A novel eight-connected metal-organic replica of CsCl based on heptanuclear zinc clusters

Inorganic Chemistry Communications

Volumn 14, Issue 4, 2011, Pages 562-565

  Zhu, Xiaofei ^a   Zhang, Hong ^a   Luo, Yuhui ^a   Pang, Yu ^a   Tian, Dan ^a  

^a NORTHEAST NORMAL UNIVERSITY   (China)

Author keywords

5 nitro 1,2,3 benzenetricarboxylate; bpp; Coordination polymer; Luminescent property

Indexed keywords

EID: 79952534225     PISSN: 13877003     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.inoche.2011.01.025     Document Type: Article

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48. 2O (15 mL) was stirred for 2 h to the clean solution and then sealed in a 25-mL Teflon-lined stainless steel vessel. After heated for 3 days at 160 °C and cooled at a rate of 5 °C/h to room temperature, colorless block crystals of 1 were separated in 63.6% yield based on Zn. Anal. Calcd (%) for 1 (C62H42Zn7N8O36): C 38.53, H 2.19, N 5.80; found: C 38.21, H 2.09, N 5.74. IR (KBr, cm-1): 3477 m, 3094 m, 1618 s, 1432 m, 1349 m, 1025 m, 861 m, 509 m.
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