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- 1) for compound 1: 3288 (s), 1520 (vs), 1448(s), 1403 (vs), 1154 (s), 946 (m), 854 (w), 759 (m), 665 (s), 481 (m).
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17
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78651327359
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note
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- 1, R1(wR2) = 0.0323 (0.0735) and S = 1.086 for 1272 reflections with I > 2σ(I). The structure was solved by direct methods and difference Fourier syntheses. Non-hydrogen atoms were refined anisotropically, and all hydrogen atoms were placed at ideal positions and allowed to ride. The crystallographic calculations were conducted using the SHELXL-97 programs.
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