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-1, KBr): 3213s, 3054m, 2940m, 2360.10, 2085vs, 2071vs, 1530m, 1452s, 1418s, 1311m, 1277w, 1231w, 761.19s, 753.00s, 743.21s, 436w.
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2 = 0.0598. CCDC = 292525. Data were collected on a Bruker ApexII CCD diffractometer with graphite-monochromated Mo Kα radiation (λ = 0.71073 Å). The structures were solved with direct methods and refined with full-matrix least-squares (SHELX-97).
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