Analyses," J. Solid State Chem., 182 [12] 3312-9 (2009).
34. G. Renaudin, J. Russias, F. Leroux, C. Cau-dit-Coumes, and, F. Frizon, " Structural Characterization of C-S-H and C-A-S-H Samplesa - Part II: Local Environment Investigated by Spectroscopic Analyses," J. Solid State Chem., 182 [12] 3320-9 (2009).
35. M. Cabeza, M. Keddam, X. R. Novoa, I. Sanchez, and, H. Takenouti, " Impedance Spectroscopy to Characterize the Pore Structure During the Hardening Process of Portland Cement Paste," Electrochim. Acta, 51 [8-9] 1831-41 (2006). (Pubitemid 43102508)
36. M. Cabeza, P. Merino, A. Miranda, X. R. Novoa, and, I. Sanchez, " Impedance Spectroscopy Study of Hardened Portland Cement Paste," Cem. Concr. Res., 32 [6] 881-91 (2002). (Pubitemid 34527058)
37. K. G. Gatos, J. G. Martinez Alcazar, G. C. Psarras, R. Thomann, and, J. Karger-Kocsis, " Polyurethane Latex/Water Dispersible Boehmite Alumina Nanocomposites: Thermal, Mechanical and Dielectrical Properties," Comp. Sci. Technol., 67 [2] 157-67 (2007).
38. G. M. Tsangaris, G. C. Psarras, and, N. Kouloumbi, " Electric Modulus and Interfacial Polarization in Composite Polymeric Systems," J. Mater. Sci., 33 [8] 2027-37 (1998). (Pubitemid 128509637)
39. D. E. Wilkosz, and, J. F. Young, " Effect of Moisture Adsorption on the Electrical Properties of Hardened Portland Cement Compacts," J. Am. Ceram. Soc., 78 [6] 1673-9 (1995).
40. A. Berg, G. A. Niklasson, K. Brantervik, B. Hedberg, and, L. O. Nilsson, " Dielectric Properties of Cement Mortar as a Function of Water Content," J. Appl. Phys., 71 [12] 5897-903 (1992).
41. W. J. McCarter, " Effects of Temperature on Conduction and Polarization in Portland Cement Mortar," J. Am. Ceram. Soc., 78 [2] 411-5 (1995).
42. G. A. Niklasson, A. Berg, K. Brantervik, B. Hedberg, and, L. O. Nilsson, " Dielectric Properties of Porous Cement Mortar: Fractal Surface Effects," Solid State Commun., 79 [1] 93-6 (1991).
43. R. A. Livingston, " Fractal Nucleation and Growth Model for the Hydration of Tricalcium Silicate," Cem. Concr. Res., 30 [12] 1853-60 (2000). (Pubitemid 32874473)
44. K. Garbev, M. Bornefeld, G. Beuchle, and, P. Stemmermann, " Cell Dimensions and Composition of Nanocrystalline Calcium Silicate Hydrate Solid Solutions. Part 2: X-Ray and Thermogravimetry Study," J. Am. Ceram. Soc., 91 [9] 3015-23 (2008).
45. H. C. Kim, and, S. S. Yoon, " Dynamic Dielectric Analysis During Early-Stage Hydration of Ordinary Portland Cement," J. Phys. D: Appl. Phys., 21 [7] 1215-20 (1988).
46. N. Shinyashiki, D. Imoto, and, S. Yagihara, " Broadband Dielectric Study of Dynamics of Polymer and Solvent in Poly (vinyl pyrrolidone)/Normal Alcohol Mixtures," J. Phys. Chem. B, 111 [9] 2181-7 (2007). (Pubitemid 46447550)
47. J. Mijovic, S. Ristic, and, J. Kenny, " Dynamics of Six Generations of PAMAM Dendrimers As Studied by Dielectric Relaxation Spectroscopy," Macromolecules, 40 [14] 5212-21 (2007). (Pubitemid 47169942)
48. S. S. Yoon, S. Y. Kim, and, H. C. Kim, " Dielectric Spectra of Fresh Cement Paste Below Freezing Point Using an Insulated Electrode," J. Mater. Sci., 29 [7] 1910-4 (1994).
49. A. Atkinson, and, A. K. Nickerson, " The Diffusion of Ions Through Water-Saturated Cement," J. Mater. Sci., 19 [9] 3068-78 (1984). (Pubitemid 14668599)