Qualitative and quantitative analysis of Fructus Corni using ultrasound assisted microwave extraction and high performance liquid chromatography coupled with diode array UV detection and time-of-flight mass spectrometry

Journal of Pharmaceutical and Biomedical Analysis

Volumn 55, Issue 3, 2011, Pages 557-562

  Liu, Zhirui ^a   Zhu, Zhenyu ^a   Zhang, Hai ^b   Tan, Guangguo ^a   Chen, Xiaofei ^a   Chai, Yifeng ^a  

^a SECOND MILITARY MEDICAL UNIVERSITY   (China)

^b EASTERN HEPATOBILIARY SURGERY HOSPITAL   (China)

Author keywords

Fructus Corni; High performance liquid chromatography; Time of flight mass spectrometry; Ultrasound assisted microwave extraction (UAME)

Indexed keywords

CORNUS OFFICINALIS EXTRACT; FRUCTUS CORNI EXTRACT; GALLIC ACID; IRIDOID; LOGANIN; METHANOL; PHENOL DERIVATIVE; PROTOCATECHUIC ACID; SWEROSIDE; UNCLASSIFIED DRUG;

AQUEOUS SOLUTION; ARTICLE; CHINESE MEDICINE; DIODE; FRUIT; HABITAT; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; PRIORITY JOURNAL; QUALITATIVE ANALYSIS; QUANTITATIVE ANALYSIS; TIME OF FLIGHT MASS SPECTROMETRY; ULTRASOUND; ULTRAVIOLET RADIATION;

CALIBRATION; CHROMATOGRAPHY, HIGH PRESSURE LIQUID; CORNUS; DRUGS, CHINESE HERBAL; FRUIT; LIMIT OF DETECTION; MICROWAVES; MOLECULAR STRUCTURE; QUALITY CONTROL; REFERENCE STANDARDS; REPRODUCIBILITY OF RESULTS; SONICATION; SPECTROMETRY, MASS, ELECTROSPRAY IONIZATION;

EID: 79953201827     PISSN: 07317085     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.jpba.2011.02.007     Document Type: Article

References (17)

1. Chen C.C., Hsu C.Y., Chen C.Y., Liu H.K. Fructus Corni suppresses hepatic gluconeogenesis related gene transcription, enhances glucose responsiveness of pancreatic beta-cells, and prevents toxin induced beta-cell death. J. Ethnopharmacol. 2008, 117:483-490.
2. Ding X., Wang M.Y., Yao Y.X., Li G.Y., Cai B.C. Protective effect of 5-hydroxymethylfurfural derived from processed Fructus Corni on human hepatocyte LO2 injured by hydrogen peroxide and its mechanism. J. Ethnopharmacol. 2010, 128:373-376.
3. Qi M.Y., Liu H.R., Dai D.Z., Li N., Dai Y. Total triterpene acids, active ingredients from Fructus Corni, attenuate diabetic cardiomyopathy by normalizing ET pathway and expression of FKBP12.6 and SERCA2a in streptozotocin-rats. J. Pharm. Pharmacol. 2008, 60:1687-1694.
4. Su W., Dai D.Z., Liu H.R., Na T., Dai Y. Upregulated endothelin system in diabetic vascular dysfunction and early retinopathy is reversed by CPU0213 and total triterpene acids from Fructus Corni. Clin. Exp. Pharmacol. Physiol. 2007, 34:1228-1233.
5. Tianniam S., Bamba T., Fukusaki E. Non-targeted metabolite fingerprinting of oriental folk medicine Angelica acutiloba roots by ultra performance liquid chromatography time-of-flight mass spectrometry. J. Sep. Sci. 2009, 32:2233-2244.
6. Pharmacopoeia Commission of PRC Pharmacopoeia of the People's Republic of China 2010, vol. 1. Chemical Industry Press, Beijing, pp. 25-26.
7. Yang Y., Liu C., Liu J., Wang Y., Zhang Z. Chemical studies on the polysaccharide in Fructus Corni. Zhongguo Zhong Yao Za Zhi 1999, 24:614-616.
8. Li K.M., Yang X.J., Yu M.Q., Xie C., Xu L.Z. Determination of loganin in Cornus officinalis Sieb. et Zucc. by TLC scanner. Zhongguo Zhong Yao Za Zhi 1994, 19:738-763.
9. Wang S.F., Chen X.G., Hu Z.D., Ju Y. Analysis of three effective components in Fructus corni and its preparations by micellar electrokinetic capillary chromatography. Biomed. Chromatogr. 2003, 17:306-311.
10. Wang R., Wang S.M., Liang S.W., Xu G.W., Weng Q.F. Separation and determination of oleanolic acid and ursolic acid from Cornus officinalis by capillary electrophoresis. Zhong Yao Cai 2007, 30:946-950.
11. Gu S., Xie C., Zhang D., Yang S., Xu L. Determination of loganin in the fruit of Cornus officinalis Sieb. et Zucc. Zhongguo Zhong Yao Za Zhi 1996, 21:429-448.
12. Du W., Cai H., Wang M., Ding X., Yang H., Cai B. Simultaneous determination of six active components in crude and processed Fructus Corni by high performance liquid chromatography. J. Pharm. Biomed. Anal. 2008, 48:194-197.
13. Yin M., Lin C., Wu H., Tsao S., Hsu C. Apoptotic effects of protocatechuic acid in human breast, lung, liver, cervix, and prostate cancer cells: potential mechanisms of action. J. Agric. Food Chem. 2009, 14:6468-6473.
14. Sunghwa F., Sakurai H., Saiki I., Koketsu M. Iodine-catalyzed etherification of morroniside. Chem. Pharm. Bull. 2009, 57:112-115.
15. Chen Y., Gu X., Huang S.Q., Li J., Wang X., Tang J. Optimization of ultrasonic/microwave assisted extraction (UAME) of polysaccharides from Inonotus obliquus and evaluation of its anti-tumor activities. Int. J. Biol. Macromol. 2010, 46:429-435.
16. Lou Z., Wang H., Zhu S., Zhang M., Gao Y., Ma C., Wang Z. Improved extraction and identification by ultra performance liquid chromatography tandem mass spectrometry of phenolic compounds in burdock leaves. J. Chromatogr. A 2010, 1217:2441-2446.
17. Zhou L., Liu Z., Wu G., Song F., Liu S. Analysis on iridoid glycosides in crude and processed extracts from cornus officinals by liquid chromatography-electrospray lonization mass spectrometry. Huaxue Xuebao 2008, 66:2712-2716.