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Tetrahedron Letters

Volumn 52, Issue 21, 2011, Pages 2776-2779

Microwave-assisted methylation of phenols with DMF-DMA

(4) Belov, Pavel a Campanella, Veronica L a Smith, Alison W a Priefer, Ronny a

a NIAGARA UNIVERSITY (United States)

Author keywords

[No Author keywords available]

Indexed keywords

CARBOXYLIC ACID; KETONE; METHYL GROUP; N,N DIMETHYLACETAMIDE; N,N DIMETHYLFORMAMIDE; N,N DIMETHYLFORMAMIDE DIMETHYLACETAL; PHENOL; UNCLASSIFIED DRUG;

ARTICLE; CHEMICAL REACTION KINETICS; ESTERIFICATION; METHYLATION; MICROWAVE IRRADIATION;

EID: 79955480567 PISSN: 00404039 EISSN: None Source Type: Journal
DOI: 10.1016/j.tetlet.2011.03.111 Document Type: Article

Times cited : (19)

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- 4, filtered, and concentrated under reduced pressure. Column chromatography (9:1 hexanes/EtOAc) afforded a 4-methylanisole (0.44 g, 78%) as clear colorless liquid. The same procedure was followed for para-substituted electron withdrawing groups with to only exception being the reaction time was decreased to a total of 30 min.

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