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max = 56°; final R indices [I > 2σ(I)], R1 = 0.0244, wR2 = 0.0596: R indices (all data). R1 = 0.0263, wR2 = 0.0589. The structure was solved by direct methods and refined by full-matrix least-squares calculations. The thermal motion of all atoms was treated anisotropically. No attempts were made to locate hydrogen atoms, All calculations were made using the Siemens SHELXTL crystallographic package.
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