Homoleptic copper(I) phenylselenolate polymer as a single-source precursor for Cu2Se nanocrystals. Structure, photoluminescence and application in field-effect transistor

Chemical Science

Volumn 1, Issue 4, 2010, Pages 515-518

  Low, Kam Hung ^a   Li, Cheng Hui ^b   Roy, Vellaisamy A L ^c   Chui, Stephen Sin Yin ^a   Chan, Sharon Lai Fung ^a   Che, Chi Ming ^a,b  

^a UNIVERSITY OF HONG KONG   (Hong Kong)

^b NANJING UNIVERSITY   (China)

^c CITY UNIVERSITY OF HONG KONG   (Hong Kong)

Author keywords

[No Author keywords available]

Indexed keywords

COMPLEX 1; HOMOLEPTIC; INERT ATMOSPHERES; POLYMERIC STRUCTURES; POWDER X RAY DIFFRACTION; REGIO-REGULAR; SINGLE PRECURSORS; SINGLE-SOURCE PRECURSOR;

FIELD EFFECT TRANSISTORS; HOLE MOBILITY; X RAY DIFFRACTION;

POLYMERS;

EID: 79954450272     PISSN: 20416520     EISSN: 20416539     Source Type: Journal    
DOI: 10.1039/c0sc00212g     Document Type: Article

References (44)

