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78651386925
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note
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2 (mmol) was added. The reaction mixture was stirred for 1-1.5 h at ambient temperature, then treated with aqueous HCl and extracted with toluene (7 mL). The organic layer was passed through a short column of silica gel. The products 1 or 3 and [60]fullerene were separated by preparative HPLC using toluene as the eluent.
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18).
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78651388769
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note
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16).
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78651402203
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note
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18).
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78651385766
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16).
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0029309154
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King, R.C.8
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