Characterization of branched ultrahigh molar mass polymers by asymmetrical flow field-flow fractionation and size exclusion chromatography

Journal of Chromatography A

Volumn 1218, Issue 27, 2011, Pages 4257-4267

  Otte, T ^a,c   Pasch, H ^b   Macko, T ^c   Brull R ^c   Stadler, F J ^d   Kaschta, J ^e   Becker, F ^f   Buback, M ^f  

^a Postnova Analytics GmbH   (Germany)

^b STELLENBOSCH UNIVERSITY   (South Africa)

^c FRAUNHOFER INSTITUTE FOR STRUCTURAL DURABILITY AND SYSTEM RELIABILITY LBF   (Germany)

^d Chonbuk National University   (South Korea)

^e UNIVERSITY OF ERLANGEN NUREMBERG   (Germany)

^f UNIVERSITY OF GÖTTINGEN   (Germany)

Author keywords

Branching; Field flow fractionation; Light scattering; Polybutadiene; Polyethylene; Polypropylene; Polystyrene; Shear degradation; Size exclusion chromatography; Ultrahigh molar masses

Indexed keywords

BRANCHING; FIELD FLOW FRACTIONATION; SHEAR DEGRADATION; SIZE EXCLUSION; ULTRAHIGH MOLAR MASSES;

CHARACTERIZATION; CRYSTALLINE MATERIALS; DEGRADATION; DIFFUSION; DISSOLUTION; FLOW FIELDS; FRACTIONATION; GEL PERMEATION CHROMATOGRAPHY; HIGH DENSITY POLYETHYLENES; HYDRODYNAMICS; LIGHT SCATTERING; LOW DENSITY POLYETHYLENES; MOLAR MASS; MOLECULES; POLYBUTADIENES; POLYMERS; POLYOLEFINS; POLYSTYRENES; PORE SIZE; REFRACTION; SHEAR FLOW;

SIZE EXCLUSION CHROMATOGRAPHY;

POLYBUTADIENE; POLYETHYLENE; POLYMER; POLYOLEFIN; POLYPROPYLENE; UNCLASSIFIED DRUG;

ARTICLE; CONTROLLED STUDY; CRYSTALLIZATION; DIFFUSION; DISSOLUTION; DISTRIBUTION VOLUME; ELUTION; FIELD FLOW FRACTIONATION; FLOW FIELD FLOW FRACTIONATION; GEL PERMEATION CHROMATOGRAPHY; HIGH TEMPERATURE; HYDRODYNAMICS; MATHEMATICAL ANALYSIS; MOLAR MASS DISTRIBUTION; MOLECULAR WEIGHT; PRIORITY JOURNAL; SEPARATION TECHNIQUE;

CHROMATOGRAPHY, GEL; DIFFUSION; FRACTIONATION, FIELD FLOW; LIGHT; MEMBRANES, ARTIFICIAL; MOLECULAR WEIGHT; PARTICLE SIZE; PLASTICS; POLYMERS; SCATTERING, RADIATION; TEMPERATURE;

EID: 79958858096     PISSN: 00219673     EISSN: 18733778     Source Type: Journal    
DOI: 10.1016/j.chroma.2010.12.072     Document Type: Article

References (45)

