Structure characterization and identification steroidal saponins from Ophiopogon japonicus Ker-Gawler (Liliaceae) by high-performance liquid chromatography with ion trap mass spectrometry

Phytochemical Analysis

Volumn 22, Issue 2, 2011, Pages 166-171

  Wang, Yongyi ^a   Xu, Jinzhong ^a   Qu, Haibin ^a  

^a NONE

Author keywords

Ophiopogon japonicus; Steroidal saponins

Indexed keywords

HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; ION CHROMATOGRAPHY; MASS SPECTROMETRY; METABOLITES;

ACTIVE CONSTITUENTS; FRAGMENTATION BEHAVIOR; HIGH-PERFORMANCE LIQUID CHROMATOGRAPHY; HPLC-ESI MS; ION-TRAP MASS SPECTROMETRY; OPHIOPOGON JAPONICUS; PHYTOCHEMICAL; STEROIDAL SAPONINS; STRUCTURE CHARACTERIZATION; STRUCTURE IDENTIFICATION;

CHROMOPHORES;

OPHIOGENIN; OPHIOPOGON ROOT; PENNOGENIN; RUSCOGENIN; SAPONIN; UNCLASSIFIED DRUG;

ANGIOSPERM; ARTICLE; CHEMICAL STRUCTURE; ELECTROSPRAY MASS SPECTROMETRY; FRAGMENTATION REACTION; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; ION TRAP MASS SPECTROMETRY; MASS SPECTROMETRY; NONHUMAN; OPHIOPOGON JAPONICUS; PHYTOCHEMISTRY; STRUCTURE ANALYSIS;

LILIACEAE; OPHIOPOGON JAPONICUS;

EID: 79951872498     PISSN: 09580344     EISSN: 10991565     Source Type: Journal    
DOI: 10.1002/pca.1263     Document Type: Article

References (13)

1. Zheng CN, Hao HP, Wang X, Wu XL, Wang GJ, Sang GW, Liang Y, Xie L, Xia CH, Yao XL. 2009. Diagnostic fragment-ion-based extension strategy for rapid screening and identification of serial components of homologous families contained in traditional Chinese medicine prescription using high-resolution LC-ESIIT-TOF/MS: Shengmai injection as an example. J Mass Spectrom 44: 230-244.
2. Zhang HJ, Wu YJ, Cheng YY. 2003. Analysis of 'SHENMAI' injection by HPLC/MS/MS. J Pharm Biomed Anal 31: 175-183.
3. Song XL, Gao GY, Ye LH. 1996. Effects of total saponin liriope spicata lour on experimental myocardial ischemia. Chin Pharmacol Bull 12: 329-332.
4. Zhou YH, Xu DS, Feng Y, Fang J, Xa HL, Liu J, Lu YQ, Ni JN, Xie QQ. 2003. Effects on Nutrition Blood Flow of Cardiac Muscle in Mice by Different Extracts in Radix Ophiopogonis. Chinese Journal of Experimental Traditional Medical Formulae 1: 22-23.
5. Fan J, Zhang XY, Zhang ZJ, Liang QL, Liu TL, Cai BC, Zhang X. 2007. Effects of different extracts from Ophiopogon japonicus on vascular endothelial cell damage induced by hydrogen peroxide. Chin J Pharmacol Toxicol 21: 131-133. (Pubitemid 46713944)
6. Bankefors J, Nord LI, Kenne L. 2008. Structural classification of acyl-substituted Quillaja saponins by electrospray ionisation ion trap multiple-stage mass spectrometry in combination with multivariate analysis. Rapid Commun Mass Spectrom 22: 3851-3860.
7. Li R, Zhou Y, Wu ZJ, Ding LS. 2006. ESI-QqTOF-MS/MS and APCI-IT-MS/MS analysis of steroid saponins from the rhizomes of Dioscorea panthaica. J Mass Spectrom 41: 1-22. (Pubitemid 43164830)
8. Liu YY, Li JB, He JM, Abliz Z, Qu J, Yu SS, Ma SG, Liu J, Du D. 2009. Identification of new trace triterpenoid saponins from the roots of Panax notoginseng by high-performance liquid chromatography coupled with electrospray ionization tandem mass spectrometry. Rapid Commun Mass Spectrom 23: 667-679.
9. Liu YY, Luo JG, Xu DR, Huang XF, Kong LY. 2008. Characterization of spirostanol saponins in Solanum torvum by high-performance liquid chromatography/evaporative light scattering detector/electrospray ionization with multi-stage tandem mass spectrometry. Rapid Commun Mass Spectrom 22: 2447-2452.
10. 27 Steroidal Glycosides from Ophiopogon japonicum. Acta Botanica Yunnanica 22: 97-102.
11. 27-steroidal glycoside fromOphiopogon japonicus. Chin Chem Lett 19: 82-84.
12. Kuroda M, Mimaki Y, Ori K, Sakagami H, Sashida Y. 2004. Steroidal Glycosides from the Bulbs of Ornithogalum thyrsoides. J Nat Prod 67: 1690-1696. (Pubitemid 39426123)
13. Domon B, Costello C. 1988. A Systematic Nomenclature for Carbohydrate Fragmentations in FAB-MS/MS Spectra of Glycoconjugates. J Glycoconj 5: 397-409. (Pubitemid 19031141)