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note
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3] (2.5 mL). The resulting suspension was stirred at 140 °C for 15-20 min. After cooling to 100 °C, the reaction mixture was diluted with EtOH (5 mL) resulting in precipitation of the product. The mixture was then cooled to room temperature with stirring. The precipitated product was collected by filtration, washed with EtOH and dried under vacuum. NMR data and mp as above.
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