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3 has been studied in detail
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3 has been studied in detail. In alkaline solution (≤15% NaOH), the yield of PH;b may reach ca. 80% using a lead cathode at temperatures above 70â°C. See Ref. [10] and, H. Tsuchiya, A. Otsuji, Yu. Sakagami, (Heisei), Jpn. Pat. 01139781A2 19890601, 1989.
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1H} NMR spectra also allowed the number of protons attached to phosphorus to be evaluated directly from the signal at δ=-17.55 ppm, confirming the presence of three protons per phosphorus
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1H} NMR spectra also allowed the number of protons attached to phosphorus to be evaluated directly from the signal at δ=-17.55 ppm, confirming the presence of three protons per phosphorus.
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18
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3PO could not be obtained owing to its quick decomposition under the working condition of the mass spectrometer.
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3PO could not be obtained owing to its quick decomposition under the working condition of the mass spectrometer.
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2, respectively (Supporting Information). The presence of these contaminants has hampered the growth of crystals suitable for a crystallographic study for either 4 or 5
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2, respectively (Supporting Information). The presence of these contaminants has hampered the growth of crystals suitable for a crystallographic study for either 4 or 5.
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