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78651338418
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note
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1H NMR(CDCl3, δ, ppm): 8.87 (s, 1H, H-4), 8.64 (d, 1H, J = 5.4, H-6′), 8.32 (d, 1H, J = 8.2, H-3′), 7.87-7.82 (m, 2H, Aryl-H), 7.63 (t, 1H, J = 8.4, Aryl-H), 7.42-7.34 (m, 3 H, Aryl-H).
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27
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78651310005
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note
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+).
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28
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78651296843
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note
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+).
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29
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78651277642
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note
-
2 = 0.0755 (I > 2σ (I)); R1 = 0.0324, wR2 = 0.0766 (for all data). The diffraction data were collected with a Bruker Smart Apex CCD area detector with graphite-monochromatized Mo-Kα radiation (λ = 0.71073 Å) at 185(2) K. The structure was solved by using the program SHELXL and Fourier difference techniques, and refined by full-matrix least-squares method on F2. All hydrogen atoms were added theoretically.
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30
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0034107424
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Thompson, M.E.10
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