1. D. Tanaka, K. Nakagawa, M. Higuchi, S. Horike, Y. Kubota, T. C. Kobayashi, M. Takata and S. Kitagawa, Angew. Chem., Int. Ed., 2008, 47, 3914
2. P. Horcajada, T. Chalati, C. Serre, B. Gillet, C. Sebrie, T. Baati, J. F. Eubank, D. Heurtaux, P. Clayette, C. Kreuz, J.-S. Chang, Y. K. Hwang, V. Marsaud, P. N. Bories, L. Cynober, S. Gil, G. Ferey, P. Coureur and R. Gref, Nat. Mater., 2009, 1, 1
3. Q. Li, W. Zhang, O. S. Miljanic, C.-H. Sue, Y.-L. Zhao, L. Liu, C. B. Knobler, J. F. Stoddart and O. M. Yaghi, Science, 2009, 325, 855
4. T. Tozawa, J. T. A. Jones, S. I. Swamy, S. Jiang, D. J. Adams, S. Shakespeare, R. Clowes, D. Bradshaw, T. Hasell, S. Y. Chong, C. Tang, S. Thompson, J. Parker, A. Trewin, J. Bacsa, A. M. Z. Slawin, A. Steiner and A. I. Cooper, Nat. Mater., 2009, 8, 973
5. N. Rosi, J. Eckert, M. Eddaoudi, D. T. Vodak, J. Kim, M. OKeeffe and O. M. Yaghi, Science, 2003, 300, 1127
6. B. Kesanli and W. Lin, Coord. Chem. Rev., 2003, 246, 305
7. B. Tell, P. M. Bridenbaugh and H. M. Kasper, J. Appl. Phys., 1976, 47, 619
8. W. S. Chen, J. M. Stewart and R. A. Mickelsen, Appl. Phys. Lett., 1985, 46, 1095
9. S. Niki, P. J. Fons, A. Yamada, Y. Lacroix, H. Shibata, H. Oyanagi, M. Nishitani, T. Negami and T. Wada, Appl. Phys. Lett., 1999, 74, 1630
10. T. Ohtani, M. Motoki, K. Koh and K. Ohshima, Mater. Res. Bull., 1995, 30, 1495
11. R. N. Bhattacharya, A. M. Fernandez, M. A. Contreras, J. Keane, A. L. Tennant, K. Ramanathan, J. R. Tuttle, R. N. Noufi and A. M. Hermann, J. Electrochem. Soc., 1996, 143, 854
12. W. Wang, Y. Geng, P. Yan, F. Liu, Y. Xie and Y. Qian, J. Am. Chem. Soc., 1999, 121, 4062
13. W. Wang, P. Yan, F. Liu, Y. Xie, Y. Geng and Y. Qian, J. Mater. Chem., 1998, 8, 2321
14. Z. Qiao, Y. Xie, J. Xu, X. Liu, Y. Zhu and Y. Qian, Can. J. Chem., 2000, 78, 1143
15. J. Zhu, O. Palchik, S. Chen and A. Gedanken, J. Phys. Chem. B, 2000, 104, 7344
16. Y. Xie, X. Zheng, X. Jiang, J. Lu and L. Zhu, Inorg. Chem., 2002, 41, 387
17. S. Xu, H. Wang, J.-J. Zhu and H.-Y. Chen, J. Cryst. Growth, 2002, 234, 263
18. Y. Cheng, T. J. Emge and J. G. Brennan, Inorg. Chem., 1996, 35, 7339.
19. M. Bettenhausen, A. Eichhofer, D. Fenske and M. Semmelmann, Z. Anorg. Allg. Chem., 1999, 625, 593
20. S. Dehnen, A. Eichhofer and D. Fenske, Eur. J. Inorg. Chem., 2002, 279
21. M. Semmelmann, D. Fenske and J. F. Corrigan, J. Chem. Soc., Dalton Trans., 1998, 2541
22. A. Tonejc, J. Mater. Sci., 1980, 15, 3090
23. O. C. Kopp and O. B. Cavin, J. Cryst. Growth, 1984, 67, 391
24. T. G. Back, S. Collins, M. V. Krishna and K. W. Law, J. Org. Chem., 1987, 52, 4258
25. X. Jin, K. Tang, Y. Long and Y. Tang, Acta Crystallogr., Sect. C: Cryst. Struct. Commun., 1999, 55, 1799
26. N. Zhu and D. Fenske, J. Chem. Soc., Dalton Trans., 1999, 1067
27. S. G. Murray and F. R. Hartley, Chem. Rev., 1981, 81, 365
28. C.-M. Che, C.-H. Li, S. S.-Y. Chui, V. A. L. Roy and K.-H. Low, Chem.-Eur. J., 2008, 14, 2965
29. Orthorhombic Cu2Se: 62.61 wt% Cu, 37.39 wt% Se; cubic Cu2Se: 62.53 wt% Cu, 37.47 wt% Se. These values correspond to a Cu : Se ratio of 2.07-2.08 : 1. Inductively coupled plasma mass spectrometry (ICP-MS) analysis showed that a 5.39 mg sample of the orthorhombic Cu2Se nanocrystals contained 3.34 mg of copper; 0.6% more than the theoretical value of 61.68% (3.32 mg) for a formula of Cu2Se
30. P. Scherrer, Nachr. Ges. Wiss. Gottingen, 1918, 26, 98
31. J. I. Langford and A. J. C. Wilson, J. Appl. Crystallogr., 1978, 11, 102
32. Y.-B. Dong, J.-P. Ma, M. D. Smith, R.-Q. Huang, B. Tang, D. Chen and H.-C. zur Loye, Solid State Sci., 2002, 4, 1313
33. E. Fournier, F. Lebrun, M. Drouin, A. Decken and P. D. Harvey, Inorg. Chem., 2004, 43, 3127
34. S. S. Y. Chui, M. F. Y. Ng and C.-M. Che, Chem.-Eur. J., 2005, 11, 1739
35. V. Kumar, S. K. Sharma, T. P. Sharma and V. Singh, Opt. Mater., 1999, 12, 115
36. V. W.-W. Yam, K. K.-W. Lo and K.-K. Cheung, Inorg. Chem., 1996, 35, 3459
37. B. Ong, Y. Wu, L. Jiang, P. Liu and K. Murti, Synth. Met., 2004, 142, 49
38. V. Podzorov, E. Menard, A. Borissov, V. Kiryukhin, J. A. Rogers and M. E. Gershenson, Phys. Rev. Lett., 2004, 93, 086602
39. V. A. L. Roy, Y.-G. Zhi, Z.-X. Xu, S.-C. Yu, P. W. H. Chan and C.-M. Che, Adv. Mater., 2005, 17, 1258
40. P. Stallinga, H. L. Gomes, F. Biscarini, M. Murgia and D. M. de Leeuw, J. Appl. Phys., 2004, 96, 5277
41. H. L. Gomes, P. Stallinga, F. Dinelli, M. Murgia, F. Biscarini, D. M. de Leeuw, M. Muccini and K. Mullen, Polym. Adv. Technol., 2005, 16, 227
42. M. B. Solomon, in Physics of Superionic Conductors, Springer-Verlag, Berlin, Germany 1979, p. 175
43. R. S. Mane, S. P. Kajve, C. D. Lokhande and S.-H. Han, Vacuum, 2006, 80, 631
44. S. K. Haram and K. S. V. Santhanam, J. Electroanal. Chem., 1995, 396, 63