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Volumn 21, Issue 7, 2010, Pages 778-781

Highly efficient synthesis of 2,3-dihydroquinazolin-4(1H)-ones catalyzed by heteropoly acids in water

Author keywords

2,3 dihydroquinazolin 4(1H) ones; Heteropoly acid; Water

Indexed keywords

EID: 79151475102 PISSN: 10018417 EISSN: None Source Type: Journal
DOI: 10.1016/j.cclet.2010.03.022 Document Type: Article

Times cited : (56)

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- General procedure for the synthesis of 2, 3-dihydroquinazolin-4(1H)-ones under aqueous conditions: anthranilamide (2 mmol) and aldehydes (2.1 mmol) was successively added to a solution of catalyst (7 mg) in water (4 mL) placed in a test tube and the reaction mixture was vigorous stirred at room temperature for 5-10 min. The progress of the reaction is monitored by TLC (thin layer chromatography)
- 4: C, 64.96; H, 5.77; N, 8.91; found: C, 65.03; H, 5.87; N, 8.82.

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