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Compounds 1, 2, 4, and 5 are obtained as pure phases, while 3 is the minor phase, with the main phase being a crystallized powder which has not been characterized
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Compounds 1, 2, 4, and 5 are obtained as pure phases, while 3 is the minor phase, with the main phase being a crystallized powder which has not been characterized.
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note
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max = 60°, 16174 measured reflns, 2307 unique reflns (R (int) = 0.031), R (F) = 0.021 (1702 reflns, I /σ(I) > 2, 95 parameters), wR2(F2) = 0.038 (all data).
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-4 M) with TBAP (0.1 M) as the supporting electrolyte. The voltammograms were recorded on a Biologic SP150 potentiostat with positive feedback compensation. Based on repetitive measurements, absolute errors on potentials were estimated to be ≈ ± 5 mV
-
-4 M) with TBAP (0.1 M) as the supporting electrolyte. The voltammograms were recorded on a Biologic SP150 potentiostat with positive feedback compensation. Based on repetitive measurements, absolute errors on potentials were estimated to be ≈ ± 5 mV.
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