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78651291630
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note
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-1, R (wR) = 0.0250 (0.0652) and GOF = 1.074 for 712 reflections with I > 2.00 σ(I). The crystal structure of 1 was solved by direct methods using the Siemens SHELXTL version 5 package of crystallographic software and refined by full-matrix least-squares techniques. Non-hydrogen atoms were located by difference Fourier maps and subjected to anisotropic refinement. All hydrogen atoms of carbon atoms were calculated in idealized positions and allowed to ride on their parent atoms.
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36
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78651314110
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note
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-1): 2930w, 2881w, 1555vs, 1450vs, 1460 s, 1315 s, 1241 m, 1153 m, 1070 s, 1025 m, 960w, 861w, 763 s, 698w, 599w, 531w.
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