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79957618862
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note
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2: Calcd (%): C 43.58, H 1.76, N, 10.16; Found (%): C 43.69, H 1.31, N 9.89. FT-IR (KBr pellet, cm-1): 2915 (m), 1652 (w), 1564 (m), 1543 (m), 1504 (s), 1238 (w), 1155 (m), 1097 (m), 930 (w), 915 (w), 806 (m), 718 (w), 650 (w), 469 (w).
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41
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0004150157
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2=0.0900 for 23612 reflections, 649 parameters, 0 restraints. Single-crystal X-ray diffraction data for 1 was collected on a Bruker-AXS Smart CCD single-crystal diffractometer with MoKα radiation (λ=0.71073 Å) at 293 K. The structure of 1 was solved by direct method using the program SHELXS-97 University of Göttingen: Göttingen
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2 using the SHELXL-97 crystallographic software package
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(1997)
SHELXS-97, Programs for X-ray Crystal Structure Solution
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Sheldrick, G.M.1
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