1. Trinkle S., Friedrich C. Rheol. Acta 2001, 40:322.
2. de Groot A.W., Hamre W.J. J. Chromatogr. 1993, 648:33.
3. Pang S., Rudin A. Polymer 1992, 33:1949.
4. Pang S., Rudin A. J. Appl. Polym. Sci. 1992, 46:763.
5. Sun T., Brant P., Chance R.R., Graessley W.W. Macromolecules 2001, 34:6812.
6. Wu S., Lilge D. J. Appl. Polym. Sci. 1993, 50:1753.
7. Jackson C., Chen Y.-J., Mays J.W. J. Appl. Polym. Sci. 1996, 61:865.
8. Friebe L., Nuyken O., Windisch H., Obrecht W. Macromol. Chem. Phys. 2002, 203:1055.
9. Kaulbach R., Gebauer U., Gehrke K., Lechner M.D., Hummel K. Angew. Makromol. Chem. 1995, 226:101.
10. Slagowski E.L., Fetters L.J., Mcintyre D. Macromolecules 1974, 7:394.
11. Barth H.G., Carlin F.J. J. Liq. Chromatogr. 1984, 7:1717.
12. Parth M., Aust N., Lederer K. Int. J. Polym. Anal. Charact. 2003, 8:175.
13. Aust N. J. Biochem. Biophys. Methods 2003, 56:323.
14. Wang P.J., Glasbrenner B.S. J. Liq. Chromatogr. 1987, 10:3047.
15. Zammit M.D. Polymer 1998, 39:5789.
16. Aust N., Parth M., Lederer K. Int. J. Polym. Anal. Charact. 2001, 6:245.
17. Zigon M., The N.K., Shuayo C., Grubisic-Gallot Z. J. Liq. Chromatogr. 1997, 20:2155.
18. Wyatt P.J. Anal. Chim. Acta 1993, 272:1.
19. Podzimek S., Vlcek T., Johann C. J. Appl. Polym. Sci. 2001, 81:1588.
20. Podzimek S., Vlcek T. J. Appl. Polym. Sci. 2001, 82:454.
21. Stadler F.J., Kaschta J., Münstedt H., Becker F., Buback M. Rheol. Acta 2009, 48:479.
22. Wintermantel M., Antonietti M., Schmidt M. J. Appl. Polym. Sci.: Appl. Polym. Symp. 1993, 52:91.
23. Johann C., Kilz P. J. Appl. Polym. Sci.: Appl. Polym. Symp. 1991, 48:111.
24. Frater D.J., Mays J.W., Jackson C.J. Polym. Sci. Part B: Polym. Phys. 1997, 35:141.
25. Gerle M., Fischer K., Roos S., Müller A.H.E., Schmidt M., Sheiko S.S., Prokhorova S.A., Möller M. Macromolecules 1999, 32:2629.
26. Percec V., Ahn C.-H., Cho W.-D., Jamieson A.M., Kim J., Leman T., Schmidt M., Gerle M., Möller M., Prokhorova S.A., Sheiko S.S., Cheng S.Z.D., Zhang A., Ungar G., Yeardley D.J.P. J. Am. Chem. Soc. 1998, 120:8619.
27. Giddings J.C. Sep. Sci. 1966, 1:123.
28. Caldwell K.D., Kesner L.F., Myers M.N., Giddings J.C. Science 1972, 176:296.
29. Liu G., Giddings J.C. Chromatographia 1992, 34:483.
30. Wahlund K.-G., Giddings J.C. Anal. Chem. 1987, 59:1332.
31. Kirkland J.J., Yau W.W., Szoka F.C. Science 1982, 215:296.
32. Giddings J.C., Myers N.M., Caldwell K.D. J. Sep. Sci. Technol. 1981, 16:549.
33. Ratanathanawongs-Williams S.K. Field-Flow Fractionation Handbook 2000, vol. 720:257-278. Wiley & Sons, New York.
34. Ratanathanawongs-Williams S.K., Lee D. J. Sep. Sci. 2006, 29:1720.
35. Oh S., Kang D., Ahn S.M., Simpson R.J., Lee B.H., Moon M.H. J. Sep. Sci. 2007, 30:1082.
36. Wahlund K.-G., Zattoni A. Anal. Chem. 2002, 74:5621.
37. Bang D.Y., Shin D.Y., Lee S., Moon M.H. J. Chromatogr. A 2007, 1147:200.
38. Yohannes G., Shan J., Jussila M., Nupponen M., Tenhu H., Riekkola M.L. J. Sep. Sci. 2005, 28:435.
39. Miller M.E., Giddings J.C. J. Microcolumn. Sep. 1998, 10:75.
40. Mes E.P.C., de Jonge H., Klein T., Welz R., Gillespie D.T. J. Chromatogr. A 2007, 1154:319.
41. Coto B., Escola J.M., Suarez I., Caballero M.J. Polym. Test. 2007, 26:568.
42. Mori S., Ishikawa M. J. Liq. Chromatogr. Rel. Technol. 1998, 21:1107.
43. Angelo R.J., Ikeda R.M., Wallach M.L. Polymer 1965, 6:141.
44. Otte T., Brüll R., Macko T., Pasch H. J. Chromatogr. A 2010, 1217:722.
45. Le Guillou J.C., Zinn-Justin J. Phys. Rev. Lett. 1977, 39:95.