Characterization of white Portland cement hydration and the C-S-H structure in the presence of sodium aluminate by 27Al and 29Si MAS NMR spectroscopy

Cement and Concrete Research

Volumn 34, Issue 5, 2004, Pages 857-868

  Andersen, Morten Daugaard ^a   Jakobsen, Hans J ^a   Skibsted, Jørgen ^a  

^a AARHUS UNIVERSITY   (Denmark)

Author keywords

Acceleration; Admixture; Calcium silicate hydrate; Portland cement; Spectroscopy

Indexed keywords

ADDITIVES; CARBOXYLIC ACIDS; CLAY MINERALS; CRYSTAL STRUCTURE; HYDRATION; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; OIL WELLS; SILICON COMPOUNDS; SODIUM COMPOUNDS;

ADMIXTURES; CALCIUM-SILICATE-HYDRATE; CLINKER MATERIALS; MAGIC-ANGLE SPINNING (MAS);

PORTLAND CEMENT;

EID: 1942535717     PISSN: 00088846     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.cemconres.2003.10.009     Document Type: Article

References (31)

1. Young J.F. A review of the mechanisms of set-retardation in Portland cement pastes containing organic admixtures. Cem. Concr. Res. 2:1972;415-433.
2. Thomas N.L., Birchall J.D. The retarding action of sugars on cement hydration. Cem. Concr. Res. 13:1983;830-842.
3. Thomas N.L., Double D.D. Calcium and silicon concentrations in solution during the early hydration of Portland cement and tricalcium silicate. Cem. Concr. Res. 11:1981;675-687.
4. Taylor H.F.W. Cement Chemistry. 2nd ed. 1997;Thomas Telford, London.
5. Double D.D. New developments in understanding the chemistry of cement hydration. Philos. Trans. R. Soc. Lond. A. 310:1983;53-66.
6. Wilding C.R., Walter A., Double D.D. A classification of inorganic and organic admixtures by conduction calorimetry. Cem. Concr. Res. 14:1984;185-194.
7. Kantro D.L. Tricalcium silicate hydration in the presence of various salts. J. Test. Eval. 3:1975;312-321.
8. 29Si MAS NMR studies of Portland cement components and effects of microsilica on the hydration reaction. Cem. Concr. Res. 18:1988;789-798.
9. 29Si MAS NMR study of the hydration of tricalcium silicate in the presence of finely divided silica. J. Mater. Sci. 23:1988;4108-4114.
10. 29Si MAS NMR study of the pozzolanic activity of condensed silica fume and the hydration of di- and tricalcium silicates. Adv. Cem. Res. 3:1990;111-116.
11. Justnes H. Accelerated hardening of mortars hydraulic binders of silica fume/lime. Nord. Concr. Res. 17:1995;30-41.
12. 27Al MAS NMR spectroscopy. Adv. Cem. Res. 15:2003;103-112.
13. Lota J.S., Bensted J., Pratt P.L. Effect of sodium aluminate on class G oilwell cement hydration at low and ambient temperatures. Proc. 10th Int. Congr. Chem. Cem., Gothenburg, Sweden. vol. 3:1997;. (paper 3iii014).
14. 29Si MAS NMR spectroscopy. J. Chem. Soc. Faraday Trans. 91:1995;4423-4430.
15. 29Si MAS NMR spectroscopy. Proc. 10th Int. Congr. Chem. Cem., Gothenburg, Sweden. vol. 2:1997;. (paper 2ii56).
16. 27Al MAS NMR spectroscopy. Inorg. Chem. 32:1993;1013-1027.
17. 27Al MAS NMR spectroscopy. J. Chem. Soc. Faraday Trans. 90:1994;2095-2098.
18. 27Al NMR and EELS. J. Am. Ceram. Soc. 76:1993;2285-2288.
19. 29Si MAS NMR investigation. Inorg. Chem. 42:2003;2280-2287.
20. Richardson I.G. The nature of C-S-H in hardened cements. Cem. Concr. Res. 29:1999;1131-1147.
21. 29Si MAS NMR study of the structure of calcium silicate hydrate. Adv. Cem. Based Mater. 3:1996;144-156.
22. 17O MAS NMR investigation of the structure of calcium silicate hydrate gel. J. Am. Ceram. Soc. 79:1996;1585-1592.
23. Skibsted J., Nielsen N.C., Bildsøe H., Jakobsen H.J. Satellite transitions in MAS NMR spectra of quadrupolar nuclei. J. Magn. Reson. 95:1991;88-117.
24. Clayden N.J., Dobson C.M., Groves G.W., Hayes C.J., Rodger S.A. Solid state NMR studies of cement hydration. Proc. Br. Ceram. Soc. 35:1984;55-65.
25. Diamond S. The microstructures of cement paste in concrete. Proc. 8th Int. Congr. Chem. Cem., Rio de Janeiro, Brazil. 1:1986;122-147.
26. Grutzeck M.W. A new model for the formation of calcium silicate hydrate (C-S-H). Mater. Res. Innov. 3:1999;160-170.
27. Richardson I.G., Groves G.W. The structure of the calcium silicate hydrate phases present in hardened pastes of white Portland cement/blast-furnace slag blends. J. Mater. Sci. 32:1997;4793-4802.
28. Famy C., Scrivener K.L., Atkinson A., Brough A.R. Effects of an early or a late heat treatment on the microstructure and composition of inner C-S-H products of Portland cement mortars. Cem. Concr. Res. 32:2002;269-278.
29. 27Al magic angle nuclear magnetic resonance study of the aluminum incorporation in calcium silicate hydrates. J. Am. Chem. Soc. 120:1998;12075-12082.
30. Faucon P., Delagrave A., Petit J.C., Richet C., Marchand J.M., Zanni H. Aluminum incorporation in calcium silicate hydrates (C-S-H) depending on their Ca/Si ratio. J. Phys. Chem. B. 103:1999;7796-7802.
31. 2O systems. Adv. Cem. Res. 11:1999;179-187.